scholarly journals Heat Treatment Design for a QP Steel: Effect of Partitioning Temperature

Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1136
Author(s):  
Marcel Carpio ◽  
Jessica Calvo ◽  
Omar García ◽  
Juan Pablo Pedraza ◽  
José María Cabrera
Keyword(s):  
Retained Austenite ◽  
High Strength Steels ◽  
High Strength ◽  
Tensile Tests ◽  
Quenching Temperature ◽  
Advanced High Strength Steels ◽  
New Family ◽  
Automotive Parts ◽  
Fresh Martensite ◽  
Industry Needs

Designing a new family of advanced high-strength steels (AHSSs) to develop automotive parts that cover early industry needs is the aim of many investigations. One of the candidates in the 3rd family of AHSS are the quenching and partitioning (QP) steels. These steels display an excellent relationship between strength and formability, making them able to fulfill the requirements of safety, while reducing automobile weight to enhance the performance during service. The main attribute of QP steels is the TRIP effect that retained austenite possesses, which allows a significant energy absorption during deformation. The present study is focused on evaluating some process parameters, especially the partitioning temperature, in the microstructures and mechanical properties attained during a QP process. An experimental steel (0.2C-3.5Mn-1.5Si (wt%)) was selected and heated according to the theoretical optimum quenching temperature. For this purpose, heat treatments in a quenching dilatometry and further microstructural and mechanical characterization were carried out by SEM, XRD, EBSD, and hardness and tensile tests, respectively. The samples showed a significant increment in the retained austenite at an increasing partitioning temperature, but with strong penalization on the final ductility due to the large amount of fresh martensite obtained as well.

scholarly journals Effect of Quenching and Partitioning Temperatures in the Q-P Process on the Properties of AHSS with Various Amounts of Manganese and Silicon

2012 ◽  
Vol 706-709 ◽  
pp. 2734-2739 ◽  
Author(s):  
Hana Jirková ◽  
Ludmila Kučerová ◽  
Bohuslav Mašek
Keyword(s):  
Tensile Strength ◽  
Retained Austenite ◽  
Isothermal Holding ◽  
Bainitic Ferrite ◽  
High Strength Steels ◽  
High Strength ◽  
Experimental Program ◽  
Quenching Temperature ◽  
Quenching And Partitioning ◽  
Advanced High Strength Steels

The use of the combined influence of retained austenite and bainitic ferrite to improve strength and ductility has been known for many years from the treatment of multiphase steels. Recently, the very fine films of retained austenite along the martensitic laths have also become the centre of attention. This treatment is called the Q-P process (quenching and partitioning). In this experimental program the quenching temperature and the isothermal holding temperature for diffusion carbon distribution for three advanced high strength steels with carbon content of 0.43 % was examined. The alloying strategies have a different content of manganese and silicon, which leads to various martensite start and finish temperatures. The model treatment was carried out using a thermomechanical simulator. Tested regimes resulted in a tensile strength of over 2000MPa with a ductility of above 14 %. The increase of the partitioning temperature influenced the intensity of martensite tempering and caused the decrease of tensile strength by 400MPa down to 1600MPa and at the same time more than 10 % growth of ductility occurred, increasing it to more than 20%.

scholarly journals Substructure Development and Damage Initiation in a Carbide-Free Bainitic Steel upon Tensile Test

Metals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 1261
Author(s):  
Mari Carmen Taboada ◽  
Amaia Iza-Mendia ◽  
Isabel Gutiérrez ◽  
Denis Jorge-Badiola
Keyword(s):  
Retained Austenite ◽  
High Strength Steels ◽  
High Strength ◽  
Tensile Tests ◽  
Formation Mechanisms ◽  
Tempered Martensite ◽  
Damage Initiation ◽  
Advanced High Strength Steels ◽  
Significant Strength ◽  
The Stability

Carbide-free bainitic (CFB) steels belong to the family of advanced high strength steels (AHSS) that are struggling to become part of the third-generation steels to be marketed for the automotive industry. The combined effects of the bainitic matrix and the retained austenite confers a significant strength with a remarkable ductility to these steels. However, CFB steels usually show much more complex microstructures that also contain MA (Martensite–Austenite) phase and auto-tempered martensite (ATM). These phases may compromise the ductility of CFB steels. The present work analyzes the substructure evolution during tensile tests in the necking zone, and deepens into the void and crack formation mechanisms and their relationship with the local microstructure. The combination of FEG-SEM imaging, EBSD, and X-ray diffraction has been necessary to characterize the substructure development and damage initiation. The bainite matrix has shown great ductility through the generation of high angle grain boundaries and/or large orientation gradients around voids, which are usually found close to the bainite and MA/auto-tempered martensite interfaces or fragmenting the MA phase. Special attention has been paid to the stability of the retained austenite (RA) during the test, which may eventually be transformed into martensite (Transformation Induced Plasticity, or TRIP effect).

scholarly journals The Role of Retained Austenite in Tempered Martensite Embrittlement of 4340 and 300-M Steels Investigated through Rapid Tempering

Metals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1349
Author(s):  
Virginia K. Euser ◽  
Don L. Williamson ◽  
Kip O. Findley ◽  
Amy J. Clarke ◽  
John G. Speer
Keyword(s):  
Retained Austenite ◽  
High Strength Steels ◽  
High Strength ◽  
Tensile Tests ◽  
Austenite Decomposition ◽  
Tempered Martensite ◽  
Mechanical Transformation ◽  
Fresh Martensite ◽  
Rapid Tempering

Tempered martensite embrittlement (TME) is investigated in two medium carbon, high strength steels, 4340 (low silicon) and 300-M (high silicon), via rapid (1, 10, or 100 s) and conventional (3600 s) tempering. Rapid tempering of 4340 diminishes the depth of the TME toughness trough, where improvements in impact toughness correspond to the suppression of retained austenite decomposition. In 300-M, retained austenite decomposition is suppressed to an even greater extent by rapid tempering. While toughness improves overall after rapid tempering, TME severity remains consistent in 300-M across the tempering conditions examined. Through interrupted tensile tests, it was found that the 300-M conditions that exhibit TME are associated with mechanically unstable retained austenite. Unstable retained austenite is shown to mechanically transform early in the deformation process, presumably resulting in fresh martensite adjacent to interlath cementite that ultimately contributes to TME. The present results emphasize the role of both the thermal decomposition and mechanical transformation of retained austenite in the manifestation of TME.

Mechanical properties and microstructure of low carbon ultra-high strength steels (UHSS) microalloyed with boron

2012 ◽  
Vol 1373 ◽  
Author(s):  
I. Mejía ◽  
A. García de la Rosa ◽  
A. Bedolla-Jacuinde ◽  
J.M. Cabrera
Keyword(s):  
Mechanical Properties ◽  
Research Work ◽  
High Strength Steels ◽  
High Strength ◽  
Tensile Tests ◽  
Low Carbon ◽  
Advanced High Strength Steels ◽  
New Family ◽  
Ultra High Strength Steels ◽  
Hot Rolled

ABSTRACTThe aim of this research work is to study the effect of boron addition on mechanical properties and microstructure of a new family of low carbon NiCrVCu advanced high strength steels (AHSS). Experimental steels are thermo-mechanically processed (TMP) (hot-rolled+quenched). Results show that the microstructure of these steels contains bainite and martensite, predominantly, which nucleate along prior austenite grain boundaries (GB). On the other hand, tensile tests reveal that the TMP steels have YS (0.2% offset) of 978 MPa, UTS of 1140 MPa and EL of 18%. On the basis of exhibited microstructure and mechanical properties, these experimental steels are classified as bainitic-martensitic complex phase (CP) advanced ultra-high strength steels (UHSS).

Influence of the Processing Variables on the Microstructure Evolution of a Bainitic Carbide-Free Steel

2016 ◽  
Vol 879 ◽  
pp. 867-872 ◽  
Author(s):  
M.C. Taboada ◽  
I. Gutiérrez ◽  
D. Jorge-Badiola ◽  
S.M.C. van Bohemen ◽  
F. Hisker ◽  
...  
Keyword(s):  
Retained Austenite ◽  
High Strength Steels ◽  
High Strength ◽  
High Volume ◽  
X Ray Diffraction ◽  
Tempered Martensite ◽  
Trip Steels ◽  
Volume Fractions ◽  
Advanced High Strength Steels ◽  
Processing Variables

New trends focused on achieving higher performance steels has led to a so-called 3rd Generation Advanced High Strength Steels (AHSS), in which the typical polygonal ferrite found in TRIP steels as a matrix phase is replaced by harder phases as Carbide-Free Bainite (CFB) and/or (tempered) martensite. Besides, large volume fractions of retained austenite (R.A.) with adequate stability are aimed for to improve the formability of the steels. Si containing steels are regarded as the most suitable to retard cementite formation and consequently reach high volume fractions of RA. In this work, CFB annealing schedules were applied to dilatometer samples of Fe-0.22C-2.0Mn-1.3Si. The overaging temperature TB was varied between 390 oC and 480 oC, and other processing variables investigated were the austenitizing temperature Taus, and the overaging holding time tB. The annealed samples analyzed with LOM, FEG-SEM, EBSD and X-ray diffraction techniques show that markedly different complex microstructures made up of bainite, ferrite, MA phase and retained austenite (R.A) are accomplished depending on the specific thermal cycle. These results are described in detail and discussed in relation to the dilatometry measurements.

scholarly journals Enhancing the Mechanical Properties of a Hot Rolled High-Strength Steel Produced by Ultra-Fast Cooling and Q&P Process

Metals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 958 ◽  
Author(s):  
Teng Wu ◽  
Run Wu ◽  
Bin Liu ◽  
Wen Liang ◽  
Deqing Ke
Keyword(s):  
Retained Austenite ◽  
High Strength Steels ◽  
High Strength ◽  
Controlled Rolling ◽  
Grain Structure ◽  
Ultra Fast Cooling ◽  
Advanced High Strength Steels ◽  
Fast Cooling ◽  
Austenite Grains ◽  
Hot Rolled

The quenching and partitioning (Q&P) process of advanced high strength steels results in a significant enhancement in their strength and ductility. The development of controlled rolling and cooling technology provides an efficient tool for microstructural design in steels. This approach allows to control phase transformations in order to generate the desired microstructure in steel and, thus, to achieve the required properties. To refine grain structure in a Fe-Si-Mn-Nb steel and to generate the microstructure consisting of martensitic matrix with embedded retained austenite grains, hot rolling and pressing combined with ultrafast cooling and Q&P process is employed. The slender martensite in hot rolled Q&P steel improves the strength of test steel and the flake retained austenite improves the plasticity and work hardening ability through the Transformation Induced Plasticity (TRIP) effect.

Quenching and Partitioning of Ni-Added High Strength Steels

2007 ◽  
Vol 539-543 ◽  
pp. 4476-4481 ◽  
Author(s):  
F.C. Rizzo ◽  
A.R. Martins ◽  
John G. Speer ◽  
David K. Matlock ◽  
A. Clarke ◽  
...  
Keyword(s):  
Retained Austenite ◽  
High Strength Steels ◽  
High Strength ◽  
Processing Parameters ◽  
Carbide Formation ◽  
X Ray Diffraction ◽  
Quenching And Partitioning ◽  
Steel Microstructure ◽  
Advanced High Strength Steels ◽  
Treatment Procedures

High strength steels containing significant fractions of retained austenite have been developed in recent years, and are the subject of growing commercial interest when associated with the TRIP phenomenon during deformation. A new process concept “quenching and partitioning” (Q&P) has been proposed by CSM/USA, and the results show the potential to create a new kind of steel microstructure with controlled amounts of retained austenite, enriched by carbon partitioning. Four steels containing C, Si, Mn, Ni, Cr and Mo, were designed with variation in the Ni and C content, aiming to decrease Bs temperature and to suppress carbide formation during the partitioning treatment. Several heat-treatment procedures were performed in specimens previously machined for tensile testing, while x-ray diffraction was used to determine the fraction of retained austenite. The tensile test results showed that except for the high C high Ni alloy, most of the processing conditions resulted in strengths superior to those of advanced high strength steels (AHSS), although it is importantly recognized that higher alloy additions were used in this study, in comparison with conventional AHSS grades.. A variety of strength and ductility combinations were observed, confirming the potential of the Q&P process and illustrating the strong influence of the final microstructure on the mechanical properties. Experimental results for samples partitioned at 400 °C indicate that higher ultimate tensile strength is associated with higher fraction of retained austenite for multiple heat treatments of each alloy investigated. The amount of retained austenite obtained was generally lower than that predicted by the model. Further studies are in progress to understand the influence of alloying and processing parameters (time/temperature) on the partitioning of carbon and precipitation of transition carbides.

scholarly journals The Evaluation of Laser Weldability of the Third-Generation Advanced High Strength Steel

Metals ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 1051 ◽  
Author(s):  
António B. Pereira ◽  
Rafael O. Santos ◽  
Bruno S. Carvalho ◽  
Marilena C. Butuc ◽  
Gabriela Vincze ◽  
...  
Keyword(s):  
Automotive Industry ◽  
Greenhouse Gas Emission ◽  
High Strength Steels ◽  
High Strength ◽  
Tensile Tests ◽  
Weld Bead ◽  
Uniaxial Tensile ◽  
Third Generation ◽  
Advanced High Strength Steels

To meet the demands of vehicular safety and greenhouse gas emission reduction, the automotive industry is increasingly using advanced high strength steels (AHSS) in the production of the components. With the development of the new generation of AHSS, it is essential to study their behavior towards manufacturing processes used in the automotive industry. For this purpose, the welding capability of newly developed third-generation Gen3 980T steel was investigated using the Nd:YAG (Neodymium:Yittrium Aluminum Garnet) laser-welding with different parameter conditions. The analysis was made by uniaxial tensile tests, micro-hardness, Scanning Electron Microscopy (SEM) and X-Ray Diffraction (XRD). The criteria used to evaluate the quality of the weld were the distance between the fracture and the weld bead and the surface finish. A relationship between the quality of the weld and the energy density was observed, expressed by a partial penetration for values below the optimal, and by irregularities in the weld bead and a high number of spatters for the values above the optimal.

scholarly journals Addressing Retained Austenite Stability in Advanced High Strength Steels

2013 ◽  
Vol 738-739 ◽  
pp. 212-216 ◽  
Author(s):  
Elena V. Pereloma ◽  
Azdiar A. Gazder ◽  
Ilana B. Timokhina
Keyword(s):  
Retained Austenite ◽  
Mechanical Stability ◽  
Volume Fraction ◽  
High Strength Steels ◽  
High Strength ◽  
Processing Parameters ◽  
Advanced High Strength Steels ◽  
Austenite Stability ◽  
Retained Austenite Stability ◽  
Size And Morphology

Advances in the development of new high strength steels have resulted in microstructures containing significant volume fractions of retained austenite. The transformation of retained austenite to martensite upon straining contributes towards improving the ductility. However, in order to gain from the above beneficial effect, the volume fraction, size, morphology and distribution of the retained austenite need to be controlled. In this regard, it is well known that carbon concentration in the retained austenite is responsible for its chemical stability, whereas its size and morphology determines its mechanical stability. Thus, to achieve the required mechanical properties, control of the processing parameters affecting the microstructure development is essential.

scholarly journals Effect of Quenching and Partitioning Heat Treatment on the Fatigue Behavior of 42SiCr Steel

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1699
Author(s):  
Marco Thomä ◽  
Guntram Wagner
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Heat Treatment ◽  
Material Properties ◽  
Retained Austenite ◽  
Fatigue Behavior ◽  
High Strength Steels ◽  
High Strength ◽  
Advanced High Strength Steels ◽  
Scanning Electron

The manufacturing of advanced high-strength steels with enhanced ductility is a persistent aim of research. The ability of a material to absorb high loads while showing a high deformation behavior is a major task for many industrial fields like the mobility sector. Therefore, the material properties of advanced high-strength steels are one of the most important impact factors on the resulting cyclic fatigue behavior. To adjust advanced material properties, resulting in high tensile strengths as well as an enhanced ductility, the heat treatment process of quenching and partitioning (QP) was developed. The quenching takes place in a field between martensite start and martensite finish temperature and the subsequent partitioning is executed at slightly elevated temperatures. Regarding the sparsely investigated field of fatigue research on quenched and partitioned steels, the present work investigates the influence of a QP heat treatment on the resulting microstructure by light and scanning electron microscopy as well as on the mechanical properties such as tensile strength and resistance against fatigue regarding two different heat treatment conditions (QP1, QP2) in comparison to the cold-rolled base material of 42SiCr steel. Therefore, the microscopic analysis proved the presence of a characteristic quenched and partitioned microstructure consisting of a martensitic matrix and partial areas of retained austenite, whereas carbides were also present. Differences in the amount of retained austenite could be observed by using X-ray diffraction (XRD) for the different QP routes, which influence the mechanical properties resulting in higher tensile strength of about 2000 MPa for QP1 compared to about 1600 MPa for QP2. Furthermore, the transition for the fatigue limit was approximated by using stepwise load increase tests (LIT) and afterwards verified by constant amplitude tests (CAT) in accordance with the staircase method, whereas the QP 1 condition reached the highest fatigue strength of 900 MPa. Subsequent light and scanning electron microscopy of selected fractured surfaces and runouts showed a different behavior regarding the size of the fatigue fracture area and also differences in the microstructure of these runouts.

Sign in / Sign up

Export Citation Format

Share Document