scholarly journals Characterization of Natural Consolidated Halloysite Nanotube Structures

Minerals ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1308
Author(s):  
Jiaqi Jin ◽  
Shoeleh Assemi ◽  
Hassnain Asgar ◽  
Greeshma Gadikota ◽  
Thang Tran ◽  
...  

Halloysite is a unique 1:1 clay mineral frequently appearing with nanotubular morphology, and having surfaces of different polarity with interesting and important technological applications. HNTs can be consolidated naturally in the earth by pressure and thermal flows. In this study of natural consolidated HNTs, the strength and hardness of these materials were found to be dependent on the presence of impurities (gibbsite, alunite, quartz, and other silica minerals), which accounted for the increased stability of such samples. In the absence of impurities, the strength of consolidated HNTs was significantly lower. The first 3D mapping of the pore structure of natural consolidated HNT is provided. The contributions of the porosity within the nanotubes and between the nanotubes were delineated using a combination of non-invasive ultra-small and small-angle X-ray scattering (USAXS/SAXS) analyses, BET/BJH pore size analyses, and computed tomography studies. A total porosity of 40%, as determined by X-ray attenuation and He porosimetry, was found for the natural consolidated HNTs, of which about one-third was due to the inter-HNT porosity. Nano-X-ray computed tomography (nano-XCT) analyses also indicated that 76% of the inter-HNT pores were smaller than 150 nm in diameter. The intra-HNT pore size determined by combined USAXS/SAXS and BET/BJH was about 10 nm. This pore network information is essential for the utilization of natural consolidated HNTs as a model geomaterial to investigate the effects of surface characteristics on confined fluid flow.

2016 ◽  
Vol 297 ◽  
pp. 247-258 ◽  
Author(s):  
Timo Hensler ◽  
Markus Firsching ◽  
Juan Sebastian Gomez Bonilla ◽  
Thorsten Wörlein ◽  
Norman Uhlmann ◽  
...  

BioResources ◽  
2020 ◽  
Vol 15 (2) ◽  
pp. 3053-3063
Author(s):  
Liangyan Guo ◽  
Hongchao Cheng ◽  
Junfeng Chen ◽  
Wentao Chen ◽  
Jingyao Zhao

The microscopic pore structure of wood is an important factor that affects its macroscopic properties. In this study, an oak sample was used for pore structure characterization. X-ray computed tomography imaging was carried out, and the scanning results (a multi-layer two-dimensional planar image) were rendered using Avizo software (a three-dimensional stereo image). A digital image processing method was used to identify the characteristics of the three-dimensional pore structure features and to calculate the characteristic parameters, i.e., the porosity (volume/surface), pore area and volume, pore size distribution, and the connectivity. The 27 mm3 oak sample had the following characteristics: a pore size which ranged from 8.56 µm to 1262.84 µm; a pore volume of 1.01 × 1010 µm3; a pore area and volume porosity of 1.12 × 109 µm2 and 37.6%, respectively; a surface porosity range of approximately 36.1% to 39.1%; a pore diameter for axial connection ranging from approximately 164.57 µm to 1262.84 µm; and had corresponding proportions of the pore area and volume of approximately 74.4% and 67.3%, respectively. This information provided useful structural data for the construction of future models.


2013 ◽  
Vol 93 (2) ◽  
pp. 135-149 ◽  
Author(s):  
Dominik Guggisberg ◽  
Marie-Therese Fröhlich-Wyder ◽  
Stefan Irmler ◽  
Mark Greco ◽  
Daniel Wechsler ◽  
...  

2006 ◽  
Vol 45 (3A) ◽  
pp. 1864-1868 ◽  
Author(s):  
Akio Yoneyama ◽  
Nobuaki Amino ◽  
Masamichi Mori ◽  
Masafumi Kudoh ◽  
Tohoru Takeda ◽  
...  

2013 ◽  
Vol 93 (2) ◽  
pp. 121-123 ◽  
Author(s):  
Doreen Fischer ◽  
Sebastian Pagenkemper ◽  
Jens Nellesen ◽  
Stephan Peth ◽  
Rainer Horn ◽  
...  

2015 ◽  
Vol 95 (3) ◽  
pp. 231-235 ◽  
Author(s):  
Joann K. Whalen ◽  
Liwen Han ◽  
Pierre Dutilleul

Whalen, J. K., Han L. and Dutilleul, P. 2015. Burrow refilling behavior of Aporrectodea turgida (Eisen) and Lumbricus terrestris L. as revealed by X-ray computed tomography scanning: Graphical and quantitative analyses. Can. J. Soil Sci. 95: 231–235. Solute and gas transport through earthworm burrows is altered when burrows become refilled. Earthworm burrow refilling was evaluated with non-invasive X-ray computed tomography in undisturbed soil cores. Proportionally, Lumbricus terrestris refilled burrows had more air-filled space left around their perimeter than those of Aporrectodea turgida, which often were completely refilled.


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