scholarly journals Texture Hardening Observed in Mg–Zn–Nd Alloy Processed by Equal-Channel Angular Pressing (ECAP)

Metals ◽  
2019 ◽  
Vol 10 (1) ◽  
pp. 35 ◽  
Author(s):  
Jitka Stráská ◽  
Peter Minárik ◽  
Stanislav Šašek ◽  
Jozef Veselý ◽  
Jan Bohlen ◽  
...  

The addition of Nd significantly improves the mechanical properties of magnesium alloys. However, only limited amounts of Nd or other rare earth (RE) elements should be used due to their high price. In this study, a low-alloyed Mg–1% Zn–1% Nd (ZN11) alloy was designed and processed by hot extrusion and subsequent equal-channel angular pressing (ECAP) in order to achieve a very fine-grained condition with enhanced strength. The microstructure, texture, and mechanical properties were thoroughly studied. The microstructure after 8 passes through ECAP was homogeneous and characterized by an average grain size of 1.5 µm. A large number of tiny secondary phase precipitates were identified as ordered Guinier–Preston (GP) zones. Detailed analysis of the Schmid factors revealed the effect of the texture on deformation mechanisms. ECAP processing more than doubled the achieved yield compression strength (YCS) of the ZN11 alloy. Significant strengthening by ECAP is caused by grain refinement and the formation of ordered Guinier–Preston zones and particles of a secondary γ-phase.

2017 ◽  
Vol 23 (3) ◽  
pp. 222 ◽  
Author(s):  
Ondřej Hilšer ◽  
Stanislav Rusz ◽  
Wojciech Maziarz ◽  
Jan Dutkiewicz ◽  
Tomasz Tański ◽  
...  

<p>Equal channel angular pressing (ECAP) method was used for achieving very fine-grained structure and increased mechanical properties of AZ31 magnesium alloy. The experiments were focused on the, in the initial state, hot extruded alloy. ECAP process was realized at the temperature 250°C and following route Bc. It was found that combination of hot extrusion and ECAP leads to producing of material with significantly fine-grained structure and improves mechanical properties. Alloy structure after the fourth pass of ECAP tool with helix matrix 30° shows a fine-grained structure with average grain size of 2 µm to 3 µm and high disorientation between the grains. More experimental results are discussed in this article.</p>


2009 ◽  
Vol 633-634 ◽  
pp. 311-319
Author(s):  
Sergey V. Dobatkin ◽  
Yuri Estrin ◽  
Valerij V. Zakharov ◽  
T.D. Rostova ◽  
O.G. Ukolova ◽  
...  

The effect of equal channel angular pressing (ECAP) on the structure and mechanical properties of Al-4% Mg-1.5% Mn-0.4% Zr and Al-4% Mg-1.5% Mn-0.4% Zr-0.4% Sc alloys in the initial as-cast state was studied. The ECAP processing was shown to lead to the formation of predominantly submicrocrystalline structure with an average grain size of 850 nm in the Al-Mg-Mn-Zr-Sc alloy and 1060 nm in the Al-Mg-Mn-Zr alloy. It is remarkable that both strength and ductility of the two alloys were enhanced by ECAP. The highest strength was observed in the Al–Mg–Mn–Zr–Sc alloy (UTS = 425MPa), in combination with elongation to failure of EL=17 %.


2007 ◽  
Vol 340-341 ◽  
pp. 913-917 ◽  
Author(s):  
Seung Chae Yoon ◽  
Young Gi Jeong ◽  
Sun Ig Hong ◽  
Byong Sun Chun ◽  
Hong Rho Lee ◽  
...  

Mg and Mg alloys are promising materials for light weight high strength applications. In this paper, grain refinement of pure Mg using severe plastic deformation was tried to enhance mechanical properties of the hard-to-deform metallic material. The microstructure and the mechanical properties of Mg processed by equal channel angular pressing (ECAP) at various processing temperatures were investigated experimentally. ECAP of channel angle of 90o and corner angle of 0o was successful without fracture of the samples at 300 oC. The hardness of the ECAP processed Mg decreased with increasing ECAP processing temperature. The effect of temperature on the hardness and microstructure of the ECAP processed Mg were explained by the dislocation glide in the basal plane and non-basal slip systems and the dynamic recrystallization and recovery.


Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 607
Author(s):  
A. I. Alateyah ◽  
Mohamed M. Z. Ahmed ◽  
Yasser Zedan ◽  
H. Abd El-Hafez ◽  
Majed O. Alawad ◽  
...  

The current study presents a detailed investigation for the equal channel angular pressing of pure copper through two regimes. The first was equal channel angular pressing (ECAP) processing at room temperature and the second was ECAP processing at 200 °C for up to 4-passes of route Bc. The grain structure and texture was investigated using electron back scattering diffraction (EBSD) across the whole sample cross-section and also the hardness and the tensile properties. The microstructure obtained after 1-pass at room temperature revealed finer equiaxed grains of about 3.89 µm down to submicrons with a high density of twin compared to the starting material. Additionally, a notable increase in the low angle grain boundaries (LAGBs) density was observed. This microstructure was found to be homogenous through the sample cross section. Further straining up to 2-passes showed a significant reduction of the average grain size to 2.97 µm with observable heterogeneous distribution of grains size. On the other hand, increasing the strain up to 4-passes enhanced the homogeneity of grain size distribution. The texture after 4-passes resembled the simple shear texture with about 7 times random. Conducting the ECAP processing at 200 °C resulted in a severely deformed microstructure with the highest fraction of submicron grains and high density of substructures was also observed. ECAP processing through 4-passes at room temperature experienced a significant increase in both hardness and tensile strength up to 180% and 124%, respectively.


2012 ◽  
Vol 468-471 ◽  
pp. 2124-2127 ◽  
Author(s):  
Shao Feng Zeng ◽  
Kai Huai Yang ◽  
Wen Zhe Chen

Equal channel angular pressing (ECAP) was applied to a commercial AZ61 magnesium alloy for up to 8 passes at temperatures as low as 473K. Microstructures and mechanical properties of as-received and ECAP deformed samples were investigated. The microstructure was initially not uniform with a “bimodal” grain size distribution but became increasingly homogeneous with further ECAP passes and the average grain size was considerably reduced from over 26 μm to below 5 μm. The ultimate tensile strength (UTS) decreases clearly after one pass, but increases significantly up to two passes, and then continuously slowly decreases up to six passes, and again increases slightly up to eight passes. In contrast, the uniform elongation increased significantly up to 3 passes, followed by considerable decrease up to 8 passes. These observations may be attributed to combined effects of grain refinement and texture development.


2006 ◽  
Vol 114 ◽  
pp. 91-96 ◽  
Author(s):  
Maxim Yu. Murashkin ◽  
M.V. Markushev ◽  
Julia Ivanisenko ◽  
Ruslan Valiev

The effects of equal channel angular pressing (ECAP), further heat treatment and rolling on the structure and room temperature mechanical properties of the commercial aluminum alloys 6061 (Al-0.9Mg-0.7Si) and 1560 (Al-6.5Mg-0.6Mn) were investigated. It has been shown that the strength of the alloys after ECAP is higher than that achieved after conventional processing. Prior ECAP solution treatment and post-ECAP ageing can additionally increase the strength of the 6061 alloy. Under optimal ageing conditions a yield strength (YS) of 434 MPa and am ultimate tensile strength (UTS) of 470 MPa were obtained for the alloy. Additional cold rolling leads to a YS and UTS of 475 and 500 MPa with 8% elongation. It was found that the post-ECAP isothermal rolling of the 1560 alloy resulted in the formation of a nano-fibred structure and a tensile strength (YS = 540 MPa and UTS = 635 MPa) that has never previously been observed in commercial non-heat treatable alloys.


2010 ◽  
Vol 667-669 ◽  
pp. 731-736 ◽  
Author(s):  
Irina P. Semenova ◽  
Alexander Medvedev

This work presents the possibility of strength enhancement in the -alloy Ti-6.8Mo-4.5Fe-1.5Al via equal channel angular pressing at room temperature without precipitation of a secondary -phase. Influence of the initial structure of the alloy and ageing temperature on the density of precipitations and dimensions of the secondary -phase is revealed. It has been stated that combination of the solid solution treatment with the subsequent ECAP processing and final ageing is an effective way to achieve superior strength and ductility.


2007 ◽  
Vol 124-126 ◽  
pp. 1397-1400 ◽  
Author(s):  
Byoung Soo Lee ◽  
Hoon Cho

The microstructures and mechanical properties of unidirectional deformation structured Al alloy during ECAP with various deformation routes were investigated. In order to fabricate unidirectional deformation structure for Al alloy, hot extrusion was carried out. It was found that the deformation route A in ECAP routes is the dominant route for the grain refinement and strengthening. In deformation route A, the high strength ultra-fine grained Al alloy with a grain size of ~ 200 nm was obtained due to the accumulation of consecutive strain process. In contrast, the strength of ECAP’ed Al alloy produced via deformation route C was greatly increased after one pass because the grains were strained and cancelled each pass. By contrast, the equiaxed grains were obtained in deformation route BC because the sample was rotated 90 O in the same sense in each pass. The deformation route BC was superior to the deformation route C because the deformation route BC was more favorable than the deformation route C in the accumulation of consecutive strain. It is also found that unidirectional deformation structured Al alloy via hot extrusion shows similar grain refinement tendency with equiaxed structured Al alloy during ECAP processing.


2008 ◽  
Vol 49 (5) ◽  
pp. 1006-1010 ◽  
Author(s):  
Eun Jeong Kwak ◽  
Cheon Hee Bok ◽  
Min Hong Seo ◽  
Taek-Soo Kim ◽  
Hyoung Seop Kim

Sign in / Sign up

Export Citation Format

Share Document