scholarly journals Effects of Silicon Content on the Microstructures and Mechanical Properties of (AlCrTiZrV)-Six-N High-Entropy Alloy Films

Entropy ◽  
2019 ◽  
Vol 21 (1) ◽  
pp. 75 ◽  
Author(s):  
Jingrui Niu ◽  
Wei Li ◽  
Ping Liu ◽  
Ke Zhang ◽  
Fengcang Ma ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Amorphous Phase ◽  
Silicon Content ◽  
High Entropy Alloy ◽  
Strengthening Effect ◽  
Nanocomposite Structure ◽  
High Entropy ◽  
Nanocrystalline Structures ◽  
Microstructures And Mechanical Properties

A series of (AlCrTiZrV)-Six-N films with different silicon contents were deposited on monocrystalline silicon substrates by direct-current (DC) magnetron sputtering. The films were characterized by the X-ray diffractometry (XRD), scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), and nano-indentation techniques. The effects of the silicon content on the microstructures and mechanical properties of the films were investigated. The experimental results show that the (AlCrTiZrV)N films grow in columnar grains and present a (200) preferential growth orientation. The addition of the silicon element leads to the disappearance of the (200) peak, and the grain refinement of the (AlCrTiZrV)-Six-N films. Meanwhile, the reticular amorphous phase is formed, thus developing the nanocomposite structure with the nanocrystalline structures encapsulated by the amorphous phase. With the increase of the silicon content, the mechanical properties first increase and then decrease. The maximal hardness and modulus of the film reach 34.3 GPa and 301.5 GPa, respectively, with the silicon content (x) of 8% (volume percent). The strengthening effect of the (AlCrTiZrV)-Six-N film can be mainly attributed to the formation of the nanocomposite structure.

scholarly journals Effects of Nb Addition on Microstructures and Mechanical Properties of Nbx-CoCrFeMnNi High Entropy Alloy Films

Coatings ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1539
Author(s):  
Yu-Hsuan Liang ◽  
Chia-Lin Li ◽  
Chun-Hway Hsueh
Keyword(s):  
Mechanical Properties ◽  
Amorphous Phase ◽  
Compressive Yield Strength ◽  
High Entropy Alloy ◽  
Face Centered Cubic ◽  
Compression Tests ◽  
Alloy Films ◽  
High Entropy ◽  
Microstructures And Mechanical Properties ◽  
Nb Addition

In the present work, Nbx-CoCrFeMnNi high entropy alloy films (HEAFs, 0 to 7.2 at.% Nb) were fabricated by radio frequency (RF) magnetron co-sputtering of CoCrFeMnNi alloy and Nb targets. The effects of Nb addition on the microstructures and mechanical properties of HEAFs were systematically investigated. For Nb-free film (0 at.% Nb), the face-centered cubic (FCC) peaks were identified in the X-ray diffraction (XRD) pattern. The addition of Nb resulted in a broadening of diffraction peaks, a decrease in peak intensity, and the vanishment of high-angle peaks. Transmission electron microscope (TEM) images indicated the formation of nanotwins at low Nb concentrations, and a transition from a single phase FCC solid solution to an amorphous phase was observed with the increasing Nb concentration. The films were strengthened with an increase in Nb concentration. Specifically, the hardness characterized by nanoindentation increased from 6.5 to 8.1 GPa. The compressive yield strength and fracture strength measured from micropillar compression tests were improved from 1.08 GPs and 2.56 GPa to 2.70 GPa and 5.76 GPa, respectively, whereas the fracture strain decreased from >29.4% (no fracture) to 15.8%. Additionally, shear banding was observed in the presence of amorphous phase.

scholarly journals Variations of the Elastic Properties of the CoCrFeMnNi High Entropy Alloy Deformed by Groove Cold Rolling

Materials ◽  
2018 ◽  
Vol 11 (8) ◽  
pp. 1337 ◽  
Author(s):  
Paul Lohmuller ◽  
Laurent Peltier ◽  
Alain Hazotte ◽  
Julien Zollinger ◽  
Pascal Laheurte ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Cold Rolling ◽  
Young’S Modulus ◽  
Crystallographic Texture ◽  
Young's Modulus ◽  
Rolling Process ◽  
High Entropy Alloy ◽  
Strengthening Effect ◽  
High Entropy ◽  
Conventional Rolling

The variations of the mechanical properties of the CoCrFeMnNi high entropy alloy (HEA) during groove cold rolling process were investigated with the aim of understanding their correlation relationships with the crystallographic texture. Our study revealed divergences in the variations of the microhardness and yield strength measured from samples deformed by groove cold rolling and conventional cold rolling processes. The crystallographic texture analyzed by electron back scattered diffraction (EBSD) revealed a hybrid texture between those obtained by conventional rolling and drawing processes. Though the groove cold rolling process induced a marked strengthening effect in the CoCrFeMnNi HEA, the mechanical properties were also characterized by an unusual decrease of the Young’s modulus as the applied groove cold rolled deformation increased up to about 0.5 before reaching a stabilized value. This decrease of the Young’s modulus was attributed to the increased density of mobile dislocations induced by work hardening during groove cold rolling processing.

Microstructure and mechanical properties of AlCrFeCoNi high-entropy alloy particle reinforced Mg-9Al-1Zn matrix composites

2021 ◽  
Vol 112 (7) ◽  
pp. 538-545
Author(s):  
Yongsheng Chen ◽  
Zesheng Ji ◽  
Maoliang Hu ◽  
Hongyu Xu ◽  
Guangjie Feng
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Volume Fraction ◽  
Dominant Role ◽  
Particle Volume Fraction ◽  
Stress Transfer ◽  
High Entropy Alloy ◽  
Compression Tests ◽  
Particle Volume ◽  
High Entropy

Abstract AlCrFeCoNi particles were added to Mg-9Al-1Zn alloy in a rotary blowing process. The microstructures and mechanical properties of Mg-9Al-1Zn based composites were characterized by means of X-ray diffraction, optical microscopy, scanning electron microscopy, transmission electron microscopy, and tensile and compression tests at room temperature. Results revealed that AlCrFeCoNi particles could effectively refine the grains, and the rotary blowing process enabled the uniform distribution of these particles. The mechanical properties of composites improved with the increase of particle volume fraction. The superior wettability of AlCrFeCoNi particles supported their reliable bonding with the Mg-9Al-1Zn matrix. The Hall–Petch strengthening and stress transfer effect played a dominant role in the improvement of compressive and tensile properties.

scholarly journals Evolution of Microstructure and Mechanical Properties of LM25–HEA Composite Processed through Stir Casting with a Bottom Pouring System

Materials ◽  
2021 ◽  
Vol 15 (1) ◽  
pp. 230
Author(s):  
Mekala Chinababu ◽  
Nandivelegu Naga Krishna ◽  
Katakam Sivaprasad ◽  
Konda Gokuldoss Prashanth ◽  
Eluri Bhaskara Rao
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Tensile Strength ◽  
Aluminum Matrix ◽  
Stir Casting ◽  
Significant Loss ◽  
Aluminum Matrix Composites ◽  
High Entropy Alloy ◽  
High Entropy ◽  
The Matrix

Aluminum matrix composites reinforced by CoCrFeMnNi high entropy alloy (HEA) particulates were fabricated using the stir casting process. The as-cast specimens were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and transmission electron microscopy (TEM). The results indicated that flake-like silicon particles and HEA particles were distributed uniformly in the aluminum matrix. TEM micrographs revealed the presence of both the matrix and reinforcement phases, and no intermetallic phases were formed at the interface of the matrix and reinforcement phases. The mechanical properties of hardness and tensile strength increased with an increase in the HEA content. The Al 6063–5 wt.% HEA composite had a ultimate tensile strength (UTS) of approximately 197 MPa with a reasonable ductility (around 4.05%). The LM25–5 wt.% HEA composite had a UTS of approximately 195 Mpa. However, the percent elongation decreased to roughly 3.80%. When the reinforcement content increased to 10 wt.% in the LM25 composite, the UTS reached 210 MPpa, and the elongation was confined to roughly 3.40%. The fracture morphology changed from dimple structures to cleavage planes on the fracture surface with HEA weight percentage enhancement. The LM25 alloy reinforced with HEA particles showed enhanced mechanical strength without a significant loss of ductility; this composite may find application in marine and ship building industries.

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