Properties of Water-Based Slurries for Fabrication of Ceramic-Metal Composites by Slip Casting Method

Author(s):  
M. Gizowska ◽  
K. Konopka ◽  
M. Szafran
Author(s):  
Justyna Zygmuntowicz ◽  
Joanna Łoś ◽  
Bernard Kurowski ◽  
Paulina Piotrkiewicz ◽  
Waldemar Kaszuwara

AbstractThe scope of work included the fabrication of ceramic-metal composites from the Al2O3-Cu and Al2O3-Cu-Mo and examining their microstructure and selected properties. The composites were fabricated by the slip casting method. The rheological behavior, microstructures, X-ray analysis, and mechanical properties were investigated. The rheological study demonstrated that all of the obtained slurries were non-Newtonian shear diluted fluids and stability on time. In both slurries, the flow limit is close to 0 Pa, which is very beneficial when casting the suspensions into molds. The X-ray analysis reveals Al2O3, Cu, and Mo phases in all specimens. No new phases were found in both types of composites after the sintering process. The results provided that the hardness for Al2O3-Cu-Mo composites was equal to 10.06 ± 0.49 GPa, while for Al2O3-Cu, it was equal to 6.81 ± 2.08 GPa. The K1C values measured, with the use of Niihara equation, for composites with and without the addition of Mo were equal to 6.13 ± 0.62 MPa m0.5 and 6.04 ± 0.55 MPa m0.5, respectively. It has been established that the mean specific wear rates of Al2O3-Cu and Al2O3-Cu-Mo samples were 0.35 × 10–5 ± 0.02 mm3 N−1 m−1 and 0.22 × 10–5 ± 0.04 mm3 N−1 m−1, respectively. It was found that molybdenum addition improved wear resistance properties of the composites.


Author(s):  
J. Zygmuntowicz ◽  
J. Kosiorek ◽  
P. Piotrkiewiecz ◽  
B. Zacharko ◽  
M. Wachowski ◽  
...  

AbstractA new ternary system of ceramic–metal composites has been fabricated from alumina, copper, and nickel powders by the slip casting method. The research aimed to avoid copper leaking during the sintering process of the formation while processing the CuNi phase. Five different compositions were examined, differing in the ratio of nickel to copper. Stable slurries with good casting properties were prepared for all compositions. The final composites after the sintering process were characterized by a homogeneous distribution of the metallic phase, but they differed in the microstructure characteristics. The addition of nickel limits the outflow of the liquid phase (copper) during sintering but does not eliminate it. This resulted in a reduction in the hardness of the samples compared to the reference material.


Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3510
Author(s):  
Marcin Wachowski ◽  
Justyna Zygmuntowicz ◽  
Robert Kosturek ◽  
Katarzyna Konopka ◽  
Waldemar Kaszuwara

In this study, ceramic–metal composites in the Al2O3/Ti/Ni system were fabricated using the slip casting method. Two series of composites with 15 vol.% metal content and different solid phase contents were obtained and examined. A proper fabrication process allows obtaining composites enhanced by intermetallic phases. The microstructure of the base powders, slurries, and sintered composites was analyzed by scanning electron microscope. Analysis of the sedimentation tendency of slurries was carried out. The phase composition of the sintered samples was examined by X-ray diffraction analysis. A monotonic compression test was used to investigate the mechanical properties of the composites. A fractography investigation was also carried out. The research conducted revealed that the slip casting method allows the obtaining of composites enhanced by intermetallic phases (TiNi, Ni3Ti). The results show the correlation between solid-phase content, microstructure, and mechanical properties of the composites.


Author(s):  
M N Halmy ◽  
S K Alias ◽  
M A Mat Shah ◽  
M K Maryam ◽  
M A Abu Bakar ◽  
...  

2006 ◽  
Vol 317-318 ◽  
pp. 143-146 ◽  
Author(s):  
Jing Long Li ◽  
Saburo Sano ◽  
Akihiro Tsuzuki ◽  
Akihiro Gotou ◽  
Yasuo Shibasaki ◽  
...  

Water-based slurries containing barium ferrite particles have been prepared and slip cast in magnetic field. This paper presents the characteristics of the suspensions in terms of Iso-Electric Points (IEP) and zeta potential that were evaluated through pH titration and polymer adsorption. Both enlarging the specific surface area of particles by planetary milling and adjusting the pH to low value apparently increase the zeta potentials. Stable slurry was obtained by adding polyethylene glycol (PEG) into the suspension at pH = 2 ~ 3.5. The steric repulsion plays key role in dispersion and PEG films served as insulative layers and mechanically kept particles from contact each other. The barium ferrite particles formed many stacks of plates during slip casting, which either aligned randomly without magnetic field applied or regularly aligned to form textured structure when magnetic field was applied.


2021 ◽  
Vol 4 (2) ◽  
pp. 64-67
Author(s):  
A.I.A. Termizi ◽  
J.J. Mohamed

Mambong pottery in Kuala Krai, Kelantan is one of the types of potteries in Malaysia other than Sayong, Terenang and Sarawak pottery. Mambong pottery was being made by traditional technique like pinching and throwing. In this research, Mambong pottery was made by using slip casting method. This method used porous mould which can absorb the water content from the clay slip. Different composition of water and clay was used and its effect on product properties was investigated. Samples with different composition of water and clay were labelled as 50C50W, 60C40W, 70C30W and 80C20W samples with addition of 0.7% of sodium silicate, Na2SiO3. The samples were characterized by its specific gravity (S.G.) of clay slip, drying and firing linear shrinkage, density and porosity and strength of the clay samples. Finding from this research showed that 70C30W sample is the optimum composition in fabricating pottery by using slip casting among other samples.


Author(s):  
Radosław Żurowski ◽  
Justyna Zygmuntowicz ◽  
Justyna Tomaszewska ◽  
Urszula Ulkowska ◽  
Paulina Piotrkiewicz ◽  
...  
Keyword(s):  

2014 ◽  
Vol 604 ◽  
pp. 293-296 ◽  
Author(s):  
Ludmila Mahnicka-Goremikina ◽  
Ruta Svinka ◽  
Visvaldis Svinka

The porous mullite ceramics doped with such metal oxides as ZrO2, WO3 and MgO in quantity of 5 wt% were prepared by slip casting method. The mullite phase was the main and dominant phase of ZrO2-, WO3- and MgO-doped samples, which were sintered at the temperatures of 1650°C, 1500°C, respectively. The ZrO2, WO3 and MgO had the positive effect on the increase of porosity and decrease of thermal conductivity of porous mullite ceramics and the degree of this effect was in the order of ZrO2<MgO<WO3.


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