The Effect of Nano-Particles in Superconducting MgB2 Thin Films on Stainless Steel Substrates

2012 ◽  
Vol 530 ◽  
pp. 62-67 ◽  
Author(s):  
Yin Bo Wang ◽  
Yi Ling Chen ◽  
Qing Rong Feng

We have fabricated several superconducting MgB2thin films on stainless steel substrates by using hybrid physical-chemical vapor deposition (HPCVD) in pure argon atmosphere. These films were observed by scanning electron microscopes (SEM) and used the energy dispersive X-ray spectroscopy (EDX) to make elements analyses. The film thickness is about 800~1000 nm. There were some cracks on the film surface when the film is bent by different angle. The number of cracks and their width increased with the increasing bending angle. Nevertheless, the films were attached to the substrates firmly. It concludes that the superconducting MgB2thin films have great ductility and adhesion to the stainless steel substrates. We found in these films many granules about tens of nanometers in size. These nano-granules can balance both the inner structure and the surface activity of the MgB2crystal. This might be an important reason for the ductility observed with the superconducting thin films. The exact explanation depends on further research.

Carbon ◽  
2021 ◽  
Vol 171 ◽  
pp. 739-749
Author(s):  
Pratik Joshi ◽  
Ariful Haque ◽  
Siddharth Gupta ◽  
Roger J. Narayan ◽  
Jagdish Narayan

1991 ◽  
Vol 226 ◽  
Author(s):  
Masahiro Jono ◽  
Atsushi Sugeta

AbstractFracture strength of amorphous A1203 insulating thin film coated on a Fe-42%Ni base metal was Investigated under static and cyclic loadings by using four point bending apparatus. It was found that the both static and cyclic fracture strength of thin film decreased with increasing coating thickness and also fracture under cyclic loading occurred at a strain below the static fracture strength. Observations In detail by the optical and scanning electron microscopes revealed that the splash particles deposited in coating process caused crack initiation origins. Evaluation method of fracture strength of thin films was discussed based on the fracture mechanics approach.


2008 ◽  
Vol 2008 ◽  
pp. 1-5 ◽  
Author(s):  
E. Barrera-Calva ◽  
J. Méndez-Vivar ◽  
M. Ortega-López ◽  
L. Huerta-Arcos ◽  
J. Morales-Corona ◽  
...  

Silica-copper oxide (silica-CuO) composite thin films were prepared by a dipping sol-gel route using ethanolic solutions comprised TEOS and a copper-propionate complex. Sols with different TEOS/Cu-propionate (Si/Cu) molar ratios were prepared and applied on stainless steel substrates using dipping process. During the annealing process, copper-propionate complexes developed into particulate polycrystalline CuO dispersed in a partially crystallized silica matrix, as indicated by the X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS) analyses. The gel thermal analysis revealed that the prepared material might be stable up to400°C. The silica-CuO/stainless steel system was characterized as a selective absorber surface and its solar selectivity parameters, absorptance (α), and emittance (ε) were evaluated from UV-NIR reflectance data. The solar parameters of such a system were mostly affected by the thickness and phase composition of theSiO2-CuO film. Interestingly, the best solar parameters (α= 0.92 andε= 0.2) were associated to the thinnest films, which comprised a CuO-Cu2Omixture immersed in the silica matrix, as indicated by XPS.


2019 ◽  
Vol 784 ◽  
pp. 231-236 ◽  
Author(s):  
Susu Wang ◽  
Hao Wang ◽  
Jie Jian ◽  
Jianguo Chen ◽  
Jinrong Cheng

2017 ◽  
Vol 71 (8) ◽  
pp. 1990-2000 ◽  
Author(s):  
José L. Ruiz-Caballero ◽  
Joaquín A. Aparicio-Bolaño ◽  
Amanda M. Figueroa-Navedo ◽  
Leonardo C. Pacheco-Londoño ◽  
Samuel P. Hernandez-Rivera

1993 ◽  
Vol 308 ◽  
Author(s):  
Karl B. Yoder ◽  
Donald S. Stone

ABSTRACTThe ability to measure the temperature-dependence of the hardness of thin films is useful from both an applications and a scientific standpoint. For this reason, we have designed and constructed a load- and depth-sensing indentation tester combining sub-nanometer resolution with the ability to operate over a range of temperatures, currently 150K to 400K. This paper describes the new experimental apparatus and reports preliminary data on 440C stainless steel substrates with and without a 0.75 μm ZrN coating.


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