Effects of Post Weld Ageing Heat Treatments on the Microstructure of 17-4PH GTA Welded Joints

2011 ◽  
Vol 264-265 ◽  
pp. 1300-1305 ◽  
Author(s):  
Seyed Ali Asghar Akbari Mousavi ◽  
S.A. Hoseini Hosein Abad

The mechanical and metallurgical properties of the 630 (17-4PH) precipitation hardening stainless steel is greatly influenced by the type of applied heat treatments cycles. In order to achieve the homogenous microstructure in the weld metal and eliminate the HAZ due to producing the weak mechanical strength, and producing similar microstructures and mechanical strength in both weld and base metal, the study was conducted to find an optimum pre and post heat treatments before and after welding. The 2.2mm thick and 48mm tube diameter made of 630 stainless steel were welded under various operational parameters. The samples were subjected to pre weld solution treatment and post weld aging heat treatment. To reveal the microstructures of the welds, the optical and scanning electron microscopy of the welds carried out. The study shows that the direct ageing treatment at 6200C after welding can give rise to the best heat treatment to produce, the uniformity in the grain size, mechanical strength and hardness, between the base metal and the weld metal.

Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 6157
Author(s):  
Matteo Vanzetti ◽  
Enrico Virgillito ◽  
Alberta Aversa ◽  
Diego Manfredi ◽  
Federica Bondioli ◽  
...  

Conventionally processed precipitation hardening aluminum alloys are generally treated with T6 heat treatments which are time-consuming and generally optimized for conventionally processed microstructures. Alternatively, parts produced by laser powder bed fusion (L-PBF) are characterized by unique microstructures made of very fine and metastable phases. These peculiar features require specifically optimized heat treatments. This work evaluates the effects of a short T6 heat treatment on L-PBF AlSi7Mg samples. The samples underwent a solution step of 15 min at 540 °C followed by water quenching and subsequently by an artificial aging at 170 °C for 2–8 h. The heat treated samples were characterized from a microstructural and mechanical point of view and compared with both as-built and direct aging (DA) treated samples. The results show that a 15 min solution treatment at 540 °C allows the dissolution of the very fine phases obtained during the L-PBF process; the subsequent heat treatment at 170 °C for 6 h makes it possible to obtain slightly lower tensile properties compared to those of the standard T6. With respect to the DA samples, higher elongation was achieved. These results show that this heat treatment can be of great benefit for the industry.


Author(s):  
Bojana Radojkovic ◽  
Bore Jegdic ◽  
Jovanka Kovacina ◽  
Sanja Stevanovic ◽  
Dunja Marunkic

The influence of the microstructure of the X5CrNi18-10 stainless steel welded joint on its resistance to general, pitting, and intergranular corrosion was analysed. The structure of weld metal, heat affected zone (HAZ) and base metal before and after electrochemical testing was analysed using SEM/EDS. The influence of the roughness level of the welded joint on its resistance to the mentioned types of corrosion was examined as well. Although the degree of sensitization of HAZ was significantly lower than the limit value, HAZ showed a noticeably greater tendency to general and pitting corrosion than weld metal and base metal. Polishing has been shown to significantly improve the corrosion resistance of HAZ than in the case of other parts of the welded joint.


Author(s):  
Mikihiro Sakata ◽  
Tomoaki Kiso ◽  
Masayuki Tanaka ◽  
Yasuhiro Sato

Duplex and super duplex stainless steels are susceptible to thermal aging embrittlement, referred to as 475°C (885°F) embrittlement. The object of this study is to understand the difference in susceptibility to 475°C (885°F) embrittlement of the base metal and the weld metal of these steels. Isothermal aging heat treatment at 300–450 °C (570–840°F) up to 1,000 hours was performed on 22% Cr duplex stainless steel: UNS S32205 and 25% Cr super duplex stainless steel: UNS S32750 and S32760 and these weld metals made using their matching SMAW electrodes or GTAW rods. After heat treatment, the embrittlement behavior was evaluated by Charpy impact test and Vickers hardness test. The results revealed the time-temperature embrittlement curves of the weld metals were displaced to a significantly shorter period of time and extended to lower temperatures compared to those of the corresponding base metals. More importantly, these results suggested that the maximum design temperature limit on these steels currently specified in the ASME Pressure Piping Codes and Boiler and Pressure Vessel Code is not always sufficient to avoid the risk of 475°C (885°F) embrittlement in their welded components.


2021 ◽  
Vol 42 ◽  
pp. 57-62
Author(s):  
Maria Stoicănescu

The 1.4301 stainless steel is part of the category of austenitic stainless steels, steels which do no undergo heat treatments in general, as they are intended for hot plastic deformation in particular. The aim of the research presented in this paper was to obtain significantly improved characteristics of the resistance properties in relation to the values obtained under classical conditions, by applying heat treatments. Samples taken from the delivery state material underwent annealing, quenching and ageing heat treatments. Subsequently, the samples thus treated were subjected to tests enabling the determination of the correlations between the heat treatment parameters, the structure and the properties.


2013 ◽  
pp. 271-324

Abstract This chapter discusses the processes used in manufacturing to thermally alter the properties of metals and alloys. It begins with a review of the iron-carbon system, the factors that affect hardenability, and the use of continuous cooling transformation diagrams. It then explains how various steels respond to heat treatments, such as annealing, normalizing, spheroidizing, tempering, and direct and interrupted quenching, and surface-hardening processes, such as flame and induction hardening, carburizing, nitriding, and carbonitriding. It also addresses the issue of temper embrittlement and discusses the effect of precipitation hardening on aluminum and other alloys.


2021 ◽  
pp. 307-325
Author(s):  
Jon L. Dossett

Abstract This article introduces some of the general sources of heat treating problems with particular emphasis on problems caused by the actual heat treating process and the significant thermal and transformation stresses within a heat treated part. It addresses the design and material factors that cause a part to fail during heat treatment. The article discusses the problems associated with heating and furnaces, quenching media, quenching stresses, hardenability, tempering, carburizing, carbonitriding, and nitriding as well as potential stainless steel problems and problems associated with nonferrous heat treatments. The processes involved in cold working of certain ferrous and nonferrous alloys are also covered.


2019 ◽  
Vol 24 ◽  
pp. 541-558 ◽  
Author(s):  
Jacopo De Nisi ◽  
Fabio Pozzi ◽  
Paolo Folgarait ◽  
Gabriele Ceselin ◽  
Mirco Ronci

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 581
Author(s):  
Ioan Milosan ◽  
Monica Florescu ◽  
Daniel Cristea ◽  
Ionelia Voiculescu ◽  
Mihai Alin Pop ◽  
...  

The appropriate selection of implant materials is very important for the long-term success of the implants. A modified composition of AISI 316 stainless steel was treated using solar energy in a vertical axis solar furnace and it was subjected to a hyper-hardening treatment at a 1050 °C austenitizing temperature with a rapid cooling in cold water followed by three variants of tempering (150, 250, and 350 °C). After the heat treatment, the samples were analyzed in terms of hardness, microstructure (performed by scanning electron microscopy), and corrosion resistance. The electrochemical measurements were performed by potentiodynamic and electrochemical impedance spectroscopy in liquids that simulate biological fluids (NaCl 0.9% and Ringer’s solution). Different corrosion behaviors according to the heat treatment type have been observed and a passivation layer has formed on some of the heat-treated samples. The samples, heat-treated by immersion quenching, exhibit a significantly improved pitting corrosion resistance. The subsequent heat treatments, like tempering at 350 °C after quenching, also promote low corrosion rates. The heat treatments performed using solar energy applied on stainless steel can lead to good corrosion behavior and can be recommended as unconventional thermal processing of biocompatible materials.


2019 ◽  
Vol 22 ◽  
pp. 118-139
Author(s):  
Faisal Aldhabib ◽  
Xiao Dong Sun ◽  
Abdullah Alsumait ◽  
Fahad Alzubi ◽  
Elias Ashe ◽  
...  

15-5PH stainless steel is widely used in the aerospace industry, from precision fuse pins to forged products, due to its various high-performance properties. However, there is little systematic evaluation of heat treatment responses, especially at ultra-high temperatures above 650°C (1200°F). The objective of this work was to evaluate the mechanical and microstructural properties of 15-5 PH stainless steel at various heat treatments. Multiple heat treatment parameters were tested. The samples tested had varied chemical compositions because they were from different vendors. The experimental work included multiple aging temperatures, time, heating rates, and the effects of multiple aging treatments. A total of 38 different heat treatments were conducted on these specimens. There was a linear correlation between hardness and ultimate and yield strength. Optical microscopy showed martensitic structures with very fine grains in all the tested samples. Scanning Electron Microscope (SEM) images showed ductile fracture in all the samples.


2012 ◽  
Vol 134 (2) ◽  
Author(s):  
Cédric Chauvy ◽  
Lionel Coudreuse ◽  
Patrick Toussaint

During fabrication of Pressure Vessels, steels undergo several heat treatments that aim to confer the required properties on the entire equipment, including welds and base metal. Indeed, the production heat treatment of the base material, which leads to achieve the target properties, is most of the time followed by post weld heat treatment (PWHT). The aim of such treatments is to insure a good behavior of the welded zones in terms of residual stresses and obviously properties such as toughness. Generally, many simulated PWHT (up to 4 or more) are required for the testing of the base material, which can affect its properties and even lead to unacceptable results. In some cases for fabrication purposes an intermediate Stress relieving treatment can be required. Special attention is paid on C-Mn steels (e.g., SA/A516 from ASME BPV Code) with the effect of thickness and Ceq (International Institute of Welding Carbon equivalent formula: see page 3) requirements on the final compromise between properties and heat treatments. In particular, toughness and ultimate tensile strength (UTS) are the critical parameters that will limit the acceptance of too high PWHT. Although micro-alloying is a mean to increase the resistance to PWHT, this leads to difficulties in softening the heat affected zones. This solution is therefore not the best one considering the whole equipment optimization. Finally, the manufacturing process can play a major role when specifications are stringent. Quenching and tempering (Q&T) can indeed provide better flexibility in terms of PWHT and improved toughness for given Ceq and thickness. The case of Cr-Mo(-V) steels, which are widely used in the energy industry, is also addressed. Indeed, PWHT requirements for increasing the toughness in the weld metal can lead to decrease the base metal properties below the specification limits. For example, the case of SA/A387gr11 is very typical of metallurgical changes that can occur during these high PWHT leading to a degradation of toughness in the base metal. Another focus is made on the Vanadium Cr-Mo grade SA/A542D that must withstand very high PWHT (705 °C and even 710 °C) because of welds toughness issues. Optimization has therefore to be done to increase the resistance to softening and to guarantee acceptable microstructure, especially in the case of thick wall vessels. Some ways for improvement are proposed on the basis of the equivalent Larson–Miller parameter (LMP) tempering parameter concept. The basic philosophy is to fulfil the need for discussion between companies involved in pressure vessels fabrication so that the best compromise can be found to ensure the best and safest behavior of the equipment as a whole. In particular, the tempering operation can sometimes be done at lower temperature than PWHT in order to offer the best properties to the final vessel.


Sign in / Sign up

Export Citation Format

Share Document