scholarly journals Mapping the Tray of Electron Beam Melting of Ti-6Al-4V: Properties and Microstructure

Materials ◽  
2019 ◽  
Vol 12 (9) ◽  
pp. 1470 ◽  
Author(s):  
E. Tiferet ◽  
M. Ganor ◽  
D. Zolotaryov ◽  
A. Garkun ◽  
A. Hadjadj ◽  
...  

Using an electron beam melting (EBM) printing machine (Arcam A2X, Sweden), a matrix of 225 samples (15 rows and 15 columns) of Ti-6Al-4V was produced. The density of the specimens across the tray in the as-built condition was approximately 99.9% of the theoretical density of the alloy, ρT. Tensile strength, tensile elongation, and fatigue life were studied for the as-built samples. Location dependency of the mechanical properties along the build area was observed. Hot isostatic pressing (HIP) slightly increased the density to 99.99% of ρT but drastically improved the fatigue endurance and tensile elongation, probably due to the reduction in the size and the distribution of flaws. The microstructure of the as-built samples contained various defects (e.g., lack of fusion, porosity) that were not observed in the HIP-ed samples. HIP also reduced some of the location related variation in the mechanical properties values, observed in the as-printed condition.

Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3603
Author(s):  
Tim Pasang ◽  
Benny Tavlovich ◽  
Omry Yannay ◽  
Ben Jakson ◽  
Mike Fry ◽  
...  

An investigation of mechanical properties of Ti6Al4V produced by additive manufacturing (AM) in the as-printed condition have been conducted and compared with wrought alloys. The AM samples were built by Selective Laser Melting (SLM) and Electron Beam Melting (EBM) in 0°, 45° and 90°—relative to horizontal direction. Similarly, the wrought samples were also cut and tested in the same directions relative to the plate rolling direction. The microstructures of the samples were significantly different on all samples. α′ martensite was observed on the SLM, acicular α on EBM and combination of both on the wrought alloy. EBM samples had higher surface roughness (Ra) compared with both SLM and wrought alloy. SLM samples were comparatively harder than wrought alloy and EBM. Tensile strength of the wrought alloy was higher in all directions except for 45°, where SLM samples showed higher strength than both EBM and wrought alloy on that direction. The ductility of the wrought alloy was consistently higher than both SLM and EBM indicated by clear necking feature on the wrought alloy samples. Dimples were observed on all fracture surfaces.


Metals ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 593
Author(s):  
Changyong Liu ◽  
Zhuokeng Mai ◽  
Deng Yan ◽  
Mingguang Jiang ◽  
Yuhong Dai ◽  
...  

This study investigated the effects of hot isostatic pressing (HIP) on the microstructures and mechanical properties of Ti6Al4V fabricated by electron beam melting (EBM). The differences of surface morphologies, internal defects, relative density, microstructures, textures, mechanical properties and tensile fracture between the as-built and HIPed samples were observed using various characterization methods including optical metallography microscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and electron backscattered diffraction (EBSD) and tensile tests. It was found that the main effects of HIP on microstructures include—the increase of average grain size from 7.96 ± 1.21 μm to 11.34 ± 1.89 μm, the increase of α lamellar thickness from 0.71 ± 0.15 μm to 2.49 ± 1.29 μm and the increase of β phase ratio from 4.7% to 10.5% in terms of area fraction on the transversal section. The combinatorial effects including densification, increase of grain size, α lamellar thickness, β phase ratio, reduction of dislocation density and transformation of dislocation patterns contributed to the improvement of elongation and ductility of EBM-fabricated Ti6Al4V. Meanwhile, these effects also resulted in a slight reduction of the yield strength and UTS mainly due to the coarsening effect of HIP.


2018 ◽  
Vol 941 ◽  
pp. 1597-1602
Author(s):  
Ken Cho ◽  
Ryota Kobayashi ◽  
Takuma Fukuoka ◽  
Jong Yeong Oh ◽  
Hiroyuki Y. Yasuda ◽  
...  

The effect of a unique layered microstructure consisting of duplex-like region and equiaxed γ grains (γ bands) on the fatigue properties of Ti-48Al-2Cr-2Nb alloy bars fabricated by electron beam melting (EBM) at an angle (θ) of 90° between the building direction and cylinder (loading) axis was investigated focusing on the layered microstructure and test temperature. We found the room temperature (RT) fatigue strength of the alloy bars fabricated at θ = 90° is higher than that of the bars fabricated at θ = 0°. Moreover, it is comparable to that of the cast alloys with hot isostatic pressing (HIP) treatment in low-cycle fatigue life region, even without HIP treatment. The high fatigue strength of the bars at RT is attributed to the γ band, which acts as a resistance for crack propagation directed perpendicular to the γ band. On the other hand, the fatigue strength of the bars at θ = 90° is lower than that of the bars at θ = 0° in low-cycle fatigue life region at 1023 K. This is because the γ bands dose not act as a resistance for crack propagation at 1023 K. Although the bars at θ = 90° exhibits low fatigue strength in the region at 1023 K, that value is comparable to that of HIP-treated cast alloys due to the fine grain size, which is one of the features for the alloys fabricated by the EBM.


2018 ◽  
pp. 86-90
Author(s):  
Алексей Александрович Педаш ◽  
Владимир Валериевич Клочихин ◽  
Тамара Александровна Митина ◽  
Валерий Григорьевич Шило

The composition, structure and mechanical properties of samples obtained from the titanium alloy Ti-6Al-4V, by selective laser melting and electron beam melting processes regarding production of responsible aviation parts were carrying-out at present article.A comparative study of macro- and microstructure, mechanical properties has been carried out after inherent of Ti-6Al-4V heat treatment with or without prior hot isostatic pressing.It was established that the advent in specimens fractures and microstructure pores and non-melt inclusions of a granules condition obligatory hot isostatic pressing of a responsible parts when this kinds of defects significantly releases and correspondingly best complex of mechanical properties are obtained.The powders from titanium Ti-6Al-4V alloy were produce by inert gas (argon) spraying process and had a different particle sizing distribution: 20-50 microns for selective laser melting and 45-105 microns for electron beam melting.The microstructure of the specimens prepared using the studied production processes features an elongated lamellar alpha phase in the transformated epitaxially grown beta-matrix and is typical for Ti-6Al-4V alloy in a heat-treated condition.It has been noted that the lamellar alpha phase in the structure of the studied specimens after hot isostatic pressing is distinguished by larger sizes in width as compared to the specimens prior to hot isostatic pressing processing.Mechanical properties of the specimens produced by selective laser melting or electron beam melting processes meet the specification requirements. Hot isostatic pressing processing results in a remarkable improvement of the impact strength.  Authors should be pointed out that application of additive technologies in the manufacture of aerospace parts requires extensive research&development works, and testing efforts to confirm repeatability of alloy characteristics. A mandatory procedure of the production process and material approval shall be conducted to ensure compliance with aircraft flight safety standards and regulations.


2021 ◽  
Vol 11 (12) ◽  
pp. 5317
Author(s):  
Rafał Malinowski ◽  
Aneta Raszkowska-Kaczor ◽  
Krzysztof Moraczewski ◽  
Wojciech Głuszewski ◽  
Volodymyr Krasinskyi ◽  
...  

The need for the development of new biodegradable materials and modification of the properties the current ones possess has essentially increased in recent years. The aim of this study was the comparison of changes occurring in poly(ε-caprolactone) (PCL) due to its modification by high-energy electron beam derived from a linear electron accelerator, as well as the addition of natural fibers in the form of cut hemp fibers. Changes to the fibers structure in the obtained composites and the geometrical surface structure of sample fractures with the use of scanning electron microscopy were investigated. Moreover, the mechanical properties were examined, including tensile strength, elongation at break, flexural modulus and impact strength of the modified PCL. It was found that PCL, modified with hemp fibers and/or electron radiation, exhibited enhanced flexural modulus but the elongation at break and impact strength decreased. Depending on the electron radiation dose and the hemp fibers content, tensile strength decreased or increased. It was also found that hemp fibers caused greater changes to the mechanical properties of PCL than electron radiation. The prepared composites exhibited uniform distribution of the dispersed phase in the polymer matrix and adequate adhesion at the interface between the two components.


Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 536 ◽  
Author(s):  
Sneha Goel ◽  
Kévin Bourreau ◽  
Jonas Olsson ◽  
Uta Klement ◽  
Shrikant Joshi

Electron beam melting (EBM) is gaining rapid popularity for production of complex customized parts. For strategic applications involving materials like superalloys (e.g., Alloy 718), post-treatments including hot isostatic pressing (HIPing) to eliminate defects, and solutionizing and aging to achieve the desired phase constitution are often practiced. The present study specifically explores the ability of the combination of the above post-treatments to render the as-built defect content in EBM Alloy 718 irrelevant. Results show that HIPing can reduce defect content from as high as 17% in as-built samples (intentionally generated employing increased processing speeds in this illustrative proof-of-concept study) to <0.3%, with the small amount of remnant defects being mainly associated with oxide inclusions. The subsequent solution and aging treatments are also found to yield virtually identical phase distribution and hardness values in samples with vastly varying as-built defect contents. This can have considerable implications in contributing to minimizing elaborate process optimization efforts as well as slightly enhancing production speeds to promote industrialization of EBM for applications that demand the above post-treatments.


Materials ◽  
2021 ◽  
Vol 14 (3) ◽  
pp. 658
Author(s):  
Yaron Itay Ganor ◽  
Eitan Tiferet ◽  
Sven C. Vogel ◽  
Donald W. Brown ◽  
Michael Chonin ◽  
...  

Additively-manufactured Ti-6Al-4V (Ti64) exhibits high strength but in some cases inferior elongation to those of conventionally manufactured materials. Post-processing of additively manufactured Ti64 components is investigated to modify the mechanical properties for specific applications while still utilizing the benefits of the additive manufacturing process. The mechanical properties and fatigue resistance of Ti64 samples made by electron beam melting were tested in the as-built state. Several heat treatments (up to 1000 °C) were performed to study their effect on the microstructure and mechanical properties. Phase content during heating was tested with high reliability by neutron diffraction at Los Alamos National Laboratory. Two different hot isostatic pressings (HIP) cycles were tested, one at low temperature (780 °C), the other is at the standard temperature (920 °C). The results show that lowering the HIP holding temperature retains the fine microstructure (~1% β phase) and the 0.2% proof stress of the as-built samples (1038 MPa), but gives rise to higher elongation (~14%) and better fatigue life. The material subjected to a higher HIP temperature had a coarser microstructure, more residual β phase (~2% difference), displayed slightly lower Vickers hardness (~15 HV10N), 0.2% proof stress (~60 MPa) and ultimate stresses (~40 MPa) than the material HIP’ed at 780 °C, but had superior elongation (~6%) and fatigue resistance. Heat treatment at 1000 °C entirely altered the microstructure (~7% β phase), yield elongation of 13.7% but decrease the 0.2% proof-stress to 927 MPa. The results of the HIP at 780 °C imply it would be beneficial to lower the standard ASTM HIP temperature for Ti6Al4V additively manufactured by electron beam melting.


Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 906
Author(s):  
Dong Han ◽  
Yongqing Zhao ◽  
Weidong Zeng

The present study focuses on the effect of 1% Zr addition on the microstructure, tensile properties and superplasticity of a forged SP700 alloy. The results demonstrated that Zr has a significant effect on inhibiting the microstructural segregation and increasing the volume fraction of β-phase in the forged SP700 alloy. After annealing at 820 °C for 1 h and aging at 500 °C for 6 h, the SP700 alloy with 1% Zr showed a completely globular and fine microstructure. The yield strength, ultimate tensile strength and tensile elongation of the alloy with optimized microstructure were 1185 MPa, 1296 MPa and 10%, respectively. The superplastic deformation was performed at 750 °C with an elongation of 1248%. The improvement of tensile properties and superplasticity of the forged SP700 alloy by Zr addition was mainly attributed to the uniform and fine globular microstructures.


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