scholarly journals Ultrasound-assisted extraction process of phenolic antioxidants from Olive leaves: a nutraceutical study using RSM and LC–ESI–DAD–MS

2017 ◽  
Vol 54 (8) ◽  
pp. 2361-2371 ◽  
Author(s):  
Habib Shirzad ◽  
Vahid Niknam ◽  
Mehdi Taheri ◽  
Hassan Ebrahimzadeh
Keyword(s):  
Extraction Process ◽  
Phenolic Antioxidants ◽  
Olive Leaves ◽  
Ultrasound Assisted Extraction ◽  
Assisted Extraction ◽  
Ultrasound Assisted

Research on Detecting Tris-(2,3-dibromopropyl)-Phosphate in Textiles with the HPLC/DAD Method

2012 ◽  
Vol 441 ◽  
pp. 640-644
Author(s):  
Ke Jie Fu ◽  
Li Sheng Yang ◽  
Chang Sheng Feng ◽  
Liang Chen
Keyword(s):  
Limit Of Detection ◽  
Extraction Process ◽  
Ultrasound Assisted Extraction ◽  
Routine Testing ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Pre Treatment ◽  
Finishing Agent ◽  
Detecting Method ◽  
Precision Test

A detecting method for toxic flame retardant finishing agent tris-(2,3-dibromopropyl) -phosphate (TRIS for short) in textiles was studied. In the method, an acetonitrile ultrasound-assisted extraction process was included in sample pre-treatment, and HPLC/DAD was used in the separation and identification of extractives. After that, the conditions of pre-treatment and chromatograph were optimized. The results showed that the limit of detection (LOD) by this method (S/N10) is 1.0 mg/kg, its recovery ranged from 78.1% to 98.4%, and RSD of the precision test is 3.2%, of which all met the requirements for routine testing.

scholarly journals Optimization of Ultrasound-Assisted Extraction of Flavonoids from Olive (Olea europaea) Leaves, and Evaluation of Their Antioxidant and Anticancer Activities

Molecules ◽  
2018 ◽  
Vol 23 (10) ◽  
pp. 2513 ◽  
Author(s):  
Bixia Wang ◽  
Jipeng Qu ◽  
Siyuan Luo ◽  
Shiling Feng ◽  
Tian Li ◽  
...  
Keyword(s):  
Olea Europaea ◽  
Maximum Yield ◽  
Flavonoid Compound ◽  
Anticancer Activities ◽  
Olive Leaves ◽  
Ultrasound Assisted Extraction ◽  
Assisted Extraction ◽  
Significant Difference ◽  
Ultrasound Assisted ◽  
Olea Europaéa

Olea europaea leaves are the major byproduct of olive farming. In this study, ultrasound-assisted extraction of flavonoids from olive leaves was optimized using response surface methodology, and the flavonoid compounds and their antioxidant and anticancer activities were investigated by high performance liquid chromatography. The results showed that the optimized conditions for achieving the maximum yield of flavonoids (74.95 mg RE/g dm) were 50 °C temperature, 270 W power, 50 min time, and 41 mL/g liquid-solid ratio. There was a significant difference in the total flavonoid content between the aged and young leaves harvested in April and July, and six main components were quantified. Among them, luteolin-4’-O-glucoside was the most predominant flavonoid compound, followed by apigenin-7-O-glucoside and rutin. Olive leaves also contained small amounts of luteolin, apigenin, and quercetin. Additionally, excellent antioxidant activity was exhibited when tested with the DPPH assay; superoxide radical-scavenging ability and reducing power was also tested. The anticancer activity of the flavonoids was assessed using HeLa cervical cancer cells, and it was observed that increasing concentrations of olive leaf flavonoids resulted in decreased cancer cell viability. These results suggest that the flavonoids from olive leaves could be used as a potential source of natural antioxidants for the pharmaceutical and food industries.

scholarly journals Effects of Ultrasound-Assisted Extraction and Solvent on the Phenolic Profile, Bacterial Growth, and Anti-Inflammatory/Antioxidant Activities of Mediterranean Olive and Fig Leaves Extracts

Molecules ◽  
2020 ◽  
Vol 25 (7) ◽  
pp. 1718 ◽  
Author(s):  
Cristina Alcántara ◽  
Tihana Žugčić ◽  
Radhia Abdelkebir ◽  
Jose V. García-Pérez ◽  
Anet Režek Jambrak ◽  
...  
Keyword(s):  
Bioactive Compounds ◽  
Bacterial Growth ◽  
Extraction Methods ◽  
Olive Leaves ◽  
Ultrasound Assisted Extraction ◽  
Phenolic Profile ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Conventional Extraction ◽  
Anti Inflammatory

Mediterranean plants, such as fig and olive leaves, are well-known to exert beneficial effects in humans because of the presence of a wide range of bioactive compounds. However, scarce information regarding the impact of extraction methods, such as ultrasound and types of solvents, on their profile of antioxidant and anti-inflammatory compounds is provided. In addition, no information is available on the effects of extraction methods and solvents on the inhibition of pathogenic bacteria or promoting probiotic growth. In this scenario, this study was aimed to study the effects of ultrasound-assisted extraction (UAE) and solvent on the phenolic profile (Triple TOF-LC-MS/MS), antioxidant and anti-inflammatory compounds of olive and fig leaves. Results showed that UAE extracted more carotenoids compared to conventional extraction, while the conventional extraction impacted on higher flavonoids (olive leaves) and total phenolics (fig leaves). The antioxidant capacity of aqueous extract of fig leaves was three times higher than the extract obtained with ethanol for conventional extraction and four times higher for UAE. In general terms, hydroethanolic extracts presented the highest bacterial growth inhibition, and showed the highest anti-inflammatory activity. In conclusion, these side streams can be used as sources of bioactive compounds for further development of high-added-value products.

scholarly journals Antioxidant Capacity and Antigenotoxic Effect of Hibiscus sabdariffa L. Extracts Obtained with Ultrasound-Assisted Extraction Process

2020 ◽  
Vol 10 (2) ◽  
pp. 560
Author(s):  
Gregorio Iván Peredo Pozos ◽  
Mario Alberto Ruiz-López ◽  
Juan Francisco Zamora Nátera ◽  
Carlos Álvarez Moya ◽  
Lucia Barrientos Ramírez ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Human Lymphocytes ◽  
Dry Weight ◽  
Extraction Process ◽  
Hibiscus Sabdariffa ◽  
Ultrasound Assisted Extraction ◽  
Solid Ratio ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Antigenotoxic Effect

Hibiscus sabdariffa (Roselle) is in high demand worldwide due to its beneficial health properties owing to the polyphenols content, mainly in the flower calyx. The objective of this study was to find the best conditions (time and liquid: solid ratio) to extract polyphenols from Roselle using Ultrasound-Assisted Extraction (UAE) (40 kHz, 180 W), with ethanol how solvent; as well as determine the yield of phenols, anthocyanin, flavonoids, tannins, antioxidant activity (DPPH) and antigenotoxic effect (comet assay). A traditional solid-liquid extraction was applied as a reference. Extraction times of 40 and 60 min resulted in the highest polyphenols (13.019 mg GAE/g dry weight (dw)), flavonoids (4.981 CE/g dw), anthocyanins (1.855 mg Cya3GE/g dw), and tannins (0.745 CE/g dw) recoveries and an antioxidant activity (DPPH) of 74.58%. Extracts from white calyces contained similar amounts of phenols and flavonoids, but very little condensed tannins (0.049 CE/g dw) and practically no anthocyanins. Extracts from red and white calyces, showed antigenotoxic activity and repaired capacity of damage caused by mutagens in human lymphocytes.

scholarly journals Bioactive Compounds in Bael Fruit Pulp Waste: Ultrasound-Assisted Extraction, Characterization, Modeling, and Optimization Approaches

2020 ◽  
Vol 11 (2) ◽  
pp. 9318-9334
Keyword(s):  
Bioactive Compounds ◽  
Food Additives ◽  
Extraction Process ◽  
Coefficient Of Determination ◽  
Fruit Pulp ◽  
Ultrasound Assisted Extraction ◽  
Modeling And Optimization ◽  
Assisted Extraction ◽  
Pharmaceutical Industries ◽  
Ultrasound Assisted

Bael fruit is an abundant source of bioactive compounds that have importance in the food and pharmaceutical industries. The process of extraction of the bael fruit juice produced a higher percentage of bael fruit pulp waste (BFPW) (37.33 %), which was recycled for the extraction of bioactive compounds. Thus the bioactive compounds like polyphenols, flavonoids, and carotenoids were extracted from BFPW by using the ultrasound-assisted extraction (UAE) technique. The modeling and optimization of the extraction process were carried out by using the experimental design of response surface methodology (RSM). The ethanol concentration of 51.22 %, ultrasound amplitude of 51.45 %, and ultrasound treatment time of 6.11 minutes were obtained to be an RSM optimized values of extraction process variables. The lower values of root mean squared error (RMSE) and mean absolute error (MAE) and higher values of coefficient of determination (R2) indicated admissibility and acceptability of RSM. This extraction process of bioactive compounds has the potential to implement it on an industrial scale for the formulation of food additives and medicines.

scholarly journals Enhanced yield of oleuropein from olive leaves using ultrasound-assisted extraction

2018 ◽  
Vol 6 (4) ◽  
pp. 1128-1137 ◽  
Author(s):  
Domenico Cifá ◽  
Mihaela Skrt ◽  
Paola Pittia ◽  
Carla Di Mattia ◽  
Nataša Poklar Ulrih
Keyword(s):  
Olive Leaves ◽  
Ultrasound Assisted Extraction ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Enhanced Yield
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