Сравнительный анализ физико-механических свойств природных материалов, применяемых в качестве загрузки фильтров

2020 ◽  
Author(s):  
A. Strelkov ◽  
P. Bykova ◽  
M. Gridneva ◽  
E. Dvorianinova
Keyword(s):  
Bulk Density ◽  
Mineral Composition ◽  
Flow Rate ◽  
Distribution System ◽  
Raw Materials ◽  
Water Flow Rate ◽  
Physicomechanical Properties ◽  
Raw Material ◽  
Oxide Concentration ◽  
Pass Through

Приведены результаты исследования физико-механических свойств фильтрующих материалов дробленого керамзита объемной насыпной массой 525 и 555 кг/м3 и Диамикс АКВА объемной насыпной массой 670 кг/м3. Сырьем для производства керамзита служат легковспучивающие глины определенного химического и минерального состава, для Диамикс АКВА материал на основе природного диатомита, в состав которого входят экзоскелеты диатомовых водорослей. Содержание оксидов в Диамикс АКВА : SiO2 не менее 83, Al2O3 не более 6 и Fe2O3 не более 3,5. На фильтрующий материал Диамикс АКВА имеется свидетельство о государственной регистрации. Результаты исследований показали, что новый фильтрующий материал на основе Диамикс АКВА может быть использован для загрузки вновь строящихся фильтровальных сооружений. Для регенерации фильтрующей загрузки необходима повышенная интенсивность промывки, что требует проверки пропускной способности дренажно-распределительной системы фильтров для пропуска повышенного расхода воды.The results of the study of physicomechanical properties of filtering materials crushed expanded clay with a bulk density of 525 and 555 kg/m3 and Diamix AQUA with a bulk density of 670 kg/m3 are presented. Easy upheaving clays of a certain chemical and mineral composition serve as raw materials for expanded clay production, for Diamix AQUA production raw material based on natural diatomite that includes exoskeletons of diatoms is used. Oxide concentration in Diamix AQUA is: SiO2 more than 83, Al2O3 less than 6 and Fe2O3 less than 3.5. Diamix AQUA filtering material has a National Registration Certificate. The research results showed that the new filtering material based on Diamix AQUA can be used as media for newly constructed filtration facilities. To regenerate the filter media, an increased backwashing rate is needed, which requires checking the throughput of the filter drainage and distribution system to pass through the increased water flow rate.

RHEOLOGICAL PROPERTIES OF CERAMIC MASSES: IMPROVEMENT BY COMPLEX MATERIAL ACTIVATION

2019 ◽  
Vol 16 (3) ◽  
pp. 334-351
Author(s):  
A. S. Mavlyanov ◽  
E. K. Sardarbekova
Keyword(s):  
Rheological Properties ◽  
Raw Materials ◽  
Sensitivity Coefficient ◽  
Raw Material ◽  
Clay Material ◽  
Fibrous Materials ◽  
Chemical Production ◽  
Production Wastes ◽  
Pass Through ◽  
The Masses

Introduction. The objective of the research is to study the effect of the complex activation of the alumina raw material on the rheological properties of the ceramic mass. In addition, the authors investigate solutions for the application of optimal coagulation structures based on loams and ash together with plastic certificates.Materials and methods. The authors used the local forest like reserves of clay loams at the BashKarasu, ash fields of the Bishkek Central Heating Centre (BTEC) and plasticizer (sodium naphthenate obtained from alkaline chemical production wastes) as fibrous materials. Moreover, the authors defined technological properties of raw materials within standard laboratory methodology in accordance with current GOSTs.Results. The researchers tested plastic durability on variously prepared masses for the choice of optimal structures. The paper demonstrated the plastic durability of complexly activated compounds comparing with non-activated and mechanically activated compounds. The sensitivity coefficient increased the amount of clay loams by mechanically and complexly activated, which predetermined the possibility of intensifying the process of drying samples based on complexly activated masses.Discussion and conclusions. However, mechanical activation of clay material reduces the period of relaxation and increases the elasticity coefficient of ceramic masses by 1.8–3.4 times, meanwhile decreases elasticity, viscosity and the conventional power during molding, which generally worsens the molding properties of the masses. Сomplex activation of ash-clay material decreases the period of relaxation and provides an increase in elasticity, plasticity of ceramic masses by 46–47%, reduction in viscosity by 1.5–2 times, conventional power on molding by 37–122% in comparison with MA clay loams. Ceramic masses based on spacecraft alumina raw materials belong to the SMT with improved rheological properties; products based on them pass through the mouthpiece for 5–7 seconds.

scholarly journals TLS and SfM Approach for Bulk Density Determination of Excavated Heterogeneous Raw Materials

Minerals ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 174 ◽  
Author(s):  
Peter Blistan ◽  
Stanislav Jacko ◽  
Ľudovít Kovanič ◽  
Julián Kondela ◽  
Katarína Pukanská ◽  
...  
Keyword(s):  
Bulk Density ◽  
Laser Scanning ◽  
Large Scale ◽  
Raw Materials ◽  
Terrestrial Laser Scanning ◽  
Mineral Resources ◽  
Point Clouds ◽  
Raw Material

A frequently recurring problem in the extraction of mineral resources (especially heterogeneous mineral resources) is the rapid operative determination of the extracted quantity of raw material in a surface quarry. This paper deals with testing and analyzing the possibility of using unconventional methods such as digital close-range photogrammetry and terrestrial laser scanning in the process of determining the bulk density of raw material under in situ conditions. A model example of a heterogeneous deposit is the perlite deposit Lehôtka pod Brehmi (Slovakia). Classical laboratory methods for determining bulk density were used to verify the results of the in situ method of bulk density determination. Two large-scale samples (probes) with an approximate volume of 7 m3 and 9 m3 were realized in situ. 6 point samples (LITH) were taken for laboratory determination. By terrestrial laser scanning (TLS) measurement from 2 scanning stations, point clouds with approximately 163,000/143,000 points were obtained for each probe. For Structure-from-Motion (SfM) photogrammetry, 49/55 images were acquired for both probes, with final point clouds containing approximately 155,000/141,000 points. Subsequently, the bulk densities of the bulk samples were determined by the calculation from in situ measurements by TLS and SfM photogrammetry. Comparison of results of the field in situ measurements (1841 kg∙m−3) and laboratory measurements (1756 kg∙m−3) showed only a 4.5% difference in results between the two methods for determining the density of heterogeneous raw materials, confirming the accuracy of the used in situ methods. For the determination of the loosening coefficient, the material from both large-scale samples was transferred on a horizontal surface. Their volumes were determined by TLS. The loosening coefficient for the raw material of 1.38 was calculated from the resulting values.

Study Formation Process of Cement Clinker Minerals by Using Calcium Carbide Slag as Raw Material

2013 ◽  
Vol 389 ◽  
pp. 341-345 ◽  
Author(s):  
Ya Li Wang ◽  
Shi Jie Dong ◽  
Lin Lin Liu ◽  
Su Ping Cui ◽  
Hai Bo Xu
Keyword(s):  
Mineral Composition ◽  
Formation Process ◽  
Phase Structure ◽  
Raw Materials ◽  
Calcium Carbide ◽  
Industrial Wastes ◽  
Raw Material ◽  
Cement Clinker ◽  
Mineral Phase ◽  
Carbide Slag

Calcium carbide Slag is one kind of industrial wastes from CaC2 hydrolysis reaction that will cause land pollution. In the research, calcium carbide Slag used as a substitute for limestone to produce cement clinker, which with a high portion of CaO content and then an excellent calcium containing raw material. As a kind of industrial wastes, the properties of Calcium carbide slag differentiate from that of natural limestone. The formation process of clinker minerals was studied by means of XRD. The results indicated that clinker minerals formation is similar to that from use of limestone. The generated clinker has a rational mineral composition and well developed mineral phase structure. But, there are many differences in decomposition temperatures between the calcium containing raw materials. Therefore, the carbide slag can be used as a substitute of limestone raw material to produce cement clinker.

scholarly journals Evaluation of Kalalani vermiculite for production of high strength porcelain insulators

2019 ◽  
Vol 51 (2) ◽  
pp. 223-232 ◽  
Author(s):  
Blasius Ngayakamo ◽  
Eugene Park
Keyword(s):  
Water Absorption ◽  
Bulk Density ◽  
Bending Strength ◽  
Raw Materials ◽  
High Strength ◽  
Microstructural Characterization ◽  
Dielectric Strength ◽  
Raw Material ◽  
Porcelain Insulators

The present work has evaluated Kalalani vermiculite as a potential raw material for the production of high strength porcelain insulators. Three porcelain compositions were prepared to contain 0, 20 and 30 wt% of Kalalani vermiculite. Porcelain samples were fabricated using a semi-drying method. The chemical, mineralogical phases and microstructural characterization of the raw materials were carried out using XRF, XRD, and SEM techniques, respectively. Water absorption, bulk density, dielectric and bending strengths were performed on porcelain samples fired up to 1300?C. However, at the sintering temperature of 1250?C, the porcelain sample with 20 wt% of Kalalani vermiculite gave the dielectric strength of 61.3 kV/mm, bending strength of 30.54 MPa, bulk density of 2.21 g/cm3 and low water absorption value of 0.21 % which is the prerequisite properties for high strength porcelain insulators. It was therefore concluded that Kalalani vermiculite has the potential to be used for the production of high strength porcelain insulators

scholarly journals Modelling the Influence of Manufacturing Process Variables on Dimensional Changes of Porcelain Tiles

2013 ◽  
Vol 2013 ◽  
pp. 1-12 ◽  
Author(s):  
Dolly Santos-Barbosa ◽  
Dachamir Hotza ◽  
Juan Boix ◽  
Gustavo Mallol
Keyword(s):  
Bulk Density ◽  
Raw Materials ◽  
Compaction Pressure ◽  
Raw Material ◽  
Main Process ◽  
Process Variables ◽  
Final Size ◽  
Dimensional Changes ◽  
Four Levels ◽  
Porcelain Tiles

A model to study the influence of main process variables (powder moisture, maximum compaction pressure, and maximum firing temperature) on the intermediate variables (mass, dry bulk density, size, and thickness) and the final dimensions of porcelain tiles is proposed. The properties of dried and fired bodies are basically determined by the process parameters when the physical, chemical, and mineralogical characteristics of the raw material are kept constant. For a given set of conditions, an equation could be sought for each property as a function of raw materials and processing. In order to find the relationship between moisture content and compaction pressure with dry bulk density, springback, and drying and firing shrinkage, a laboratory experimental design with three factors and four levels was applied. The methodology was validated in lab scale for a porcelain tile. The final size and thickness were estimated, and the influence of the main process variables was analysed.

Preparation and Mechanism of Cordierite by Using Calcined Bauxite as Raw Material at Relatively Low Temperature

2013 ◽  
Vol 785-786 ◽  
pp. 1066-1071
Author(s):  
Jian Feng Wu ◽  
Bin Zheng Fang ◽  
Xiao Hong Xu ◽  
Xin Bin Lao
Keyword(s):  
Low Temperature ◽  
Bulk Density ◽  
Bending Strength ◽  
Raw Materials ◽  
Xrd Analysis ◽  
Raw Material ◽  
Synthetic Process ◽  
Synthetic Temperature ◽  
Sintering Method

The cordierite was synthesized at relatively low temperature by pressureless sintering method, using calcined bauxite, talcum , quartz and feldspar as raw materials in this paper. The water absorption (Wa), porosity (Pa), bulk density (Db) and bending strength of samples have been tested, and the synthetic process and mechanism have been investigated by XRD, SEM, and so on. The results showed that the cordierite could be synthesized at 1280°C and the range of synthetic temperature is 1160~1300°C, when the sample was sintered at 1280°C for 2h, its bulk density and bending strength were 2.20g/cm3and 72.13MPa, respectively. XRD analysis showed that the main phase of sample was cordierite, the cordierite content was about 88wt%, and the minor phases were MgAl2O4spinel and corundum. SEM results showed that the samples were dense and the pore sizes were 5 μm~100μm, the grains were growth and development well, the grains size were 0.5μm~6μm. High reaction activity corundum and mullite were provided by calcined bauxite, then coupled with the role of feldspar, thus reduced the synthetic temperature of cordierite.

scholarly journals LIGHTWEIGHT AGGREGATE AND ASHES SLAG BASED CONCRETE WITH HIGH RESIDUAL FUEL CONTENT

2020 ◽  
Vol 17 (34) ◽  
pp. 678-688
Author(s):  
Maratbek T ZHUGINISSOV ◽  
Zhanar O ZHUMADILOVA
Keyword(s):  
Compressive Strength ◽  
Bulk Density ◽  
Lightweight Concrete ◽  
Raw Materials ◽  
Lightweight Aggregate ◽  
Mineralogical Composition ◽  
Raw Material ◽  
Unburned Fuel ◽  
Surrounding Areas ◽  
Slag Waste

Ashes slag materials in the chemical and mineralogical composition are largely identical to natural mineral raw materials. They are a source of environmental pollution, pose a threat to public health, and a threat to the flora and fauna of the surrounding areas. Ashes slag waste contains a large amount of unburned fuel. In some ashes, the content of unburned fuel can reach 20-40%. In this case, it is advisable to use it as a raw material for the production of artificial porous aggregates. The paper presents the results of studies on the development of lightweight aggregate technology based on ashes slag with a high residual fuel content. To develop the technology of lightweight aggregate, ashes slag was used by Nova Zinc LLP (Karaganda region, Kazakhstan), in which the content of unburned coal is up to 75%. Based on ashes slag, lightweight aggregates were obtained using burning and non-burning technologies. By roasting (burning) technology, aggregates were obtained by burning at a temperature of 1000 and 1100 °C. The aggregates obtained have a bulk density of 395-687 kg/m3 and a compressive strength in the cylinder of 0.5-2.4 MPa. By non-burning technology Portland cement M400 was used as an astringent. After hardening, the aggregates have a bulk density of 400-600 kg/m3 and a 679 compressive strength of 0.65-1.5 MPa in the cylinder. Samples of light concrete with a density of 1200 and 1700 kg/m3, a compressive strength of 80 (B5) and 120 kg/cm2 (B7.5), and thermal conductivity coefficients of 0.43 and 0.67 W/mоС were obtained on the basis of the non-fired light aggregate, respectively. Lightweight aggregate and lightweight concrete in their functional properties meet the requirements of regulatory documents.

scholarly journals Olive Stone Ash as Secondary Raw Material for Fired Clay Bricks

2016 ◽  
Vol 2016 ◽  
pp. 1-9 ◽  
Author(s):  
D. Eliche-Quesada ◽  
M. A. Felipe-Sesé ◽  
A. Infantes-Molina
Keyword(s):  
Compressive Strength ◽  
Water Absorption ◽  
Bulk Density ◽  
Raw Materials ◽  
Linear Shrinkage ◽  
Raw Material ◽  
Engineering Properties ◽  
Clay Bricks ◽  
Olive Stone ◽  
Secondary Raw Material

This work evaluates the effect of incorporation of olive stone ash, as secondary raw material, on the properties of fired clay bricks. To this end, three compositions containing 10, 20, and 30 wt% olive stone ash in a mixture of clays (30 wt% red, 30 wt% yellow, and 40 wt% black clay) from Spain were prepared. The raw materials, clay and olive stone ash, were characterized by means of XRD, XRF, SEM-EDS, and TG-TDA analysis. The engineering properties of the press molded specimens fired at 900°C (4 h) such as linear shrinkage, bulk density, apparent porosity, water absorption, and compressive strength were evaluated. The results indicated that the incorporation of 10 wt% of olive stone ash produced bricks with suitable technological properties, with values of compressive strength of 41.9 MPa but with a reduced bulk density, by almost 4%. By contrast, the incorporation of 20 wt% and 30 wt% sharply increased the water absorption as a consequence of the large amount of open porosity and low mechanical strength presented by these formulations, which do not meet the standards for their use as face bricks. The bricks do not present environmental problems according to the leaching test.

scholarly journals Characteristics of Kaolinitic Raw Materials from the Lokoundje River (Kribi, Cameroon) for Ceramic Applications

2021 ◽  
Vol 11 (13) ◽  
pp. 6118
Author(s):  
Paul-Désiré Ndjigui ◽  
Jean Aimé Mbey ◽  
Soureiyatou Fadil-Djenabou ◽  
Vincent Laurent Onana ◽  
Elie Constantin Bayiga ◽  
...  
Keyword(s):  
Flexural Strength ◽  
Water Absorption ◽  
Bulk Density ◽  
Mineral Assemblage ◽  
Raw Materials ◽  
Thermal Characteristics ◽  
Linear Shrinkage ◽  
Physicomechanical Properties ◽  
Geochemical Data ◽  
Physical Chemical

Eight kaolinitic materials from the Lokoundje River at Kribi were sampled and investigated for their physical, chemical, mineralogical and thermal characteristics in order to evaluate their potential suitability as raw materials in ceramics. The Lokoundje kaolinitic materials are clayey to silty clayey and are predominantly composed of kaolinite and quartz. The alkali (Na2O + K2O) content ranges between 1 and 2.5 wt.%; these low values do not favor vitrification of the ceramics but may be improved through flux amendment. The presence of goethite in some samples limits their utilization in white ceramics. The minerals content, color, metallic sound, cohesion, linear shrinkage, flexural strength, bulk density, water absorption and microstructure were determined. The XRD data reveal that kaolinite and goethite were transformed, respectively, into mullite and hematite. The colors of the fired products are characteristic of their mineral assemblage. The metallic sound is indicative of low vitrification which is confirmed by the presence of cracks due to low flux contents. The cohesion is good to very good, due to the abundance of kaolinite. The physicomechanical properties increase with temperature as well as densification. The geochemical data show that the Lokoundje alluvial clays are suitable for the manufacture of white stoneware tiles.

Liquid Chromatographic Methods for Fluoxetine Hydrochloride, Its meta Isomer, and Related Compounds in Raw Materials

1995 ◽  
Vol 78 (2) ◽  
pp. 334-338 ◽  
Author(s):  
Pauline M Lacrok ◽  
Patrick N Yat ◽  
Edward G Lovering
Keyword(s):  
Flow Rate ◽  
Mobile Phase ◽  
Raw Materials ◽  
Raw Material ◽  
Fluoxetine Hydrochloride ◽  
Assay Precision ◽  
Liquid Chromatographic ◽  
Related Compounds ◽  
Meta Isomer

Abstract Liquid chromatographic (LC) methods were developed for assay of fluoxetine hydrochloride, its meta isomer, and 12 related compounds in drug raw materials. The method for assay and determination of the meta isomer requires an Exsil ODS-B column; a mobile phase consisting of tetrahydrofuran, acetonitrile, and buffer; a flow rate of 1 mL/min; and detection at 214 nm. The method for related compounds specifies a Spherisorb nitrile column; a mobile phase consisting of tetrahydrofuran, acetonitrile, and buffer; a flow rate of 1 mL/min; and detection at 214 nm. The limits of quantitation in the presence of the drug are 0.1% for the meta isomer and 0.05% or less for the related compounds. Assay precision was less than 1.0% on triplicate weighings. Drug contents of 4 raw material samples were between 98.8 and 100.1%. Impurity levels in the 4 samples ranged from 0.14 to 0.45%. In addition, one sample contained ca 0.13% of the meta isomer. A second analyst, using columns from different suppliers, obtained similar results.

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