scholarly journals CHARACTERISTIC FEATURES OF THE OIL-HEAT TREATED WOODS FROM TROPICAL FAST GROWING WOOD SPECIES

Wood Research ◽  
2021 ◽  
Vol 66 (3) ◽  
pp. 365-378
Author(s):  
Intan Fajar Suri ◽  
Byantara Darsan Purusatama ◽  
Seung Hwan Lee ◽  
Nam Hun Kim ◽  
Wahyu Hidayat ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Wood Species ◽  
Untreated Wood ◽  
Tangential Direction ◽  
Melia Azedarach ◽  
Wall Area ◽  
Fast Growing ◽  
Fiber Wall ◽  
Heat Treated ◽  
Increasing Temperature

This study aimed to evaluate the effect of oil-heat treatment on the anatomical, physical, and chemical properties of the tropical fast-growing wood species as gmelina (Gmelinaarborea) and mindi (Melia azedarach) wood. Vessel lumen area and diameter in radial and tangential direction of both species increased with increasing temperature. The fiber lumen areas in both woods were remarkably decreased by oil-heat treatment, and the fiber wall area increased considerably with increasing temperature. Both woods tended to gain weight after heat treatment at 180°C and 200°C, and then lose weight after heat treatment at 220°C. The density of mindi increased greatly at 180°C and 200°C and slightly decreased at 220°C. The dimension of the specimens in tangential direction increased with heat treatment, but the rate decreased with increasing temperature. The relative crystallinity and crystallite width of the heat-treated woods were greater than those of the untreated wood. In the Fourier transform infrared analyses, the peaks from the carbohydrates were changed after oil-heat treatment, mainly due to the degradation of hemicellulose. Consequently, it was revealed that the heat treatment affected various properties of gmelina and mindi woods. Differing characteristics between the species were also noted.

scholarly journals COLOR CHANGE — MASS LOSS CORRELATION FOR HEAT-TREATED WOOD

2014 ◽  
Vol 2 ◽  
pp. 345-352 ◽  
Author(s):  
Cristina Marinela Olarescu ◽  
Mihaela Campean
Keyword(s):  
Heat Treatment ◽  
Mass Loss ◽  
Color Change ◽  
Treated Wood ◽  
Untreated Wood ◽  
Cost Effective ◽  
Assessment Procedure ◽  
Mathematical Correlation ◽  
Heat Treated ◽  
Two Parameters

Heat treatment is renowned as the most environmentally friendly process of dimensional stabilization that can be applied to wood, in order to make it suitable for outdoor uses. It also darkens wood color and improves wood durability. The intensity of heat treatment can be appreciated by means of two parameters: the color change occured in wood due to the high temperature, and the mass loss, which is a measure of the degree of thermal degradation. In order to find a mathematical correlation between these two parameters, an experimental study was conducted with four European wood species, which were heat-treated at 180°C and 200ºC, for 1-3 hours, under atmosheric pressure.The paper presents the results concerning the color changes and mass losses recorded for the heat-treated wood samples compared to untreated wood.  For all four species, the dependency between the color change and the mass loss was found to be best described by a logarithmic regression equation with R2 of 0.93 to 0.99 for the soft species (spruce, pine and lime), and R2 of 0.77 for beech. The results of this study envisage to simplify the assessment procedure of the heat treatment efficiency, by only measuring the color – a feature that is both convenient and cost-effective. 

scholarly journals Calorific Power Improvement of Wood by Heat Treatment and Its Relation to Chemical Composition

Energies ◽  
2020 ◽  
Vol 13 (20) ◽  
pp. 5322
Author(s):  
Idalina Domingos ◽  
Umit Ayata ◽  
José Ferreira ◽  
Luisa Cruz-Lopes ◽  
Ali Sen ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Chemical Composition ◽  
Lignin Content ◽  
Treated Wood ◽  
Untreated Wood ◽  
High Heating Value ◽  
Heat Treated ◽  
Positive Linear Correlation ◽  
Total Extractives ◽  
Calorific Power

Chemical composition influences the calorific power of wood, mainly due to the calorific power of structural compounds and extractives. Heat treatment changes the chemical composition of treated wood. This work studies the relationship between chemical composition and calorific power improvement by heat treatment. Samples were heat-treated by the ThermoWood process ® for 1 h and 2 h. High heating value (HHV) and chemical composition; lignin, cellulose, hemicelluloses and extractives in dichloromethane, ethanol, and water were determined. The HHV of untreated wood ranged between 18.54–19.92 MJ/kg and increased with heat treatment for all the tested species. A positive linear correlation was found between HHV and Klason lignin (R2 = 0.60). A negative trend was observed for holocellulose, cellulose, and hemicelluloses content against HHV, but with low determination coefficients for linear regression. The best adjust for polysaccharides was found for hemicelluloses content. A positive correlation could be found for dichloromethane extractives (R2 = 0.04). The same was obtained in relation to ethanol extractives with R2 = 0.20. For water and total extractives, no clear positive or negative trends could be achieved. The results showed that the HHV of wood increased with heat treatment and that this increase was mainly due to the increase in lignin content.

scholarly journals Heat-Treated Wood as a Substrate for Coatings, Weathering of Heat-Treated Wood, and Coating Performance on Heat-Treated Wood

2019 ◽  
Vol 2019 ◽  
pp. 1-9 ◽  
Author(s):  
Vlatka Jirouš-Rajković ◽  
Josip Miklečić
Keyword(s):  
Heat Treatment ◽  
Wood Species ◽  
Treated Wood ◽  
Wood Properties ◽  
Treatment Method ◽  
Coating Performance ◽  
Treatment Processes ◽  
Treatment Conditions ◽  
Heat Treated ◽  
Trade Names

Heat treatment is a method of wood modification with increasing market acceptance in Europe. The major patented European commercial heat treatment processes have trade names ThermoWood, Platowood, Retiwood, Le Bois Perdure, and Oil-Heat-Treated Wood (OHT). To what extent modification of wood affects the resistance of wood to weathering is also an important aspect for wood applications, especially where appearance is important. Unfortunately, heat-treated wood has poor resistance to weathering, and surface treatment with coatings is required for both protection and aesthetic reasons. As a substrate for coating, heat-treated wood has altered characteristics such as lower hygroscopicity and liquid water uptake and changed acidity, wettability, surface free energy, and anatomical microstructure. Various wood species, heat treatment method, treatment intensity, and treatment conditions exhibited a different extent of changes in wood properties. These altered properties could affect coating performance on heat-treated wood. The reported changes in acidity and in surface energy due to heat treatments are inconsistent with one another depending on wood species and temperature of the treatments. This paper gives an overview of the research results with regards to properties of heat-treated wood that can affect coating performance and weathering of uncoated and coated heat-treated wood.

Wettability of Heat-Treated Wood

Holzforschung ◽  
2003 ◽  
Vol 57 (3) ◽  
pp. 301-307 ◽  
Author(s):  
M. Pétrissans ◽  
P. Gérardin ◽  
I. El bakali ◽  
M. Serraj
Keyword(s):  
Heat Treatment ◽  
Water Drop ◽  
Chemical Change ◽  
Treated Wood ◽  
Untreated Wood ◽  
Adsorbed Water ◽  
Inert Atmosphere ◽  
Contact Angles ◽  
Heat Treated ◽  
Before And After

Summary The aim of this work was to study the wettability and chemical composition of heat-treated wood. Heat treatment was performed at 240°C under inert atmosphere on four European wood species (pine, spruce, beech and poplar). Contact angle measurements before and after treatment indicated a significant increase in wood hydrophobicity. Advancing contact angles of a water drop were in all cases systematically higher for heat-treated than for untreated wood. Chemical modifications of wood after heat treatment were investigated using FTIR and 13C NMR analysis. FTIR spectra indicated little structural change which could be attributed either to carbon-carbon double bond formation or to adsorbed water. NMR spectra also revealed little chemical change except for the degree of cellulose crystallinity which was considerably higher in heat-treated wood and could explain the higher contact angles.

High Purity Ti2AlC Powder Prepared by a Novel Method

2010 ◽  
Vol 658 ◽  
pp. 340-343 ◽  
Author(s):  
Jian Feng Zhu ◽  
Guo Quan Qi ◽  
Fen Wang ◽  
Hai Bo Yang
Keyword(s):  
Heat Treatment ◽  
Thermal Treatment ◽  
High Purity ◽  
High Energy ◽  
High Energy Milling ◽  
Heat Treated ◽  
Novel Method ◽  
Increasing Temperature ◽  
Milled Powders

Ti2AlC powders with high purity were successfully synthesized via high energy milling and heat treatment of Ti, C and Al powders. The effects of composition and thermal treatment on the formation and purity of Ti2AlC were examined in detail. The results shown a mechanically induced self-propagating reaction (MSR) was triggered to form Ti3AlC2, TiC and TiAlx during the high energy milling. When the as-milled powders were heat treated, Ti2AlC was initially formed by the reaction between TiAl and TiC. With continuously increasing temperature, Ti2AlC was also produced by the reaction between TiAl and Ti3AlC2.

scholarly journals Coating Performance on Exterior Oil-Heat Treated Wood

Coatings ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 225 ◽  
Author(s):  
Mojgan Nejad ◽  
Mahdi Dadbin ◽  
Paul Cooper
Keyword(s):  
Moisture Content ◽  
Wood Species ◽  
Color Change ◽  
Treated Wood ◽  
Untreated Wood ◽  
Average Moisture Content ◽  
Southern Pine ◽  
Coating Performance ◽  
Spruce Wood ◽  
Heat Treated

Thermal modification and the degree of improved properties from the treatment depend on wood species and treatment parameters. Southern yellow pine and spruce are two wood species commonly used for decking, fences, and siding in North America. This study evaluated coating performance when applied on oil-heat-treated Southern pine and spruce wood samples. Moisture content, color, and gloss changes of samples were analyzed before weathering and then after each month for the first three months and then every six months during 18 months of natural weathering exposure in Toronto, Canada. The results showed that coated heat-treated woods had lower moisture uptake, lower color change, and overall better appearance ranking than coated-untreated wood samples. Coated-spruce wood samples had lower checking and splitting, and in general, much better performance than coated-Southern pine treated samples. Notably, the average moisture content of treated spruce wood samples was significantly lower than that of Southern pine, which explains lower checking and improved coatings’ appearance.

scholarly journals Surface roughness and wettability of surface densified heat-treated Norway spruce (Picea abies L. Karst.)

2019 ◽  
Vol 70 (4) ◽  
pp. 377-382
Author(s):  
Nadir Ayrilmis ◽  
Mirko Kariz ◽  
Jin Heon Kwon ◽  
Manja Kitek Kuzman
Keyword(s):  
Heat Treatment ◽  
Surface Roughness ◽  
Picea Abies ◽  
Cold Water ◽  
Longitudinal Direction ◽  
Tangential Direction ◽  
Treatment Temperature ◽  
Densified Wood ◽  
Surface Densification ◽  
Heat Treated

Surface roughness and wettability of the heat-treated and then surface densified spruce (Picea abies L. Karst.) wood were measured to determine the effect of densification and heat-treatment on wood surface properties. The process of heat-treatment with an initial vacuum was performed in a vacuum chamber on oven dried lamellas with dimensions of 630 mm (longitudinal direction) x 45 mm (tangential direction) x 25 mm (radial direction). The lamellas were heat-treated at four different temperatures which were 170 °C, 190 °C, 210 °C and 230 °C. Control specimens were not exposed to heat-treatment. The lamellas were first heated to 100 °C, the creation of a vacuum taking 30 min at this temperature, and then heated to the desired temperature, and treated at this constant temperature for 3 h. The lamellas were then cooled down by using coils with cold water inside the chamber. Surface densification of lamellas with compression from 22 mm to 15 mm thickness was made by press platens heated at 150 °C and held in that position for 60 s. After the 1 min, the heated platen was cooled to 90 °C, whilst the specimen remained under compression to minimize immediate spring back. The total time of compression was 2 min (30 s closing, 60 s pressing and approx. 30 s cooling). In the treatment groups, the optimum treatment temperature on the one-side densified wood specimens was found to be 170 °C based on the surface roughness and wettability values. Surface densification significantly decreased the surface roughness of the wood specimens. The surface quality of wood can be improved when the wood is exposed to the heat-treatment and then surface densification.

Water absorption behavior of heat-treated and untreated red balau saw dust/LDPE composites: Its kinetics and effects on mechanical properties

2018 ◽  
Vol 32 (10) ◽  
pp. 1408-1426 ◽  
Author(s):  
Ruth A Lafia-Araga ◽  
Aziz Hassan ◽  
R Yahya ◽  
N Abd Rahman ◽  
Fauzani Md Salleh
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Water Absorption ◽  
Water Immersion ◽  
Treated Wood ◽  
Untreated Wood ◽  
Thermoplastic Composites ◽  
Wood Composites ◽  
Saw Dust ◽  
Heat Treated

The hygroscopic nature of wood limits the use of wood thermoplastic composites (WTC) in outdoor industrial and domestic applications. To reduce this tendency, red balau saw dust was heat treated at 180 and 200°C for 1 h and compounded with Low Density Poly(ethylene) (LDPE) into 20 and 37 wt% and then molded into test specimens by injection molding. Samples were immersed in distilled water at room temperature for 4 months. Heat-treated wood composites showed remarkable water resistance relative to untreated ones. Wood composites made from wood treated at 180 and 200°C exhibited almost similar water absorption pattern. Reduced water absorption of heat-treated wood composites relative to untreated ones indicates that heat treatment has resulted in a degree of modification of the wood. Most of the composites displayed the Fickian mode of water absorption with n values close to 0.5. Also, the diffusion coefficient reduced with wood content in untreated wood composites due to interaction of water with the polar groups in wood through hydrogen bonding. Untreated wood composites exhibited poorer mechanical properties with water immersion as a result of degradation due to moisture. The mechanical properties of the heat-treated wood composites were not adversely affected with water absorption. Therefore, heat treatment can reduce the proneness to water absorption in WTCs and alleviate the detrimental effects on mechanical properties.

scholarly journals Effect Of Heat-Treatment On Microstructure And Magnetic Properties Of Nanocrystallized Mn-Zn Ferrite Powders

2015 ◽  
Vol 60 (2) ◽  
pp. 1347-1350
Author(s):  
W.H. Lee ◽  
C.S. Hong ◽  
S.Y. Chang
Keyword(s):  
Heat Treatment ◽  
Magnetic Properties ◽  
Saturation Magnetization ◽  
High Energy ◽  
Treatment Temperature ◽  
Heat Treated ◽  
Zn Ferrite ◽  
Energy Ball ◽  
Size Of Particles ◽  
Increasing Temperature

Abstract The initial ferrite powders were subjected to high energy ball milling at 300rpm for 3h, and subsequently heat-treated at 573-1273K for 1h. Based on the observation of microstructure and measurement of magnetic properties, the heat-treatment effect was investigated. The size of initial powders was approximately 70μm. After milling, the powders with approximately 230nm in size were obtained, which were composed of the nano-sized particles of approximately 15nm in size. The milled powders became larger to approximately 550nm after heat-treatment at 973K. In addition, the size of particles increased to approximately 120nm with increasing temperature up to 973K. The coercivity of initial powders was almost unchanged after milling, whereas the saturation magnetization increased. As the heat-treatment temperature increased, the saturation magnetization gradually increased and the maximum coercivity was obtained at 773K.

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