scholarly journals Microstructure Evaluation and Thermal–Mechanical Properties of ABS Matrix Composite Filament Reinforced with Multi-Walled Carbon Nanotubes by a Single Screw Extruder for FDM 3D Printing

2021 ◽  
Vol 11 (19) ◽  
pp. 8798
Author(s):  
Thai-Hung Le ◽  
Van-Son Le ◽  
Quoc-Khanh Dang ◽  
Minh-Thuyet Nguyen ◽  
Trung-Kien Le ◽  
...  
Keyword(s):  
Carbon Nanotubes ◽  
Fused Deposition Modeling ◽  
Acrylonitrile Butadiene Styrene ◽  
Melt Flow Index ◽  
Tensile Tests ◽  
Flow Index ◽  
Fused Deposition ◽  
Multi Walled Carbon Nanotubes ◽  
Walled Carbon Nanotubes ◽  
Composite Filament

This paper reports the synthesis of a new printable ABS–MWCNT composite filament, for use in fused deposition modeling (FDM), using an extrusion technique. Acrylonitrile butadiene styrene (ABS) and multi-walled carbon nanotubes (MWCNTs) were the initial materials used for fabricating the filaments. The MWCNTs were dispersed in ABS resin, then extruded through a single-shaft extruder in filament form, with MWCNT contents of 0.5%, 1%, 1.5%, 2%, 3% or 4% by weight. After extrusion, the diameter of the filaments was about 1.75 mm, making them appropriate for FDM. The as-synthesized filaments were then used in FDM to print out samples, on which tensile tests and other analyses were carried out. The results demonstrate that the sample with 2% MWCNTs had the highest strength value, 44.57 MPa, comprising a 42% increase over that of the pure ABS sample. The morphology and dispersion of MWCNTs in the composite were observed by field emission scanning electron microscopy (FESEM), demonstrating the uniform distribution of MWCNTs in the ABS matrix. The thermal behavior results indicated no significant change in the ABS structure; however, the melt flow index of the filaments decreased with an increase in the MWCNT content.

Optical Humidity Sensor Based on Tapered Fiber with Multi-walled Carbon Nanotubes Slurry

2017 ◽  
Vol 6 (1) ◽  
pp. 97 ◽  
Author(s):  
Habibah Mohamed ◽  
Ninik Irawati ◽  
Fauzan Ahmad ◽  
Mohd Haniff Ibrahim ◽  
Sumiaty Ambran ◽  
...  
Keyword(s):  
Carbon Nanotubes ◽  
Humidity Sensor ◽  
Fused Deposition Modeling ◽  
Acrylonitrile Butadiene Styrene ◽  
Performance Comparison ◽  
Tapered Fiber ◽  
Fused Deposition ◽  
Multi Walled Carbon Nanotubes ◽  
Deposition Modeling ◽  
Walled Carbon Nanotubes

<p>We demonstrated performance comparison of optical humidity sensor for bare and Multi-walled carbon nanotubes (MWCNTs) slurry coated tapered optical fiber. The starting material for MWCNTs slurry is MWCNTs- acrylonitrile butadiene styrene (ABS) based fused deposition modeling (FDM) 3D printer filament. The ABS was dissolved using acetone to produce MWCNTs-acetone suspension. The MWCNTs-acetone suspension was drop-casted on the tapered fiber to produce MWCNTs slurry by evaporation process at room temperature, which resulted the MWCNTs slurry attach to the tapered fiber. The MWCNTs slurry acts as the cladding for humidity changes measurement. The experimental works showed improvement of sensitivity from 3.811 μW/% of bare tapered fiber to 5.17 μW/% for the coated tapered fiber with MWCNTs slurry when the humidity varied from 45% to 80%.</p>

Effects of Multi-Walled Carbon Nanotubes on the Properties of Acrylonitrile Butadiene Styrene Nanocomposites Potentially Used for Fused Deposition Modeling

2017 ◽  
Vol 898 ◽  
pp. 2384-2391
Author(s):  
Jin Zhu ◽  
Biao Wang
Keyword(s):  
Carbon Nanotubes ◽  
Fused Deposition Modeling ◽  
Loss Modulus ◽  
Linear Thermal Expansion ◽  
Acrylonitrile Butadiene Styrene ◽  
Low Frequencies ◽  
Fused Deposition ◽  
Multi Walled Carbon Nanotubes ◽  
Walled Carbon Nanotubes ◽  
Butadiene Styrene

Multi-walled carbon nanotubes (MWCNTs)/acrylonitrile butadiene styrene (ABS) nanocomposites were prepared by melt blending and then filaments were obtained by melt extrusion method. The Scanning electron microscope (SEM) exhibited good dispersion of MWCNTs in the SAN phase of the ABS matrix. The rheological results showed that incorporation of MWCNTs into ABS resulted in higher storage modulus (G′) and loss modulus (G′′) than those of ABS, especially at low frequencies. The tensile strength and modulus of MWCNT/ABS nanocomposite filaments substantially increased with the MWCNTs content while the elongation at break decreased. Additionally, the addition of MWCNTs decreased the coefficient of linear thermal expansion. This study provides a basis for further development of MWCNT/ABS nanocomposites used for FDM process with desirable mechanical properties and good dimension stability.

scholarly journals POM/EVA Blends with Future Utility in Fused Deposition Modeling

Materials ◽  
2020 ◽  
Vol 13 (13) ◽  
pp. 2912 ◽  
Author(s):  
Mateusz Galeja ◽  
Klaudiusz Wypiór ◽  
Jan Wachowicz ◽  
Przemysław Kędzierski ◽  
Aleksander Hejna ◽  
...  
Keyword(s):  
3D Printing ◽  
Fused Deposition Modeling ◽  
Headspace Analysis ◽  
Melt Flow Index ◽  
Ethylene Vinyl Acetate ◽  
Tensile Tests ◽  
Index Structure ◽  
Flow Index ◽  
Scanning Calorimetry ◽  
Fused Deposition

Polyoxymethylene (POM) is one of the most popular thermoplastic polymers used in the industry. Therefore, the interest in its potential applications in rapid prototyping is understandable. Nevertheless, its low dimensional stability causes the warping of 3D prints, limiting its applications. This research aimed to evaluate the effects of POM modification with ethylene-vinyl acetate (EVA) (2.5, 5.0, and 7.5 wt.%) on its processing (by melt flow index), structure (by X-ray microcomputed tomography), and properties (by static tensile tests, surface resistance, contact angle measurements, differential scanning calorimetry, and thermogravimetric analysis), as well as very rarely analyzed emissions of volatile organic compounds (VOCs) (by headspace analysis). Performed modifications decreased stiffness and strength of the material, simultaneously enhancing its ductility, which simultaneously increased the toughness even by more than 50% for 7.5 wt.% EVA loading. Such an effect was related to an improved linear flow rate resulting in a lack of defects inside the samples. The decrease of the melting temperature and the slight increase of thermal stability after the addition of EVA broadened the processing window for 3D printing. The 3D printing trials on two different printers showed that the addition of EVA copolymer increased the possibility of a successful print without defects, giving space for further development.

scholarly journals A Study on Melt Flow Index on Copper-ABS for Fused Deposition Modeling (FDM) Feedstock

2015 ◽  
Vol 773-774 ◽  
pp. 8-12 ◽  
Author(s):  
Noor Mu'izzah Ahmad Isa ◽  
Nasuha Sa'ude ◽  
M. Ibrahim ◽  
Saiful Manar Hamid ◽  
Khairu Kamarudin
Keyword(s):  
Injection Molding ◽  
Fused Deposition Modeling ◽  
Acrylonitrile Butadiene Styrene ◽  
Melt Flow Index ◽  
Internal Force ◽  
Flow Index ◽  
Fused Deposition Modelling ◽  
Melt Flow ◽  
Volume Percentage ◽  
Fused Deposition

This paper presents of Polymer Matrix Composite (PMC) as feedstock used in Fused Deposition Modelling (FDM) machine. This study discussed on the development of a new PMC material by the injection molding machine. The material consist of copper powder filled in an acrylonitrile butadiene styrene (ABS), binder and surfactant material. The effect of metal filled in ABS and binder content was investigated experimentally by the Melt Flow Index (MFI) machine. Based on the result obtained, an increment of copper filled in ABS by volume percentage (vol. %) effected on melt flow index results. With highly filled copper in PMC composites increase the melt flow index results. It was concluded that, the propensity of the melt flow allow an internal force in PMC material through the injection molding and FDM machine.

scholarly journals Rapid Prototyping of Efficient Electromagnetic Interference Shielding Polymer Composites via Fused Deposition Modeling

2018 ◽  
Vol 9 (1) ◽  
pp. 37 ◽  
Author(s):  
Luiz Ecco ◽  
Sithiprumnea Dul ◽  
Débora Schmitz ◽  
Guilherme Barra ◽  
Bluma Soares ◽  
...  
Keyword(s):  
Carbon Nanotubes ◽  
Electrical Conductivity ◽  
Electromagnetic Interference ◽  
Fused Deposition Modeling ◽  
Processing Parameters ◽  
Emi Shielding ◽  
Fused Deposition ◽  
Multi Walled Carbon Nanotubes ◽  
Deposition Modeling ◽  
Walled Carbon Nanotubes

Acrylonitrile–butadiene–styrene (ABS) filled with 6 wt.% of multi-walled carbon nanotubes and graphene nanoplatelets was extruded in filaments and additively manufactured via fused deposition modeling (FDM). The electrical conductivity and electromagnetic interference shielding efficiency (EMI SE) in the frequency range between 8.2 and 12.4 GHz of the resulting 3D samples were assessed. For comparison purposes, compression molded samples of the same composition were investigated. Electrical conductivity of about 10−4 S·cm−1 and attenuations of the incident EM wave near 99.9% were achieved for the 3D components loaded with multi-walled carbon nanotubes, almost similar to the correspondent compression molded samples. Transmission electron microscopy (TEM) images of ABS composite filaments show that graphene nanoplatelets were oriented along the polymer flow whereas multi-walled carbon nanotubes were randomly distributed after the extrusion process. The electrical conductivity and electromagnetic interference (EMI) shielding properties of compression molded and FDM manufactured samples were compared and discussed in terms of type of fillers and processing parameters adopted in the FDM process, such as building directions and printing patterns. In view of the experimental findings, the role of the FDM processing parameters were found to play a major role in the development of components with enhanced EMI shielding efficiency.

scholarly journals Melt Flow Index of Recycle ABS for Fused Deposition Modeling (FDM) Filament

2015 ◽  
Vol 773-774 ◽  
pp. 3-7 ◽  
Author(s):  
Nasuha Sa'ude ◽  
Khairu Kamarudin ◽  
Mustaffa Ibrahim ◽  
Mohd Halim Irwan Ibrahim
Keyword(s):  
Material Properties ◽  
Fused Deposition Modeling ◽  
Acrylonitrile Butadiene Styrene ◽  
Melt Flow Index ◽  
Flow Index ◽  
Melt Flow ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
Higher Temperature ◽  
Butadiene Styrene

This paper presents the melt flow index (MFI) of acrylonitrile butadiene styrene (ABS) and recycle ABS filament wire for Fused Deposition Modeling (FDM) machine. In this study, the effect of MFI on recycle ABS material was investigated experimentally based on the melting temperature, density, screw speed and material properties. The MFI result on ABS recycle in wire filament was investigated using Melt Indexer Machine (MIM). Based on the result obtained, it was found that, ABS recycle was increase the density and MFI results. It can be observed that, the higher temperature was melt the recycle ABS material through the MIM and extruder machine.

scholarly journals A Study Of Welding Of Heterogenous Polycarbonate Substances Utilizing Hybrid Filaments Of Fused Deposition Modeling

2021 ◽  
Vol 23 (12) ◽  
pp. 146-157
Author(s):  
Afroza Bano ◽  
◽  
Manish Kumar Gupta ◽  
Keyword(s):  
Fused Deposition Modeling ◽  
Acrylonitrile Butadiene Styrene ◽  
Cost Effective ◽  
Melt Flow Index ◽  
Polyamide 6 ◽  
Flow Index ◽  
Fused Deposition Modelling ◽  
Friction Stir ◽  
Fused Deposition ◽  
Minimal Work

Friction-based welding is one of the most cost-effective and dependable methods for joining thermoplastics. However, there has been minimal work that has demonstrated the procedure/methods/equipment for welding two distinct types of thermoplastics. There is, nevertheless, a significant possibility of connecting the various thermoplastic materials by matching their melt flow index (MFI). One way for modifying the MFI is to reinforce it with micro/nano sized fillers. Fused deposition modelling (FDM) is a fast prototyping technology that employs thermoplastic-based filament to print components. The current study focuses on connecting aluminium (Al) metal powder reinforced acrylonitrile butadiene styrene (ABS) and polyamide 6 (PA6) thermoplastic substrates (3D printed by FDM) utilising friction welding (FW) / friction stir welding (FSW) / friction stir spot welding (FSSW). It was observed that the PA6 with 50% Al fillers (PA6-50% Al) and ABS matrix with 15% Al fillers (ABS-15% Al) produced MFIs of 11.97g/10min and 11.57g/10min, respectively.

scholarly journals Carbon Nanotube-Based Composite Filaments for 3D Printing of Structural and Conductive Elements

2021 ◽  
Vol 11 (3) ◽  
pp. 1272
Author(s):  
Bartłomiej Podsiadły ◽  
Piotr Matuszewski ◽  
Andrzej Skalski ◽  
Marcin Słoma
Keyword(s):  
Carbon Nanotubes ◽  
Fused Deposition Modeling ◽  
Supply Voltage ◽  
Acrylonitrile Butadiene Styrene ◽  
Structural Elements ◽  
Filling Fraction ◽  
Fused Deposition ◽  
Structural Electronics ◽  
Measured Sample ◽  
Deposition Modeling

In this publication, we describe the process of fabrication and the analysis of the properties of nanocomposite filaments based on carbon nanotubes and acrylonitrile butadiene styrene (ABS) polymer for fused deposition modeling (FDM) additive manufacturing. Polymer granulate was mixed and extruded with a filling fraction of 0.99, 1.96, 4.76, 9.09 wt.% of CNTs (carbon nanotubes) to fabricate composite filaments with a diameter of 1.75 mm. Detailed mechanical and electrical investigations of printed test samples were performed. The results demonstrate that CNT content has a significant influence on mechanical properties and electrical conductivity of printed samples. Printed samples obtained from high CNT content composites exhibited an improvement in the tensile strength by 12.6%. Measurements of nanocomposites’ electrical properties exhibited non-linear relation between the supply voltage and measured sample resistivity. This effect can be attributed to the semiconductor nature of the CNT functional phase and the occurrence of a tunnelling effect in percolation network. Detailed I–V characteristics related to the amount of CNTs in the composite and the supply voltage influence are also presented. At a constant voltage value, the average resistivity of the printed elements is 2.5 Ωm for 4.76 wt.% CNT and 0.15 Ωm for 9.09 wt.% CNT, respectively. These results demonstrate that ABS/CNT composites are a promising functional material for FDM additive fabrication of structural elements, but also structural electronics and sensors.

scholarly journals Polymeric Composites Based on Polyurea Matrix Reinforced with Carbon Nanotubes

2017 ◽  
Vol 54 (1) ◽  
pp. 41-44 ◽  
Author(s):  
Maria Adina Vulcan ◽  
Celina Damian ◽  
Paul Octavian Stanescu ◽  
Eugeniu Vasile ◽  
Razvan Petre ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Carbon Nanotubes ◽  
Thermal Stability ◽  
Scanning Electron Microscopy ◽  
Tensile Tests ◽  
Mechanical Analysis ◽  
Multi Walled Carbon Nanotubes ◽  
Walled Carbon Nanotubes ◽  
Scanning Electron

This paper deals with the synthesis of polyurea and its use as polymer matrix for nanocomposites reinforced with multi-walled carbon nanotubes (MWCNT). Two types of materials were obtained during this research, the first cathegory uses the polyurea as matrix and the second one uses a mixture between epoxy resin and polyurea. The nanocomposites were characterized by Thermogravimetric Analysis (TGA), Dynamic Mechanical Analysis (DMA), Scanning Electron Microscopy (SEM) and Tensile Tests .The elastomeric features of nanocomposites were highlighted by the results which showed low value of Tg. Also higher thermal stability with ~40oC compared with commercial products (M20) were observed, but lower mechanical properties compared to neat polyurea.

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