scholarly journals Preparation of 1060, 2024 and 7075 Aluminum Alloy Anodic Oxide Films

Coatings ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1498
Author(s):  
Chaojie Jing ◽  
Ruijue Wang ◽  
Fangchao Zhao ◽  
Lunwu Zhang ◽  
Qiongyao He ◽  
...  
Keyword(s):  
Aluminum Alloys ◽  
Anodic Oxidation ◽  
Constant Pressure ◽  
Oxide Films ◽  
Anodic Oxide ◽  
Phosphoric Acid Solution ◽  
X Ray Diffraction ◽  
X Ray ◽  
Mixed Stage ◽  
Highly Uniform

On aluminum alloys of grades 1060, 2024 and 7075, regular and highly uniform oxide films were formed by anodic oxidation. Anodizing was carried out at a constant pressure in a phosphoric acid solution of various concentrations. Using scanning electron microscopy (SEM) and X-ray diffraction (XRD), the optimal characteristics of the method of anodic oxidation for forming uniform oxide films on aluminum alloys were determined: anodic oxidation time, temperature, voltage and the concentration of H3PO4. It was found that, in the process of anodizing, the films have gone through four stages: a non-porosity stage, a mixed stage, an ordered porosity stage and a disordered porosity stage.

Effect of Amino Acids on the Structure and Corrosion Resistance of Mg-Li Alloy Anodic Oxide Film

2010 ◽  
Vol 146-147 ◽  
pp. 785-788 ◽  
Author(s):  
Li Min Chang ◽  
Peng Wang ◽  
Wei Liu
Keyword(s):  
Corrosion Resistance ◽  
Amino Acid ◽  
Electrochemical Impedance ◽  
Oxide Films ◽  
Anodic Oxide ◽  
Carbon Chain ◽  
Anodic Oxide Film ◽  
X Ray Diffraction ◽  
X Ray ◽  
Anodic Oxide Films

In this paper, Mg-Li alloy anodic oxide films were prepared with different amino acid as additive. The microstructure and phase composition of the coatings were studied by scanning electron microscopy (SEM) and X-ray diffraction (XRD), respectively. The corrosion resistance was evaluated by potentiodynamic polarization techniques and electrochemical impedance spectroscopy (EIS). The results show that the main compositions of the anodic oxide films are MgO, Mg(OH)2 and LiOH. The anodic oxide films with amino acid as additive have uniformer surface and higher corrosion resistance than that without additive, but with the increase of the carbon chain of amino acid, the effect is reduced gradually.

Magnetic Properties of Sputtered Fe-O and Co-O Thin Films

1995 ◽  
Vol 403 ◽  
Author(s):  
D. V. Dimitrov ◽  
A. S. Murthy ◽  
G. C. Hadjipanayis ◽  
C. P. SWANN
Keyword(s):  
Grain Size ◽  
Low Temperatures ◽  
Room Temperature ◽  
Oxide Films ◽  
X Ray Diffraction ◽  
Dc Magnetron Sputtering ◽  
Large Shift ◽  
X Ray ◽  
Grain Size And Shape ◽  
Spherical Grains

AbstractFe-O and Co-O films were prepared by DC magnetron sputtering in a mixture of Ar and O2 gases. By varying the oxygen to argon ratio, oxide films with stoichiometry FeO, Fe3O4, α-Fe2O3, CoO and Co3O4 were produced. TEM studies showed that the Fe – oxide films were polycrystalline consisting of small almost spherical grains, about 10 nm in size. Co-O films had different microstructure with grain size and shape dependent on the amount of oxygen. X-ray diffraction studies showed that the grains in Fe-O films were randomly oriented in contrast to Co-O films in which a <111> texture was observed. Pure FeO and α-Fe2O3 films were found to be superparamagnetic at room temperature but strongly ferromagnetic at low temperatures in contrast to the antiferromagnetic nature of bulk samples. A very large shift in the hysteresis loop, about 3800 Oe, was observed in field cooled Co-CoO films indicating the presence of a large unidirectional exchange anisotropy.

Behavior of glycerol concentration in a HCl electrolyte for obtaining Titania nanostructures by anodic oxidation

MRS Advances ◽  
2019 ◽  
Vol 4 (53) ◽  
pp. 2873-2880
Author(s):  
E. Martínez Cantú ◽  
D. J. Araujo-Pérez ◽  
L. García-González ◽  
A. Báez Rodríguez ◽  
J. Hernández-Torres ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Anodic Oxidation ◽  
Anatase Phase ◽  
Glycerol Concentration ◽  
X Ray Diffraction ◽  
X Ray ◽  
Anodization Time ◽  
Voltage Variation ◽  
Titania Nanostructures

ABSTRACTIn this work, the anodization of grade 2 titanium was performed using a HCl-based electrolyte in order to obtain Titania nanostructures. Different glycerol concentrations were added to the HCl electrolyte to study the effect it has on the shape and density of the nanostructures, additionally, anodization time and voltage was also varied. The anodized samples were observed by SEM microscopy and studied by Raman spectroscopy and X-ray diffraction. Raman spectroscopy and XRD showed the formation of the anatase phase of the TiO2. By SEM it was possible to observe several changes in the shape of the structures, by adding glycerol ball-like structures were visible, anodization time did not change the shape of the nanostructures. However, the voltage variation showed a clear control on the shape of the structures, forming nanotubes at higher voltages. It was concluded that a better control of the shape and density of the nanostructures is achieved by adding glycerol, however, in order to overcome the resistance that the electrolyte brings, higher voltages are required.

Accelerated Thermal Decomposition of Graphene Oxide Films in Air via in Situ X-ray Diffraction Analysis

2016 ◽  
Vol 120 (27) ◽  
pp. 14984-14990 ◽  
Author(s):  
Qin Pan ◽  
Ching-Chang Chung ◽  
Nanfei He ◽  
Jacob L. Jones ◽  
Wei Gao
Keyword(s):  
Thermal Decomposition ◽  
Graphene Oxide ◽  
Diffraction Analysis ◽  
Oxide Films ◽  
X Ray Diffraction ◽  
X Ray

X-ray Diffraction of Thin Oxide Films on Soldered Module Pins

1988 ◽  
Vol 32 ◽  
pp. 303-310
Author(s):  
T. Paul Adi ◽  
H. F. Stehmeyer
Keyword(s):  
Oxide Films ◽  
Interplanar Distance ◽  
X Ray Diffraction ◽  
Metal Oxide Films ◽  
X Ray ◽  
Highly Sensitive ◽  
Thin Oxide Films ◽  
Thin Oxide ◽  
Diffraction Patterns

AbstractThe presence of metal oxide films from wave solder baths on timed module pins are partly responsible for non-wet problems in subsequent soldering steps. The cylindrical geometry of the pins lends itself to the characterization of thin oxide films by using the highly sensitive Debye-Scherrer camera method. As confirmed by Electron Hicroprobe Analysis (EMA), pins containing thin oxide films were used to obtain the diffraction patterns. A software program was developed that subtracts the diffraction angles of an oxids-free control pin from the pattern of the contaminated pin, and tabulates the residual d-spacing (interplanar distance) of the contaminant film.

Anti-Wear Coating Grown by Micro-Plasma Oxidation on Aluminum Alloys in the Solution of Aluminate-Titania

2011 ◽  
Vol 239-242 ◽  
pp. 667-670 ◽  
Author(s):  
Li Gong Zhang ◽  
Gui Mei Zhao ◽  
Xiao Ming Lai
Keyword(s):  
Aluminum Alloys ◽  
Ceramic Coating ◽  
Ceramic Coatings ◽  
Wear Property ◽  
Plasma Oxidation ◽  
X Ray Diffraction ◽  
Electrolytic Solution ◽  
X Ray ◽  
Hardness Tester ◽  
Wear Coating

In this paper, Aluminum trioxide ceramic coatings were grown on surfaces of 2024 Aluminum alloys by micro-plasma oxidation in an aluminate electrolytic solution. In order to decrease the density of the pores and increase the anti-wear property of the ceramic coatings, Titania were added into the aluminate electrolytic solution. The struture and anti-wear property of the produced ceramic coatings were measured by X-ray diffraction, scanning electron microscope , hardness tester and frictionometer. The results show that the thickness of the ceramic coating is about 24±1 μm, surfaces of the ceramic coatings are very uniform. The hardness of the doped coating is up to 930 HV, and the wear property of the coating is the more excellent than that of undoped coating.

Formation of Aluminum Nitride Films by Gas Nitriding

2014 ◽  
Vol 625 ◽  
pp. 651-656 ◽  
Author(s):  
Masashi Yoshida ◽  
Zhou Tao ◽  
Noah Utsumi
Keyword(s):  
Aluminum Alloys ◽  
Aluminum Nitride ◽  
Electron Probe ◽  
Treatment Time ◽  
Film Surface ◽  
Nitride Film ◽  
X Ray Diffraction ◽  
Good Adhesion ◽  
X Ray ◽  
Gas Nitriding

In this study, aluminum alloys were subjected to nitriding at 823 K for 0–18.0 ks using alumina and magnesium powders for improving their radiation performance. After nitriding, aluminum nitride films were formed on the aluminum substrate. The thickness of the formed films varied from 1.5 to 11 μm, and the color of the film surface was dark brown or black. The thickness of the aluminum nitride film increased with an increase in the treatment time. X-ray diffraction and electron probe microanalysis results showed that the film was composed of aluminum nitride, alumina, aluminum, and magnesium. Further, the film showed good adhesion at 0 ks.

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