Research on Detecting Tris-(2,3-dibromopropyl)-Phosphate in Textiles with the HPLC/DAD Method
Keyword(s):
A detecting method for toxic flame retardant finishing agent tris-(2,3-dibromopropyl) -phosphate (TRIS for short) in textiles was studied. In the method, an acetonitrile ultrasound-assisted extraction process was included in sample pre-treatment, and HPLC/DAD was used in the separation and identification of extractives. After that, the conditions of pre-treatment and chromatograph were optimized. The results showed that the limit of detection (LOD) by this method (S/N10) is 1.0 mg/kg, its recovery ranged from 78.1% to 98.4%, and RSD of the precision test is 3.2%, of which all met the requirements for routine testing.
2020 ◽
Vol 11
(2)
◽
pp. 9318-9334
2015 ◽
Vol 6
(3)
◽
pp. 289-299
◽
2016 ◽
Vol 166
◽
pp. 73-82
◽
2017 ◽
Vol 54
(8)
◽
pp. 2361-2371
◽
2012 ◽
Vol 21
(6)
◽
pp. 1701-1706
◽
Keyword(s):