The Research on Preparation and Application of a Silicon-Based Efficient Coagulant

2011 ◽  
Vol 295-297 ◽  
pp. 543-546
Author(s):  
Jiao Jiao Wang ◽  
Chun Ying Han ◽  
Li Dan Zhang
Keyword(s):  
Industrial Wastewater ◽  
Experimental Results ◽  
Good Stability ◽  
Molar Ratio ◽  
Good Effect ◽  
Activation Time ◽  
Preparation Conditions ◽  
Silicon Based

In this paper, research was focused on the synthesis of a new efficient coagulant, boron -containing poly-silicate zinc (PSZB).The effect of the SiO2 concentration, Zn/Si molar ratio, B/Si molar ratio, activation time on flocculation properties were examined in detail. And the optimal preparation conditions were determined. At the same time, the industrial wastewater and life wastewater were treated for the properties test. The experimental results showed that the flocculant had good stability and good effect. It is a kind of good performance of flocculants.

scholarly journals Preparation of fly ash-based flocculant and flocculation performance

2021 ◽  
Vol 2079 (1) ◽  
pp. 012006
Author(s):  
Junxin Zhang ◽  
Xiumei Duan
Keyword(s):  
Fly Ash ◽  
Sodium Carbonate ◽  
Thermal Power ◽  
Liquid Product ◽  
Acid Leaching ◽  
Raw Material ◽  
Molar Ratio ◽  
Activation Time ◽  
Activation Temperature ◽  
Preparation Conditions

Abstract Using fly ash from a thermal power plant in Yingkou City as raw material, The inorganic polymer flocculant polyaluminum ferric chloride (PAFC) was prepared by sodium carbonate impregnation, high temperature roasting activation, and acid leaching. The influence of activation temperature and activation time on the leaching of aluminum and iron was investigated through single factor test and orthogonal test. The PAFC preparation conditions were optimized, and the prepared PAFC flocculant product was applied to kaolin turbidity water. The test results showed that the content of aluminum in fly ash was 7.08%, and the content of iron was 4.95%. The mass ratio of the activator sodium carbonate and fly ash was 10:7, the activation temperature was 800°C, and the activation time was 2h. The leaching rates of aluminum and iron were the highest, 88.31% and 53.66% respectively. The optimal conditions for the preparation of the flocculant were as follows: the molar ratio of aluminum to iron was 5.7:1, and the reaction time was 1.5h. The liquid product obtained under these conditions was yellowish brown, and the solid product obtained after being dried was yellow powder.

Catalytic Application of H4SiW12O40/TiO2-SiO2 in Synthesis of Acetals and Ketals

2014 ◽  
Vol 692 ◽  
pp. 320-325
Author(s):  
Fang Peng ◽  
Yu Lin Xu ◽  
Shi Yin Xiang ◽  
Shui Jin Yang
Keyword(s):  
Calcination Temperature ◽  
Heteropoly Acid ◽  
Load Ratio ◽  
Acid Catalyst ◽  
Molar Ratio ◽  
Impregnation Method ◽  
Activation Time ◽  
Preparation Conditions ◽  
Catalytic Application

The environmental friendly catalyst, H4SiW12O40/TiO2-SiO2 was prepared by the impregnation method. The synthesis of cyclohexanone glycol ketal was as the probe reaction and investigated the different influences on the catalytic activity of H4SiW12O40/TiO2-SiO2 by the quality of the carrier TiO2-SiO2 ratio, load of heteropoly acid, catalyst preparation conditions of the activation time and the calcination temperature, etc. The results showed the best condition for the preparation of the catalyst is the mass ratio of TiO2 and SiO2 is 1: 5, the load ratio of H4SiW12O40 is 10 %, calcination temperature is 300 oC and the roasting time is 3.0 h. Under the condition of the molar ratio of aldehydes (ketones) and glycol (1,2-propanediol) is 1: 1.6, the mass percent of the catalyst is 1.4 %, and the reaction time of 70 min, the yields of eight kinds acetal (ketal) are 71.6 %~ 90.5 %.

Synthesis and Infrared Spectrum Characterization of Phenylalanine Chelated Calcium Complex

2011 ◽  
Vol 396-398 ◽  
pp. 1549-1553
Author(s):  
Yu Qi Wu ◽  
Lian Jin Weng ◽  
Yuan Yuan Han ◽  
Xin Yang ◽  
Di Geng
Keyword(s):  
Infrared Spectrum ◽  
Chelate Ring ◽  
Uniform Design ◽  
Water System ◽  
Experimental Result ◽  
Molar Ratio ◽  
Optimal Parameters ◽  
Single Factor ◽  
Preparation Conditions

The preparation conditions in the water system of phenylalanine chelated calcium complex have been evaluated though single-factor tests and optimized by uniform design. Then the optimal parameters were obtained as follows: reaction temperature is 40 °C, reaction time is 182 min, the molar ratio of phenylalanine to calcium is 4.3 and pH = 9.0. Under the best conditions, the experimental result gives chelating rate = 87.40% that is 17.12% lower than the prediction = 104.52%.The infrared spectrum characterization has confirmed the formation of phenylalanine-Ca2+ chelates and the existence of chelate ring.

Preparation and Adsorption Properties of Starch-g-Polyacrylamide/Montmorillonite Nanocomposites

2015 ◽  
Vol 1120-1121 ◽  
pp. 343-346
Author(s):  
Cai Ning Zhang ◽  
Xu Man Wang
Keyword(s):  
Aqueous Solution ◽  
Methylene Blue ◽  
Adsorption Capacity ◽  
Crosslinking Agent ◽  
Adsorption Properties ◽  
Experimental Results ◽  
Solution Polymerization ◽  
Preparation Conditions ◽  
Montmorillonite Nanocomposites

By means of solution polymerization, a series of cross-linked starch-g-polyacrylamide/ montmorillonite (St-g-PAM/MMT) nanocomposites were prepared and used to adsorb methylene blue (MB). The effects of different preparation conditions on the adsorption capacity of the nanocomposites were investigated. The experimental results demonstrated that the prepared St-g-PAM/MMT nanocomposites were effective adsorbents for removal of MB from aqueous solution. Furthermore, adsorption capacity increased with the MMT contents up to 14% and decreased as the MMT contents further increased. Adsorption capacity increased with the increasing of the ratio of starch to acrylamide, whereas adsorption capacity decreased with the increasing of crosslinking agent contents.

scholarly journals ADSORPTION OF FLUORIDE FROM INDUSTRIAL WASTEWATER IN FIXED BED COLUMN USING JAVA PLUM (SYZYGIUM CUMINI)

2016 ◽  
Vol 9 (9) ◽  
pp. 320 ◽  
Author(s):  
Tej Pratap Singh ◽  
Sanjay Ghosh ◽  
Majumder Cb
Keyword(s):  
Residence Time ◽  
Industrial Wastewater ◽  
Fluoride Concentration ◽  
Fixed Bed ◽  
Experimental Results ◽  
Fixed Bed Reactor ◽  
Thomas Model ◽  
Fixed Bed Column ◽  
Empty Bed Residence Time

ABSTRACTObjective: The quality of drinking water is important for public safety and quality of life. Thus, providing every person on earth safe drinking waterseems to be the biggest challenge in front of mankind. For this purpose, here we have investigated the fluoride removal capacity of java plum.Methods: In this study, removal of fluoride from industrial wastewater using fixed-bed reactor adsorption techniques by java plum seed (Syzygiumcumini) was investigated. Fixed-bed column experiments were carried out for different bed depths, influent fluoride concentrations, and various flowrates. The Thomas model and bed depth service time model were applied to the experimental results. Both model predictions verify the experimentaldata for all the process parameters studied, indicating that the models were suitable for java plum (S. cumini) seeds (Biosorbent) fix-bed columndesign.Results: The empty bed residence time (EBRT) model optimizes the EBRT, and the Thomas model showed that the adsorption capacity is stronglydependent on the flow rate, initial fluoride concentration, and bed depth and is greater under conditions of a lower concentration of fluoride, lowerflow rate, and higher bed depth.Conclusion: The experimental results were encouraging and indicate that java plum (S. cumini) seed is a feasible option to use as a biosorbent toremove fluoride in a fixed bed adsorption process.Keywords: Adsorption, Column experiment, Thomas model, Empty bed residence time, Java plum.

scholarly journals Relationship Among Preparation, Structure and Superconductivity in Ti-Ca-Ba-Cu-O Compounds

1993 ◽  
Vol 15 (3-4) ◽  
pp. 117-138
Author(s):  
I. Kirschner ◽  
S. Leppävuori ◽  
A. Uusimäki
Keyword(s):  
Single Phase ◽  
Substantial Effect ◽  
Experimental Results ◽  
Characteristic Parameters ◽  
Term Stability ◽  
Long Term Stability ◽  
Preparation Conditions ◽  
Superconducting Parameters

Analysis of a comprehensive set of experimental results has proven the substantial effect of the precise preparation conditions upon the structure and superconducting parameters of Ti-Ca-Ba-Cu-O samples. The techniques required for the preparation of specimens of single phase and long-term stability, together with methods for improvement of the characteristic parameters have been determined. Comparing results derived from samples prepared by different methods has allowed the quantitative differences of the characteristic parameters to be evaluated.

scholarly journals Aging aerosol in a well-mixed continuous-flow tank reactor: an introduction of the activation time distribution

2019 ◽  
Vol 12 (5) ◽  
pp. 2647-2663 ◽  
Author(s):  
Franz Friebel ◽  
Amewu A. Mensah
Keyword(s):  
Continuous Flow ◽  
Experimental Approach ◽  
Cloud Condensation Nuclei ◽  
Experimental Results ◽  
Mathematical Framework ◽  
Activation Time ◽  
Mean Values ◽  
Tank Reactor ◽  
Atmospheric Aging ◽  
Observation Times

Abstract. Two approaches are commonly used to simulate atmospheric aging processes in the laboratory. The experiments are either performed in large aerosol chambers (several m3) in order to achieve extended observation times or in small chambers (< 1 m3), compensating for the short observation times by elevated reactant concentrations. We present an experimental approach that enables long observation times at atmospherically relevant reactant concentrations in small chamber volumes by operating the aerosol chamber as a continuous-flow stirred tank reactor (CSTR). We developed a mathematical framework that allows the retrieval of data beyond calculating mean values, such as O3 exposure or equivalent atmospheric aging time, using the new metric, activation time (tact). This concept was developed and successfully tested to characterize the change in cloud condensation nuclei (CCN) activity of soot particles due to heterogeneous ozone oxidation. We found very good agreement between the experimental results and the theoretical predictions. This experimental approach and data analysis concept can be applied for the investigation of any transition in aerosol particles properties that can be considered a binary system. Furthermore, we show how tact can be applied to the analysis of data originating from other reactor types such as oxidation flow reactors (OFRs), which are widely used in atmospheric sciences. The new tact concept significantly supports the understanding of data acquired in OFRs, especially those from deviating experimental results in intercomparison campaigns.

Photocatalytic Degradation of Methyl Orange on Iron Niobate Prepared by Solid-State Reaction

2010 ◽  
Vol 113-116 ◽  
pp. 2021-2024 ◽  
Author(s):  
Wen Jie Zhang ◽  
Xin Sun ◽  
Bai Han Chen
Keyword(s):  
Methyl Orange ◽  
Solid State ◽  
Photocatalytic Degradation ◽  
Solid State Reaction ◽  
Irradiation Time ◽  
Molar Ratio ◽  
Preparation Conditions ◽  
New Type ◽  
Iron Niobate ◽  
Degradation Of Methyl Orange

Iron niobate photocatalyst as a new type of photocatalyst was prepared by solid-state reaction of Fe3O4 and Nb2O5 and its activity was evaluated using photocatalytic degradation of methyl orange. Preparation conditions such as calcination temperature and time, and irradiation time were investigated according to photocatalytic efficiencies. FeNb2O6 was produced during calcination below 700 oC and FeNbO4 was produced above 800 oC. Iron niobate with optimum activity could be prepared after calcination at 700 oC for 8 h when Fe:Nb molar ratio was 0.8:1. Methyl orange degradation rate was 72.7% after 180 min of irradiation at photocatalyst concentration of 4 g/l.

Removal of Copper Ion in Industrial Wastewater by Magnetic Flocculation Experimental Research

2013 ◽  
Vol 295-298 ◽  
pp. 1231-1234 ◽  
Author(s):  
Yong Gui Yang ◽  
Yun Long Yang ◽  
Xiao Hong Kang
Keyword(s):  
Industrial Wastewater ◽  
Ph Value ◽  
Copper Ions ◽  
Removal Rate ◽  
Copper Ion ◽  
Good Effect ◽  
Magnetic Powder ◽  
Wastewater Discharge ◽  
Sedimentation Time

An experiment on the removal of heavy metal copper ions from industrial wastewater by magnetic flocculation was studied and the influences of PFS dosage static sedimentation time，temperature，pH value and magnetic powder dosage on treatment effect were discussed at the same time .The result of the test showed that when the dosage of PFS and magnetic powder were 100 and 400 mg/l respectively the pH value was 8.0，the static sedimentation time was 20min, the said process had a good effect on copper containing wastewater treatment. The removal rate of copper ions was over 97％，and the mass concentration of copper ions in the effluent water was below 0.5mg/l. Therefore after be treated by magnetic flocculation the quality of copper-containing wastewater could meet the requirement of GB 8978-1996 Integrated Wastewater Discharge Standard .

Face Recognition Method Based on the Fuzzy Neural Network

2011 ◽  
Vol 128-129 ◽  
pp. 134-137
Author(s):  
Xiang Pan
Keyword(s):  
Neural Network ◽  
Artificial Neural Network ◽  
Face Recognition ◽  
Fuzzy Neural Network ◽  
Experimental Results ◽  
Fuzzy Rules ◽  
Good Effect ◽  
Recognition Method ◽  
Fuzzy Neural ◽  
Artificial Neural

This paper discusses a face recognition method based on the fuzzy neural network (FNN). The fuzzy neural network has more advantages than artificial neural network alone. The paper firstly introduces the structure of the FNN. Than proposed the fuzzy rules and the study algorithm. Thirdly it researches on the process of face recognition. The experimental results prove that this method can achieve good location performance and good effect of extraction.

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