scholarly journals Tailoring hydroxyapatite microspheres by spray-drying for powder bed fusion feedstock

2021 ◽  
Author(s):  
Pedro Navarrete-Segado ◽  
Christine Frances ◽  
David Grossin ◽  
Mallorie Tourbin
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Spray Drying ◽  
Laser Processing ◽  
Operating Conditions ◽  
Air Pressure ◽  
Final Particle ◽  
Powder Bed ◽  
Powder Feedstock

The present work deals with a study on the physical characteristics of hydroxyapatite microspheres produced by spray-drying process through different operating conditions. Obtained hydroxyapatite microspheres will be used as powder feedstock in powder bed selective laser processing additive manufacturing technologies where the flowability and the particle size distribution of the powder feedstock is of special importance. Spray air pressure and solid content of the slurries were the most influent parameters to control the final particle size distribution, while higher air pressure and temperatures gave the higher process recovery rate. The use of polyvinyl alcohol as organic binder increased the granules strength. The produced hydroxyapatite microspheres were found to fulfil the powder bed selective laser processing feedstock requirements, keeping the physico-chemical properties of the material. These promising results confirm the use of a spray dryer as an efficient method for the production of hydroxyapatite microspheres for powder bed selective laser processing.

Influence of particle size distribution and morphology on the properties of the powder feedstock as well as of AlSi10Mg parts produced by laser powder bed fusion (LPBF)

2020 ◽  
Vol 34 ◽  
pp. 101286 ◽  
Author(s):  
Kirstin Riener ◽  
Nikolaj Albrecht ◽  
Stefan Ziegelmeier ◽  
Robert Ramakrishnan ◽  
Lukas Haferkamp ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Powder Feedstock

scholarly journals Effect of Particle Size Distribution on Laser Powder Bed Fusion Manufacturability of Copper

2021 ◽  
Author(s):  
Massimiliano Bonesso ◽  
Pietro Rebesan ◽  
Claudio Gennari ◽  
Simone Mancin ◽  
Razvan Dima ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Physical And Mechanical Properties ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Cooling Channels ◽  
Scan Speed

AbstractOne of the major benefits of the Laser Powder Bed Fusion (LPBF) technology is the possibility of fabrication of complex geometries and features in only one-step of production. In the case of heat exchangers in particular, this is very convenient for the fabrication of conformal cooling channels which can improve the performance of the heat transfer capability. Yet, obtaining dense copper parts printed via LPBF presents two major problems: the high reflectivity of 1 μm (the wavelength of commonly used laser sources) and the high thermal conductivity of copper that limits the maximum local temperature that can be attained. This leads to the formation of porous parts.In this contribution, the influence of the particle size distribution of the powder on the physical and mechanical properties of parts produced via LPBF is studied. Three copper powders lots with different particle size distributions are used in this study. The effect on densification from two laser scan parameters (scan speed and hatching distance) and the influence of contours scans on the lateral surface roughness is reported. Subsequently, samples manufactured with the optimal process parameters are tested for thermal and mechanical properties evaluation.

scholarly journals Grinding Kinetics of Slag and Effect of Final Particle Size on the Compressive Strength of Alkali Activated Materials

Minerals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 714 ◽  
Author(s):  
Evangelos Petrakis ◽  
Vasiliki Karmali ◽  
Georgios Bartzas ◽  
Konstantinos Komnitsas
Keyword(s):  
Particle Size ◽  
Compressive Strength ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Ageing Time ◽  
Reduction Rate ◽  
Curing Temperature ◽  
Alkali Activation ◽  
Final Particle ◽  
Alkali Activated

This study aims to model grinding of a Polish ferronickel slag and evaluate the particle size distributions (PSDs) of the products obtained after different grinding times. Then, selected products were alkali activated in order to investigate the effect of particle size on the compressive strength of the produced alkali activated materials (AAMs). Other parameters affecting alkali activation, i.e., temperature, curing, and ageing time were also examined. Among the different mathematical models used to simulate the particle size distribution, Rosin–Rammler (RR) was found to be the most suitable. When piecewise regression analysis was applied to experimental data it was found that the particle size distribution of the slag products exhibits multifractal character. In addition, grinding of slag exhibits non-first-order behavior and the reduction rate of each size is time dependent. The grinding rate and consequently the grinding efficiency increases when the particle size increases, but drops sharply near zero after prolonged grinding periods. Regarding alkali activation, it is deduced that among the parameters studied, particle size (and the respective specific surface area) of the raw slag product and curing temperature have the most noticeable impact on the compressive strength of the produced AAMs.

A SIMULATION STUDY ON THE EFFECT OF PARTICLE SIZE DISTRIBUTION ON THE PRINTED GEOMETRY IN SELECTIVE LASER MELTING

2021 ◽  
pp. 1-14
Author(s):  
Vaishak Ramesh Sagar ◽  
Samuel Lorin ◽  
Johan Göhl ◽  
Johannes Quist ◽  
Christoffer Cromvik ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Layer Thickness ◽  
Selective Laser Melting ◽  
Laser Melting ◽  
Powder Bed ◽  
Mean Particle Size ◽  
Final Layer ◽  
Effect Of Particle Size

Abstract Selective laser melting (SLM) process is a powder bed fusion additive manufacturing process that finds applications in aerospace and medical industries for its ability to produce complex geometry parts. As the raw material used is in powder form, particle size distribution (PSD) is a significant characteristic that influences the build quality in turn affecting the functionality and aesthetics aspects of the product. This paper investigates the effect of PSD on the printed geometry for 316L stainless steel powder, where three coupled in-house simulation tools based on Discrete Element Method (DEM), Computational Fluid Dynamics (CFD), and Structural Mechanics are employed. DEM is used for simulating the powder bed distribution based on the different powder PSD. The CFD is used as a virtual testbed to determine thermal parameters such as heat capacity and thermal conductivity of the powder bed viewed as a continuum. The values found as a stochastic function of the powder distribution is used to analyse the effect on the melted zone and deformation using Structural Mechanics. Results showed that mean particle size and PSD had a significant effect on the packing density, melt pool layer thickness, and the final layer thickness after deformation. Specifically, a narrow particle size distribution with smaller mean particle size and standard deviation produced solidified final layer thickness closest to nominal layer thickness. The proposed simulation approach and the results will catalyze in development of geometry assurance strategies to minimize the effect of particle size distribution on the geometric quality of the printed part.

scholarly journals Plasma Spheroidisation of Irregular Ti6Al4V Powder for Powder Bed Fusion

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1763
Author(s):  
Nthateng Nkhasi ◽  
Willie du Preez ◽  
Hertzog Bissett
Keyword(s):  
Particle Size ◽  
Additive Manufacturing ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Metal Powder ◽  
Weight Ratio ◽  
High Strength ◽  
Powder Bed Fusion ◽  
Metal Powders ◽  
Powder Bed

Metal powders suitable for use in powder bed additive manufacturing processes should ideally be spherical, dense, chemically pure and of a specified particle size distribution. Ti6Al4V is commonly used in the aerospace, medical and automotive industries due to its high strength-to-weight ratio and excellent corrosion resistance properties. Interstitial impurities in titanium alloys have an impact upon mechanical properties, particularly oxygen, nitrogen, hydrogen and carbon. The plasma spheroidisation process can be used to spheroidise metal powder consisting of irregularly shaped particles. In this study, the plasma spheroidisation of metal powder was performed on Ti6Al4V powder consisting of irregularly shaped particles. The properties of the powder relevant for powder bed fusion that were determined included the particle size distribution, morphology, particle porosity and chemical composition. Conclusions were drawn regarding the viability of using this process to produce powder suitable for additive manufacturing.

Effect of Particle Size Distribution on the Deep-Bed Capture Efficiency of an Exhaust Particulate Filter

2014 ◽  
Author(s):  
Sandeep Viswanathan ◽  
Stephen S. Sakai ◽  
Mitchell Hageman ◽  
David E. Foster ◽  
Todd Fansler ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Particle Deposition ◽  
Operating Conditions ◽  
Particulate Filter ◽  
Particulate Emissions ◽  
Filter Loading ◽  
Particle Sizer ◽  
The Impact

The exhaust filtration analysis system (EFA) developed at the University of Wisconsin – Madison was used to perform micro-scale filtration experiments on cordierite filter samples using particulate matter (PM) generated by a spark-ignition direct injection (SIDI) engine fueled with gasoline. A scanning mobility particle sizer (SMPS) was used to characterize running conditions with four distinct particle size distributions (PSDs). The distributions selected differed in the relative number of accumulation versus nucleation mode particles. The SMPS and an engine exhaust particle sizer (EEPS) were used to simultaneously measure the PSD downstream of the EFA and the real-time particulate emissions from the SIDI engine to determine the evolution of filtration efficiency during filter loading. Cordierite filter samples with properties representative of diesel particulate filters (DPFs) were loaded with PM from the different engine operating conditions. The results were compared to understand the impact of particle size distribution on filtration performance as well as the role of accumulation mode particles on the diffusion capture of PM. The most penetrating particle size (MPPS) was observed to decrease as a result of particle deposition within the filter substrate. In the absence of a soot cake, the penetration of particles smaller than 70 nm was seen to gradually increase with time, potentially due to increased velocities in the filter as flow area reduces during filter loading, or due to decreasing wall area for capture of particles by diffusion. Particle re-entrainment was not observed for any of the operating conditions.

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