scholarly journals Ceramization Mechanism of Ceramizable Silicone Rubber Composites with Nano Silica at Low Temperature

Materials ◽  
2020 ◽  
Vol 13 (17) ◽  
pp. 3708
Author(s):  
Penghu Li ◽  
Haiyun Jin ◽  
Shichao Wei ◽  
Huaidong Liu ◽  
Naikui Gao ◽  
...  
Keyword(s):  
Low Temperature ◽  
Flexural Strength ◽  
Silicone Rubber ◽  
Glass Frit ◽  
Nano Silica ◽  
Linear Contraction ◽  
Ceramic Phase ◽  
Ceramic Samples ◽  
Different Temperatures ◽  
Similar Materials

Ceramizable composite is a kind of polymer matrix composite that can turn into ceramic material at a high temperature. It can be used for the ceramic insulation of a metal conductor because of its processability. However, poor low-temperature ceramization performance is a problem of ceramizable composites. In this paper, ceramizable composites were prepared by using silicone rubber as a matrix. Ceramic samples were sintered at different temperatures no more than 1000 °C, according to thermogravimetric analysis results of the composites. The linear contraction and flexural strength of the ceramics were measured. The microstructure and crystalline phase of ceramics were analyzed using scanning electron microscope (SEM) and X-ray diffraction (XRD). The results show that the composites turned into ceramics at 800 °C, and a new crystal and continuous microstructure formed in the samples. The flexural strength of ceramics was 46.76 MPa, which was more than twice that of similar materials reported in other research sintered at 1000 °C. The maximum flexural strength was 54.56 MPa, when the sintering temperature was no more than 1000 °C. Moreover, glass frit and nano silica played important roles in the formation of the ceramic phase in this research. A proper content of nano silica could increase the strength of the ceramic samples.

Development of High Permeability Core Materials for Embeddable Inductors in Flexible Organic Substrates

2003 ◽  
Vol 769 ◽  
Author(s):  
C. K. Liu ◽  
P. L. Cheng ◽  
S. Y. Y. Leung ◽  
T. W. Law ◽  
D. C. C. Lam
Keyword(s):  
Low Temperature ◽  
Sol Gel ◽  
Circuit Board ◽  
Organic Substrates ◽  
Circuit Boards ◽  
High Permeability ◽  
Electrical Measurements ◽  
Different Temperatures ◽  
Spiral Inductors ◽  
Ceramic Tape

AbstractCapacitors, resistors and inductors are surface mounted components on circuit boards, which occupy up to 70% of the circuit board area. For selected applications, these passives are packaged inside green ceramic tape substrates and sintered at temperatures over 700°C in a co-fired process. These high temperature processes are incompatible with organic substrates, and low temperature processes are needed if passives are to be embedded into organic substrates. A new high permeability dual-phase Nickel Zinc Ferrite (DP NZF) core fabricated using a low temperature sol-gel route was developed for use in embedded inductors in organic substrates. Crystalline NZF powder was added to the sol-gel precursor of NZF. The solution was deposited onto the substrates as thin films and heat-treated at different temperatures. The changes in the microstructures were characterized using XRD and SEM. Results showed that addition of NZF powder induced low temperature transformation of the sol-gel NZF phase to high permeability phase at 250°C, which is approximately 350°C lower than transformation temperature for pure NZF sol gel films. Electrical measurements of DP NZF cored two-layered spiral inductors indicated that the inductance increased by three times compared to inductors without the DP NZF cores. From microstructural observations, the increase is correlated with the changes in microstructural connectivity of the powder phase.

scholarly journals GERMINATION AND VIGOUR IN SEEDS OF THE COWPEA IN RESPONSE TO SALT AND HEAT STRESS

2019 ◽  
Vol 32 (1) ◽  
pp. 143-151 ◽  
Author(s):  
Luma Rayane de Lima Nunes ◽  
Paloma Rayane Pinheiro ◽  
Charles Lobo Pinheiro ◽  
Kelly Andressa Peres Lima ◽  
Alek Sandro Dutra
Keyword(s):  
Salt Stress ◽  
Heat Stress ◽  
High Temperature ◽  
Low Temperature ◽  
Vigna Unguiculata ◽  
Salt Concentration ◽  
Dry Weight ◽  
Germination Percentage ◽  
Different Types ◽  
Different Temperatures

ABSTRACT Salinity is prejudicial to plant development, causing different types of damage to species, or even between genotypes of the same species, with the effects being aggravated when combined with other types of stress, such as heat stress. The aim of this study was to evaluate the tolerance of cowpea genotypes (Vigna unguiculata L. Walp.) to salt stress at different temperatures. Seeds of the Pujante, Epace 10 and Marataoã genotypes were placed on paper rolls (Germitest®) moistened with different salt concentrations of 0.0 (control), 1.5, 3.0, 4.5 and 6.0 dS m-1, and placed in a germination chamber (BOD) at temperatures of 20, 25, 30 and 35°C. The experiment was conducted in a completely randomised design, in a 3 × 4 × 5 scheme of subdivided plots, with four replications per treatment. The variables under analysis were germination percentage, first germination count, shoot and root length, and total seedling dry weight. At temperatures of 30 and 35°C, increases in the salt concentration were more damaging to germination in the Epace 10 and Pujante genotypes, while for the Marataoã genotype, damage occurred at the temperature of 20°C. At 25°C, germination and vigour in the genotypes were higher, with the Pujante genotype proving to be more tolerant to salt stress, whereas Epace 10 and Marataoã were more tolerant to high temperatures. Germination in the cowpea genotypes was more sensitive to salt stress when subjected to heat stress caused by the low temperature of 20°C or high temperature of 35°C.

A Method for Predicting the Behavior of Plastics at Different Temperatures

2014 ◽  
Vol 1039 ◽  
pp. 107-111
Author(s):  
Yang Chen ◽  
Gui Qin Li ◽  
Bin Ruan ◽  
Xiao Yuan ◽  
Hong Bo Li
Keyword(s):  
High Temperature ◽  
Low Temperature ◽  
Constitutive Model ◽  
Research And Development ◽  
Mechanical Behavior ◽  
Plastic Material ◽  
Different Temperatures ◽  
Plastic Parts

The mechanical behavior of plastic material is dramatically sensitive to temperature. An method is proposed to predict the mechanical behavior of plastics for cars, ranging from low-temperature low temperature ≤-40°C to high temperature ≥80°C. It dominates the behavior of plastic material based on improved constitutive model in which the parameters adjusted by a series of tests under different temperatures. The method is validated with test and establishes the basis for research and development of plastic parts for automobile as well.

Ag diffusion inhibition and enhanced flexural strength in low temperature co-fired CaO-Al2O3-B2O3-SiO2 glasses

2019 ◽  
Vol 782 ◽  
pp. 1094-1102 ◽  
Author(s):  
Kuei-Chih Feng ◽  
Pin-Yi Chen ◽  
Chi-Shun Tu ◽  
Cheng-Sao Chen ◽  
R.R. Chien ◽  
...  
Keyword(s):  
Low Temperature ◽  
Flexural Strength

Ageing in embryos from wheat grains stored at different temperatures: oxidative stress and antioxidant response

2011 ◽  
Vol 38 (7) ◽  
pp. 624 ◽  
Author(s):  
Carmelina Spanò ◽  
Stefania Bottega ◽  
Roberto Lorenzi ◽  
Isa Grilli
Keyword(s):  
Oxidative Stress ◽  
Low Temperature ◽  
Seed Viability ◽  
Storage Period ◽  
Antioxidant Response ◽  
Protective Role ◽  
Native Page ◽  
Wheat Grains ◽  
Different Temperatures ◽  
Enzymatic Machinery

In the present work we studied oxidative stress as an important cause of seed deterioration during ageing in embryos from durum wheat grains stored at room temperature and at low temperature (10°C). The protective role of low temperature on seed viability was confirmed. The increase of hydrogen peroxide content during dry storage was strongly correlated with the decrease of germinability. Ascorbate and glutathione showed a good correlation with grain germinability and significantly increased upon imbibition, in particular in embryos from viable grains. Ascorbate peroxidase (APX), dehydroascorbate reductase (DHAR), glutathione reductase (GR), glutathione peroxidase (GPX) and catalase (CAT) were studied quantitatively (enzymatic assays). APX, GR, and GPX were also studied qualitatively by native PAGE. The enzymes were active in dry, still viable, embryos whereas no activity was detected in non-viable embryos. With the exception of APX, all enzymatic activities decreased upon imbibition. The study of grains stored in different conditions indicated a negative correlation between the efficiency of the antioxidant enzymatic machinery and the age of the grain. The differences detected in differently stored materials confirmed that both germination parameters and the length of storage period are important in determining grain condition.

Short-period (Si14 / Si0.75 Ge0.25)20 Superlattices for the Growth of High-quality Si0.75 Ge0.25

2003 ◽  
Vol 765 ◽  
Author(s):  
M.M. Rahman ◽  
T. Tambo ◽  
C. Tatsuyama
Keyword(s):  
Low Temperature ◽  
Alloy Layer ◽  
Buffer Layers ◽  
Threading Dislocations ◽  
Strained Layers ◽  
Temperature Growth ◽  
Low Temperature Growth ◽  
Defect Sites ◽  
Short Period ◽  
Different Temperatures

AbstractIn the present experiment, we have grown 2500-Å thick Si0.75Ge0.25 alloy layers on Si(001) substrate by MBE process using a short-period (Si14/Si0.75Ge0.25)20 superlattice (SL) as buffer layers. In the SL layers, first a layer of 14 monolayers (MLs) of Si (thickness about 20Å) then a thin layer of Si0.75Ge0.25 (thickness 5-6Å) were grown. This Si/(Si0.75Ge0.25) bilayers were repeated for 20 times. The buffer layers were grown at different temperatures from 300-400°C and the alloy layers were then grown at 500°C on the buffer layers. The alloy layer showed low residual strain (about -0.16%) and smooth surface (rms roughness ~15Å) with 300°C grown SL buffer. Low temperature growth of Si in SL layer introduces point defects and low temperature growth of Si1-xGex in SL layer reduces the Ge segregation length, which leads to strained SL layer formation. Strained layers are capable to make barrier for the propagation of threading dislocations and point defect sites can trap the dislocations.

Self-Toughness Porous Sodium Titanate Bioceramics Prepared via In Situ Grown Na2Ti6O13 Rods

2017 ◽  
Vol 727 ◽  
pp. 806-814 ◽  
Author(s):  
Xiao Wei Ma ◽  
Jian Xing Shen ◽  
Ke Chang Zhang ◽  
Ling Kai Kong ◽  
Jia Le Sun ◽  
...  
Keyword(s):  
Fracture Toughness ◽  
Compressive Strength ◽  
Sodium Titanate ◽  
The Novel ◽  
Ceramic Samples ◽  
Porous Bioceramic ◽  
Different Temperatures ◽  
Growth Method ◽  
Titanate Ceramics

Here in, we report the porous bioceramic with Na2Ti6O13 rods prepared by in‒situ growth method. The samples were prepared using cold uniaxial pressing (40 MPa) technique and further sintered at different temperatures. The structure and morphology were characterized by XRD and SEM. The porosity, compressive strength and fracture toughness were also investigated. The bone-like apatite deposition ability of the fabricated ceramic samples was evaluated by Kokubo simulated body fluid (SBF) soaking method. The results indicated that the Na2Ti6O13 rods with about 1‒3 μm in diameter are uniformly distributed in the self‒toughness porous sodium titanate ceramics (SPSTC). The SPSTC with a porosity of 61.10±1.12 % exhibits good compressive strength (43.36±2.43 MPa) and fracture toughness (3.47±0.21 MPa·m1/2). The results indicate that the novel SPSTC scaffolds are promising for bone tissue engineering applications.

scholarly journals Effects of laminating and co-firing conditions on the performance of anode-supported Ce0.8Sm0.201.9 film electrolyte

2011 ◽  
Vol 43 (3) ◽  
pp. 305-312 ◽  
Author(s):  
X. Li ◽  
J. Lu ◽  
H. Wang
Keyword(s):  
Glass Transition ◽  
Transition Temperature ◽  
Glass Transition Temperature ◽  
Flexural Strength ◽  
Single Cell ◽  
Open Circuit Voltage ◽  
Open Circuit ◽  
Maximum Power Density ◽  
Film Electrolyte ◽  
Different Temperatures

In order to evaluate the laminating and co-firing technique on the performance of anode-supported Ce0.8Sm0.2O1.9 (SDC) film electrolyte and its single cell, NiO-YSZ and NiOSDC anode-supported SDC film electrolytes were fabricated by laminating 24 sheets of anode plus one sheet of electrolyte and co-firing. La0.4Sr0.6Co0.2Fe0.8O3-? (LSCF)-SDC cathode was coated on the SDC electrolytes to form a single cell. The lamination was tried at different laminating temperatures and pressures and the co-firing was carried out at different temperatures. The results showed that the laminating temperature should above the glass transition temperature (Tg) of the binder. The laminating pressure of 70 MPa resulted in warp of the samples. The best co-firing temperature of the anode-supported SDC film electrolyte was 1400?C. The SDC film electrolyte formed well adherence to the anode. The NiO-YSZ anode had larger flexural strength than the NiO-SDC anode. The NiO-YSZ anode-supported SDC film electrolyte single cell had an open circuit voltage of 0.803 V and a maximum power density of 93.03 mW/cm2 with hydrogen as fuel at 800?C.

scholarly journals Experimental study on the compression characteristics of soft soil based on low temperature effect

2021 ◽  
Vol 9 (4B) ◽  
Author(s):  
Jian Zhang ◽  
◽  
Chunpeng Han ◽  
Jiayi Tian ◽  
Qingjie Dong ◽  
...  
Keyword(s):  
Low Temperature ◽  
Phase Change ◽  
Compression Test ◽  
Variable Temperature ◽  
Soft Soil ◽  
Test Methods ◽  
Variable Load ◽  
Compression Tests ◽  
Different Temperatures ◽  
Freezing Condition

Based on the characteristics of long annual freezing time and short suitable construction period of soft soil in cold region, this paper discusses the feasibility of foundation treatment of soft soil in freezing-thawing layer under freezing condition. The deformation characteristics of soft soil in freezing-thawing layer in Hulunbuir area in China are studied by using two compression test methods, namely, constant temperature and variable load (CTVL) test, variable temperature and variable load (VTVL) test. The compressibility indexes under different temperatures and consolidation pressures are obtained. The research shows that the freezing-thawing soft soil has large compressibility, the maximum strain of CTVL test is 19.89%, and the maximum compression of VTVL test can reach 18.16%. The results of CTVL compression tests show that when the soil temperature is in the range of severe phase change (-1.5℃-0℃), the temperature change has the greatest influence on the compression coefficient of soil. The result of VTVL compression test shows that some additional deformation occurs under the action of low temperature. The additional deformation is further increased when the soil is under high consolidation pressure and in the severe phase change (-1.5℃-0℃).

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