scholarly journals Influence of Heat Treatment on Cyclic Response of Nickel-Based Superalloy Inconel 718 up to Very-High Cycle Regime

Materials ◽  
2020 ◽  
Vol 13 (23) ◽  
pp. 5358
Author(s):  
Mengxiong Zhao ◽  
Zhenhua Zhao ◽  
Lulu Liu ◽  
Gang Luo ◽  
Wei Chen

Cyclic response and fatigue behavior are sensitive to the microstructure of material induced by heat treatment. In this paper, three sets of high-temperature superalloy Inconel 718 with different heat treatment, namely annealed, aged, and directly aged high quality (DAHQ), are compared. Difference in grain size distribution, phase, and precipitate, etc., were investigated using an optical camera and scanning electron microscopy. Yield and ultimate strength were found to increase obviously after aging heat treatment. Self-heating phenomenon at 20 kHz was attenuated as grain size decreased. There was a transition from cyclic hardening to softening. Very-high cycle fatigue (VHCF) behavior of Inconel 718 was tested using an ultrasonic fatigue device. Crack initiation duration occupied greater than 99% of the total fatigue life. It concluded that average grain size influences VHCF strength and crack initiation mechanism, and that self-heating phenomenon is not a decisive factor on VHCF strength for Inconel 718.

Author(s):  
Ming-Liang Zhu ◽  
Fu-Zhen Xuan ◽  
Zhengdong Wang

The fatigue properties of a low strength weld metal in a dissimilar welding joint in high cycle and very high cycle regimes were investigated by fully reversed axial tests in air at room temperature and 370°C. A clear duplex S-N curve existed as a result of the transition of fatigue failure mode from surface-induced failure to internal-induced failure at 370°C, while the S-N curve was continuously decreased at room temperature. A new model was successfully proposed to predict fatigue life, and interpret the crack initiation modes transition from surface inclusion to interior inclusion. It was concluded that cracks were initiated by competition among non-metallic inclusions, welding pores and discontinuous microstructures in high cycle regime. While in the very high cycle regime, non-metallic inclusions were the dominant crack initiation mechanism which depended on stress level, inclusion size as well as inclusion depth.


2018 ◽  
Vol 165 ◽  
pp. 14004
Author(s):  
Benoît Bracquart ◽  
Charles Mareau ◽  
Nicolas Saintier ◽  
Franck Morel

In this work, the influence of the geometrical defect size on the high cycle fatigue behavior of polycrystalline aluminium with different grain sizes is investigated, to better understand the role of internal length scales. Two sizes of grains and defect are used: 100 μm and 1000 μm, the grain size being controlled with thermomechanical treatments. Fully reversed stress-controlled fatigue tests are then carried out. According to fatigue test results, surface crack initiation is delayed when the grain size is reduced, while an approximation of the fatigue limit shows that it is not much influenced by the average grain size. The relative defect diameter (compared to the grain size) seems to be the leading parameter influencing fatigue crack initiation from a defect. Finally, Electron BackScattered Diffraction (EBSD) maps are collected for specimens with large grains and small defects. Fatigue crack initiation from a defect is found to be strongly impacted by the crystallographic orientation of the surrounding grain, crack initiation preferably occurring in crystals being favorably oriented for plastic slip.


2018 ◽  
Vol 8 (9) ◽  
pp. 1614 ◽  
Author(s):  
Baohua Nie ◽  
Dongchu Chen ◽  
Zihua Zhao ◽  
Jianglong Zhang ◽  
Yu Meng ◽  
...  

The very high cycle fatigue (VHCF) property of TC21 titanium alloy blunt-notched specimens were investigated by using an ultrasonic fatigue test machine with a frequency of 20 kHz. S–N of blunt-notched specimens illustrated a continuous decrease characteristic with a horizontal line over the 105–109 cycle regimes. However, the fatigue life showed a large scatter for blunt-notched specimens. Blunt-notch significantly reduced the fatigue property in the high cycle and very high cycle regimes compared with that of smooth specimens. The crack initiation modes for blunt-notched specimens in the very high cycle regime can be divided into three types: (i) surface initiation, (ii) subsurface with flat facet, and (iii) subsurface with “facet + fine granular area”. The crack initiation mechanism of blunt-notched specimens is discussed in view of the interaction of notch stress gradient distribution and heterogeneous microstructure. Furthermore, the fatigue limit model based on the theory of critical distance (TCD) was modified for the very high cycle regime, and the scatter of the fatigue property of the blunt-notched specimens were well predicted by using this model.


2007 ◽  
Vol 336-338 ◽  
pp. 505-508
Author(s):  
Cheol Jin Kim ◽  
In Sup Ahn ◽  
Kwon Koo Cho ◽  
Sung Gap Lee ◽  
Jun Ki Chung

LiNiO2 thin films for the application of cathode of the rechargeable battery were fabricated by Li ion diffusion on the surface oxidized NiO layer. Bi-axially textured Ni-tapes with 50 ~ 80 μm thickness were fabricated using cold rolling and annealing of Ni-rod prepared by cold isostatic pressing of Ni powder. Surface oxidation of Ni-tapes were conducted using tube furnace or line-focused infrared heater at 700 °C for 150 sec in flowing oxygen atmosphere, resulted in NiO layer with thickness of 400 and 800 μm, respectively. After Li was deposited on the NiO layer by thermal evaporation, LiNiO2 was formed by Li diffusion through the NiO layer during subsequent heat treatment using IR heater with various heat treatment conditions. IR-heating resulted in the smoother surface and finer grain size of NiO and LiNiO2 layer compared to the tube-furnace heating. The average grain size of LiNiO2 layer was 0.5~1 μm, which is much smaller than that of sol-gel processed LiNiO2. The reacted LiNiO2 region showed homogeneous composition throughout the thickness and did not show any noticeable defects frequently found in the solid state reacted LiNiO2, but crack and delamination between the reacted LiNiO2 and Ni occurred as the reaction time increased above 4hrs.


2005 ◽  
Vol 475-479 ◽  
pp. 3985-3988
Author(s):  
Chun Gen Zhou ◽  
Na Wang ◽  
Sheng Kai Gong ◽  
Hui Bin Xu

The as-sprayed zirconia coating had an average grain size of 67 nm. Thermal treatment results showed that the grains of the nanostructured coating grew slightly below 900°C, whereas over 1000°C the gains grew rapidly. The thermal diffusivity of the coating increases with increasing heat-treatment temperatures.


Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1023 ◽  
Author(s):  
Byung-Hoon Lee ◽  
Sung-Woo Park ◽  
Soong-Keun Hyun ◽  
In-Sik Cho ◽  
Kyung-Taek Kim

The effect of heat treatment condition on non-Cu AA7021 alloy was investigated with respect to mechanical properties and very high cycle fatigue behavior. With a focus on the influence of heat treatment, AA7021 alloy was solution heat-treated at 470 °C for 4 h and aged at 124 °C. Comparing the results of solution-treated and peak-aged AA7021 alloy shows a significant increase in Vickers hardness and tensile strength. The hardness of AA7021 alloy was increased by 65% after aging treatment, and both tensile strength and yield strength were increased by 50~80 MPa in each case. In particular, this paper investigated the very high cycle fatigue behavior of AA7021 alloy with the ultrasonic fatigue testing method using a resonance frequency of 20 kHz. The fatigue results showed that the stress amplitude of peak-aged AA7021 alloy was about 50 MPa higher than the solution-treated alloy at the same fatigue cycles. Furthermore, it was confirmed that the size of the crack initiation site was larger after peak aging than after solution treatment.


2021 ◽  
Vol 1016 ◽  
pp. 125-131
Author(s):  
Masahiro Goto ◽  
T. Yamamoto ◽  
S.Z. Han ◽  
J. Kitamura ◽  
J.H. Ahn ◽  
...  

On the thermomechanical treatments of Cu-Ni-Si alloy, cold-rolling (CR) before solution heat treatment (SHT) is commonly conducted to eliminate defects in a casting slab. In addition, a rolling is applied to reduce/adjust the thickness of casting slab before SHT. In a heavily deformed microstructure by CR, on the other hand, grain growth during a heating in SHT is likely to occur as the result of recrystallization. In general, tensile strength and fatigue strength tend to decrease with an increase in the grain size. However, the effect of difference in grain sizes produced by with and without CR before SHT on the fatigue strength is unclear. In the present study, fatigue tests of Cu-6Ni-Si alloy smooth specimens with a grain fabricated through different thermomechanical processes were conducted. The fatigue behavior of Cu-Ni-Si alloy was discussed.


2021 ◽  
Vol 1016 ◽  
pp. 1503-1509
Author(s):  
Kosuke Ueki ◽  
Soh Yanagihara ◽  
Kyosuke Ueda ◽  
Masaaki Nakai ◽  
Takayoshi Nakano ◽  
...  

The Co-20Cr-15W-10Ni (CCWN, mass%) alloy has excellent corrosion resistance and strength-ductility balance and is applied in almost all balloon-expandable stent platforms. To further reduce the invasiveness of stent placement, it is necessary to reduce the diameter of the stent. That is, both high strength and high ductility should be achieved while maintaining a low yield stress. In our previous studies, it was discovered that low-temperature heat-treatment (LTHT) at 873 K improves the elongation of the CCWN alloy. In this study, we focused on the grain refinement by swaging and static recrystallization to improve the strength of the alloy. The as-swaged alloy was recrystallized at 1373–1473 K for 100–300 s, followed by LTHT. A fine grain structure with an average grain size of 3–17 μm was obtained by static recrystallization. The η-phase (M12X-M6X type precipitates, M: metallic elements, X: C and/or N) formed during the recrystallization at 1373–1448 K. The alloys recrystallized at 1448 and 1473 K had a homogeneous structure with a small variation in the grain size. On the other hand, the alloys recrystallized at 1373 and 1423 K had an inhomogeneous structure in which fine and coarse grains were mixed. Both the strength and ductility of the CCWN alloy were improved by combining high-temperature short-time recrystallization and LTHT.


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