scholarly journals Recovering Scandium from Scandium Rough Concentrate Using Roasting-Hydrolysis-Leaching Process

Processes ◽  
2020 ◽  
Vol 8 (3) ◽  
pp. 365 ◽  
Author(s):  
Junhui Xiao ◽  
Yang Peng ◽  
Wei Ding ◽  
Tao Chen ◽  
Kai Zou ◽  
...  

In this study, a roasting-hydrolysis-acid leaching process is used to extract scandium from the scandium rough concentrate. The scandium rough concentrate containing Sc2O3 of 76.98 g/t was obtained by magnetic separation, gravity separation, and electric separation from Sc-bearing Vi-Ti magnetite tailings in the Panxi area of China. The majority of scandium in scandium rough concentrate mainly occurs in diopside, titanopyroxene, montmorillonite, chlorite, talc, aluminosilicate minerals, and isomorphism. Sodium salt and scandium coarse concentrate are added into the roasting furnace for roasting, which makes the fusion reaction of silicon, aluminum and sodium salt to produce soluble salts such as sodium silicate and sodium metaaluminate. Scandium is further recovered from the hydrolysis residue by acid leaching. Test results show scandium leaching recovery of 95.12% and the acid leaching residue with Sc2O3 content of 8.12 g/t are obtained, while the extraction of scandium is obvious. There is no obvious peak value of Scandium spectrum in hydrochloric acid leach residue. Most of scandium in hydrolytic residue is dissolved into Sc3+ and enters into the liquid phase. The main minerals in leach residue are perovskite, ferric silicate, and olivine.

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 810
Author(s):  
Zhanyong Guo ◽  
Ping Guo ◽  
Guang Su ◽  
Fachuang Li

In this paper, nickel-containing residue, a typical solid waste produced in the battery production process, was used to study the cavitation characteristics of ultrasonic waves in a liquid–solid reaction. The ultrasonically-enhanced leaching technology for multicomponent and complex nickel-containing residue was studied through systematic ultrasonic-conventional comparative experiments. An ultrasonic leaching kinetics model was established which provided reliable technological guidance and basic theory for the comprehensive utilization of nickel-containing residue. In the study, it was found that ultrasonically-enhanced leaching for 40 min obtained the same result as conventional leaching for 80 min, and the Ni extraction degree reached more than 95%. According to the kinetic fitting of the leaching process, it was found that the sulfuric acid leaching process belonged to the diffusion-controlled model of solid product layers under conventional and ultrasonic conditions, and the activation energy of the reaction was Ea1 = 17.74 kJ/mol and Ea2 = 5.04 kJ/mol, respectively.


2012 ◽  
Vol 588-589 ◽  
pp. 614-617
Author(s):  
Zhi Hua Wang ◽  
Mei Ling Li ◽  
Jian Zhang ◽  
Li Wang ◽  
Yong Xu

The Equivalent Turn Number of Coil (ETNC) is proposed for induction coil design. Simulation results show that the vibrationonthe induction coil’s structure. The optimized coil is composed by two symmetry parts on the condition of sinusoidal vibration. The effective value of output EMF of optimized coil increases 51.39% than uniform coil’s. In the experiment, the optimized and uniform coils are fabricated with 600 turns and comparatively studied in the same vibration-to-electrical generator. The test results show that the peak-to-peak value and effective value of output EMF of the optimized coil can increase up to 52.59% and 48.76%, respectively, compared with the uniform coil.


2013 ◽  
Vol 765-767 ◽  
pp. 3158-3161
Author(s):  
Jun Liu ◽  
Zheng Li Zhang

Tests of bird strike have been carried out on plate made from LY-12 Aluminium. The test was down with the projectile impacting the target perpendicularly at velocity of 40m/s, 80m/s, 120m/s respectively. The displacement-time history curves and strain-time history curves of on LY-12 Aluminium plate were measured. The good agreement of the results between two specimens in one group indicated that the results tested in the presnet paper are reliable. The dynamic response of the plate and damage modes of the bird influenced by striking velocity were analyzed. The peak value of the displacement linear enlarged with the increasing of the striking velocity. The test results in the present paper provided valuable data for aircraft design impacted by bird, and also provided abundant test datas for the numerical simulation model applied in bird striking.


2013 ◽  
Vol 591 ◽  
pp. 122-125
Author(s):  
Li Jiao Yang ◽  
Si Chen ◽  
Yan Zhang ◽  
Nan Chun Chen ◽  
Jun Gao ◽  
...  

Extracting indium from water quenching slag, which contains poor indium, by two process of leaching, the effect of different oxidants and dosages on the leaching rate of indium in water quenching slag were studied. The leaching conditions: temperature 80 °C, leaching time 2 h, the liquid to solid ratio of neutral leaching 8︰1, the liquid to solid ratio of acid leaching 2︰1, initial concentration of sulfuric acid 500 g·L-1, adding different oxidants, the concentration was detected by crystal violet spectrophotometry. Test results showed that the leaching rate of indium was significantly improved by adding hydrogen peroxide and potassium permanganate. Compared with the effect of different oxidants, the effect of potassium permanganate was significantly higher than that of hydrogen peroxide on the leaching rate of indium.


2011 ◽  
Vol 94-96 ◽  
pp. 1146-1151 ◽  
Author(s):  
Guan Rong ◽  
Xiao Jiang Wang

Permeability test for complete stress-strain process of coarse sandstone were carried out in triaxial test instrument. On the basis of test results, the influence of confining pressure and strain on the hydraulic conductivity was discussed. It is shown that in the complete stress-strain process, hydraulic conductivity changes in the law that presents the same character with the curve of stress-strain. The hydraulic conductivity reduces slightly with the increase of deviatoric stress in the stage of micro fracture compressing and elastic; In the elastoplastic stage, along with the expansion of new fractures, the hydraulic conductivity increases slowly at first and then reaches sharply to the maximum value after peak point; In the post-peak stage, the fracture which controls the hydraulic conductivity of coarse sandstone is compressed because of the confining pressure and the hydraulic conductivity decreases. During the process of deformation and failure, the hydraulic conductivity is more sensitive to the change of circumferential strain. With the increase of confining pressure, the increased value from initial to peak value and the decreased value from peak to residual value decreases.


Minerals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 613
Author(s):  
Kevin Cleary Wanta ◽  
Widi Astuti ◽  
Indra Perdana ◽  
Himawan Tri Bayu Murti Petrus

The kinetics study has an essential role in the scale-up process because it illustrates the real phenomena of a process. This study aims to develop a mathematical model that can explain the mechanism of the leaching process of laterite ore using a low concentration of the citric acid solution and evaluate that model using the experimental data. As a raw material, this process used powder-shaped limonite laterite ores with a size of 125–150 µm. The leaching process is carried out using 0.1 M citric acid solution, F:S ratio of 1:20, and a leaching time of 2 h. The temperature parameter was varied at 303, 333, and 358 K. The experimental results showed that the higher the operating temperature, the higher the extracted nickel. The results of this experiment were used to evaluate the shrinking core kinetics model and the lumped model. The simulation results for both models show that the lumped model can provide better simulation results. Quantitatively, the percentage of errors from the shrinking core model is around 3.5 times greater than the percentage of errors from using the lumped model. This result shows that in this leaching process, the process mechanism that occurs involves the reactant diffusion step and the chemical reactions step; those steps run simultaneously.


2019 ◽  
Vol 36 (9) ◽  
pp. 1244-1257 ◽  
Author(s):  
Ping Wu ◽  
Lijuan Zhang ◽  
Yongdi Liu ◽  
Xinxin Xie ◽  
Jun Zhou ◽  
...  

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