Effects of Alloy Powder for WC/Steel Base Surface Composite Structure and Interface

2011 ◽  
Vol 328-330 ◽  
pp. 1268-1271
Author(s):  
Yu Dong Sui ◽  
Ye Hua Jiang ◽  
Zu Lai Li ◽  
Quan Shan ◽  
Fei Liu

Use Cr15 high chrome steel as base, WC particles as reinforcing particles, and adopting casting-infiltration method, a kind of quite steel-base surface wear-resistant material was prepared. The effect of Alloy powder for WC/steel base surface composite structure and interface was tested by OM, SEM and EDS. The results showed that after adding nickel powder into the composite layer, martensite, austenite, pearlite and eutectic carbide distributed in the matrix; after adding tungsten iron powder into the composite layer, more martensite distributed in the matrix; after adding molybdenum iron powder into the composite layer, martensite, austenite, pearlite and carbide distributed in the matrix. If the base material was high chrome (Cr15) and adds molybdenum iron powder in the composite layer, composite layer interface transition is good, more WC particles and irregular small carbide particles in composite layer.

2010 ◽  
Vol 649 ◽  
pp. 61-66
Author(s):  
Zoltán Kálazi ◽  
Viktória Janó ◽  
Gábor Buza

Tungsten (W) based alloy composite layer reinforced with TiC particles has been successfully prepared on unalloyed steel sample by LMI technology. In order to obtain in situ produced TiC reinforcement, pure titanium has been introduced to the melt pool. WC powder was added for increasing the carbon content of the layer in order to avoid the softening of the matrix (with low carbon content) during TiC formation. The present study aims to investigate the optimum amount of injected WC and Ti powder to improve wear resistance and hardness of the layer. Samples were investigated using scanning electron microscopy (SEM) and X-ray diffraction (XRD). The maximum hardness of the layer has been reached ~900HV in case of 2-4wt% of titanium content. Ti has been collected all of the carbon from the matrix when titanium content was 9,6wt%, which resulted that the austenite and (Fe,W)6C phases have been disappeared. Only α-Fe and TiC phases were presented in the layer. The hardness of the layer reduced to the hardness of the base material.


2019 ◽  
Vol 26 (04) ◽  
pp. 1850182
Author(s):  
P. MUTHUKUMAR ◽  
S. JEROME ◽  
R. JOHN FELIX KUMAR ◽  
S. PRAKASH

In this work, aluminum/titanium carbide (Al/TiC) surface composite has been fabricated by friction stir processing using a novel modular Direct Particle Injection Tool (DPI–FSP). The tool has a unique feature wherein the TiC particles have been transferred from the tool itself by spring adjusted plunger movement into the matrix. The microstructural observations from optical and scanning electron microscope (SEM)-EDS results revealed the homogeneous distribution of particles in the stirred zone (SZ) and the thickness of the formed surface composite layer (SCL) is approximately 0.34[Formula: see text]mm. X-ray diffraction results confirmed that the particles are reinforced in the aluminum matrix, and no intermetallics have been formed in the composite. The microhardness of composite was increased from 68 to 135[Formula: see text]Hv, and the impact test results showed that the toughness was almost comparable to that of the base metal.


2017 ◽  
Vol 17 (1) ◽  
pp. 143-146 ◽  
Author(s):  
S. Sobula ◽  
E. Olejnik ◽  
T. Tokarski

Abstract Wear resistance of TiC-cast steel metal matrix composite has been investigated. Composites were obtained with SHSB method known as SHS synthesis during casting. It has been shown the differences in wear between composite and base cast steel. The Miller slurry machine test were used to determine wear loss of the specimens. The slurry was composed of SiC and water. The worn surface of specimens after test, were studied by SEM. Experimental observation has shown that surface of composite zone is not homogenous and consist the matrix lakes. Microscopic observations revealed the long grooves with SiC particles indented in the base alloy area, and spalling pits in the composite area. Due to the presence of TiC carbides on composite layer, specimens with TiC reinforced cast steel exhibited higher abrasion resistance. The wear of TiC reinforced cast steel mechanism was initially by wearing of soft matrix and in second stage by polishing and spalling of TiC. Summary weight loss after 16hr test was 0,14÷0,23 g for composite specimens and 0,90 g for base steel.


2017 ◽  
Vol 62 (1) ◽  
pp. 321-326 ◽  
Author(s):  
J. Górka

Abstract This study presents tests concerned with welding thermal process-induced precipitation processes taking place in 10 mm thick steel S700MC subjected to the Thermo-Mechanical Control Process (TMCP) with accelerated cooling. The thermomechanical processing of steel S700MC leads to its refinement, structural defects and solutioning with hardening constituents. Tests of thin foils performed using a transmission electron microscope revealed that the hardening of steel S700MC was primarily caused by dispersive (Ti,Nb)(C,N) precipitates (being between several and less than twenty nanometers in size). In arc welding, depending on a welding method and linear energy, an increase in the base material in the weld is accompanied by the increased concentration of hardening microagents in the weld. The longer the time when the base material remains in the liquid state, the greater the amount of microagents dissolved in the matrix. During cooling, such microagents can precipitate again or remain in the solution. An increase in welding linear energy is accompanied by an increase in the content of hardening phases dissolved in the matrix and, during cooling, by their another uncontrolled precipitation in the form of numerous fine-dispersive (Ti,Nb)(C,N) precipitates of several nm in size, leading to a dislocation density increase triggered by type 2 internal stresses.


Author(s):  
E. Dilara Koçak

Producing composites from natural fibers is known to be common. These fibers benefit from their mechanical performances, low density, and their biodegradability. However, it is necessary for the fibers to form adhesion in the matrix. Therefore, it is necessary to apply a chemical process to the surface of the fibers. In this study, four different processes in conventional and ultrasonic energies were applied on luffa cylindrical fibers. At the end of the application, a composite structure was formed on the fibers that were obtained by using unsaturated polyester resin. The changes in the characteristics of the composite structure were recorded by mechanical tests, Fourier transform infrared, X-ray diffractometer, and their morphological characteristics by means of scanning electron microscopy. Considering all the results, formic acid and acetic acid process results were found to adequately modify the fiber surfaces.


2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
M. Poornesh ◽  
Shreeranga Bhat ◽  
E.V. Gijo ◽  
Pavana Kumara Bellairu

PurposeThis article aims to study the tensile properties of a functionally graded composite structure with Al–18wt%Si alloy as the matrix material and silicon carbide (SiC) particles as the reinforcing element. More specifically, the study's primary objective is to optimize the composition of the material elements using a robust statistical approach.Design/methodology/approachIn this research, the composite material is fabricated using a combination of stir casting and the centrifugal casting technique. Moreover, the test specimen required to study the tensile strength are prepared according to the ASTM (American Society for Testing and Materials) standards. Eventually, optimal composition to maximize the tensile property of the material is determined using the mixture design approach.FindingsThe investigation results imply that the addition of the SiC plays a crucial role in increasing the tensile strength of the composite. The optical microstructural images of the composite show the adequate distribution of the reinforcing particles with the matrix. The proposed regression model shows better predictability of tensile strength. In addition, the methodology aids in optimizing the mixture component values to maximize the tensile strength of the produced functionally graded composite structure.Originality/valueLittle work has been reported so far where a hypereutectic Al–Si alloy is considered the matrix material to produce the composite structure. The article attempts to make a composite structure by using a combination of stir casting and centrifugal casting. Furthermore, it employs the mixture design to optimize the composition and predict the model of the study, which is one of a kind in the field of material science.


2012 ◽  
Vol 1518 ◽  
pp. 79-84 ◽  
Author(s):  
Hideaki Miyakawa ◽  
Tomofumi Sakuragi ◽  
Hitoshi Owada ◽  
Osamu Kato ◽  
Kaoru Masuda

ABSTRACTIodine filters expended after nuclear fuel reprocessing contain radioactive iodine (I-129), almost all of which exists as silver iodide (AgI). The synthetic rock technique is a solidification treatment technique using hot isostatic press (HIP), in which the alumina adsorbent base material is synthesized to form a dense solidified material (synthetic rock), and I-129 is physically confined in the form of AgI in the alumina matrix. Thus, it is necessary to understand the matrix dissolution behavior to evaluate the iodine release behavior.Experiments involving the dissolution of the matrix were carried out under various temperatures (35–70 °C) and pH values (10–12.5) that reflect the disposal conditions. The results of the experiments showed that the dissolution rate of Al visibly increases with temperature and pH. The dissolution rate constant was calculated from the initial data assuming the dissolution of the matrix as a primary reaction. The logarithmic rate constant showed a good linear correlation with the pH and the reciprocal of temperature. The 27Al-NMR analysis of the solutions of the dissolved matrix showed that the major chemical species present in the solutions was Al(OH)4-. This indicated that the dissolution of the matrix can be described by the following equation: Al2O3 + 2OH- + 3H2O → 2Al(OH)4-. Subsequently, the empirical equation of the rate of dissolution of the matrix as a function of the temperature and pH was derived. It will be used to evaluate the iodine release behavior from the synthetic rock.


2020 ◽  
Vol 1002 ◽  
pp. 140-150
Author(s):  
Ali H. Al-Helli ◽  
Ahmed R. Alhamaoy ◽  
Ayad Murad Takhakh

Friction Stir Processing (FSP) technology was wielded to output the Al7075/ Al2O3 surface composite. The effects parameters of processing method on particle distribution have been studied. The microstructure and mechanical characteristics of the samples were examined using the optical microscope, SEM and hardness examination. Acquired consequences, showed that Al2O3 particles were in a good interior distribution inside the basement. This technique produced excellent bonding between the surface composite and the base material. On other hand the surface hardness was increased about 25% as compared with the substrate. In addition, grain matrix refinement and enhanced particle distribution were obtained after each FSP pass. Also the dispersion of Al2O3 particles in the stirred area became more homogeneous and the average hardness improved by increasing the number of passes.


2011 ◽  
Vol 415-417 ◽  
pp. 170-173
Author(s):  
Jing Wang ◽  
Si Jing Fu ◽  
Yi Chao Ding ◽  
Yi San Wang

A wear resistant TiC-Cr7C3/Fe surface composite was produced by cast technique and in-situ synthesis technique. The microstructure and dry-sliding wear behavior of the surface composite was investigated using scanning electron microscope(SEM), X-ray diffraction(XRD) and MM-200 wear test machine. The results show that the surface composite consists of TiC and Cr7C3as the reinforcing phase, α-Fe and γ-Fe as the matrix. The surface composite has excellent wear-resistance under dry-sliding wear test condition with heavy loads.


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