Relaxor Properties and Tunability of Electron-Irradiated Thin Poly(vinlidene fluoride-trifluoroethylene) Copolymer Film

2012 ◽  
Vol 560-561 ◽  
pp. 892-898 ◽  
Author(s):  
Li Tian ◽  
Xiang Jian Meng ◽  
Jing Yang ◽  
Jing Lan Sun ◽  
Sheng Zhao Yuan ◽  
...  

The effect of high energy electron irradiation on poly(vinlidene fluoride-trifluoroethylene) copolymer film with thickness about 180 nm has been studied. Both dielectric spectroscopy investigation and X-Ray Diffraction show that all-trans conformation of pre-irradiated films is transformed to trans-gauche conformation after irradiation. The relaxor behavior of irradiated sample obeys the modified Curie-Weiss and Vogel-Fulcher law. And the tunability is increased from 42% to 63% after irradiation.

2011 ◽  
Vol 208 (11) ◽  
pp. 2552-2557 ◽  
Author(s):  
V. B. Molodkin ◽  
S. I. Olikhovskii ◽  
E. G. Len ◽  
B. V. Sheludchenko ◽  
S. V. Lizunova ◽  
...  

2017 ◽  
Vol 19 (19) ◽  
pp. 12064-12074 ◽  
Author(s):  
Emilia I. Wisotzki ◽  
Paolo Tempesti ◽  
Emiliano Fratini ◽  
Stefan G. Mayr

Small-angle X-ray scattering revealed ranging structural differences in physically entangled and irradiation-crosslinked gelatin hydrogels.


1993 ◽  
Vol 8 (2) ◽  
pp. 321-323 ◽  
Author(s):  
Ryusuke Kita ◽  
Takashi Hase ◽  
Hiromi Takahashi ◽  
Kenichi Kawaguchi ◽  
Tadataka Morishita

The growth of BaO and SrO on SrTiO3(100) substrates using mass-separated low-energy (50 eV) O+ beams has been studied using x-ray diffraction, reflection high-energy electron diffraction, and high-resolution transmission electron microscopy. It was found that the BaO and SrO films have been epitaxially grown with new structures different from those of corresponding bulk crystals: The BaO films have a cubic structure with a lattice constant of 4.0 Å, and the SrO films have a tetragonal structure with a lattice constant of a = 3.7 Å parallel to the substrate and with c = 4.0 Å normal to the substrate.


1993 ◽  
Vol 312 ◽  
Author(s):  
A. H. Bensaoula ◽  
A. Freundlich ◽  
A. Bensaoula ◽  
V. Rossignol

AbstractPhosphorus exposed GaAs (100) surfaces during a Chemical Beam Epitaxy growth process are studied using in-situ Reflection High Energy Electron Diffraction and ex-situ High Resolution X-ray Diffraction. It is shown that the phosphorus exposure of a GaAs (100) surface in the 500 – 580 °C temperature range results in the formation of one GaP monolayer.


1980 ◽  
Vol 1 ◽  
Author(s):  
J. T. Schott ◽  
J. J. Comer

ABSTRACTVarious characterization techniques are applied to pulsed and cw laser-annealed polysilicon layers deposited on oxide layers. The results are used to compare these techniques as to the type and completeness of information provided, as well as sample preparation requirements and general ease or difficulty of measurement. The techniques employed include scanning electron microscopy (SEM), electron channeling micrographs and selected area channeling patterns (SACP), reflection (high energy) electron diffraction (RHEED), transmission electron microscopy (TEM) and selected area diffraction (SAD), x-ray diffraction, optical techniques and etching techniques.


2002 ◽  
Vol 16 (28n29) ◽  
pp. 4302-4305 ◽  
Author(s):  
LIWEN TAN ◽  
JUN WANG ◽  
QIYUAN WANG ◽  
YUANHUAN YU ◽  
LANYING LIN

The γ- Al 2 O 3 films were grown on Si (100) substrates using the sources of TMA ( Al ( CH 3)3) and O 2 by very low-pressure chemical vapor deposition (VLP-CVD). It has been found that the γ- Al 2 O 3 film has a mirror-like surface and the RMS was about 2.5nm. And the orientation relationship was γ- Al 2 O 3(100)/ Si (100). The thickness uniformity of γ- Al 2 O 3 films for 2-inch epi-wafer was less than 5%. The X-ray diffraction (XRD) and reflection high-energy electron diffraction (RHEED) results show that the crystalline quality of the film was improved after the film was annealed at 1000°C in O 2 atmosphere. The high-frequency C-V and leakage current of Al /γ- Al 2 O 3/ Si capacitor were also measured to verify the annealing effect of the film. The results show that the dielectric constant increased from 4 to 7 and the breakdown voltage for 65-nm-thick γ- Al 2 O 3 film on silicon increases from 17V to 53V.


2013 ◽  
Vol 1501 ◽  
Author(s):  
Tetsuhiko Miyadera ◽  
Hiroki Mitsuta ◽  
Noboru Ohashi ◽  
Tetsuya Taima ◽  
Ying Zhou ◽  
...  

ABSTRACTWe have developed a method for epitaxial growth of C60 thin films on tetracene single crystals. The crystal orientation of the C60 film was examined by reflection high energy electron diffraction (RHEED) and X-ray diffraction (XRD). In-situ observation by RHEED revealed that the C60 crystallizes from the very initial stage of the deposition (0.1 nm). A 6-fold symmetric pattern, which was observed in a XRD polar scan, can be taken as direct evidence for the epitaxial growth of C60 commensurate with the tetracene (001) surface lattice.


1997 ◽  
Vol 474 ◽  
Author(s):  
G. Chern ◽  
C. L. Chang ◽  
Y. R. Chean

AbstractThe growth and structural characterization of Fe3O4/MgO superlattices on MgO(001) and Fe-coated MgO(001) are compared. Long modulated coherence and sharp interface are revealed by X-ray diffraction and reflection high energy electron diffraction (RHEED). For the superlattice grown directly on MgO(001), high crystalline quality is comparable to the previous report on the oxide superlattice system. For the superlattice grown on Fe/MgO(001), both chemical and lattice spacing modulations are maintained which is different from the polycrystlline structure of the Fe3O4/NiO grown on Ni-based system. This superiority of the growth on Fe-coated surface results from both the smaller lattice mismatch and the oxidation state of Fe relative to MgO. The changes of the RHEED intensity during the growth of these superlattices are also measured. The evolution of the oxide interface during the growth of Fe3O4/MgO is quantitatively presented.


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