Ultrasonic-Assisted Oxalic Acid Extraction of Copper from Plateau Red Soil and Tessier Speciation Evaluation

2013 ◽  
Vol 726-731 ◽  
pp. 2368-2371
Author(s):  
Yan Zheng ◽  
Xue Jin Zhou ◽  
Yun Tao Gao ◽  
Sheng Li Huang ◽  
Ruo Sen Yuan ◽  
...  
Keyword(s):  
Oxalic Acid ◽  
Extraction Method ◽  
Red Soil ◽  
Extraction Rate ◽  
Extraction Time ◽  
Acid Extraction ◽  
Activation Effect ◽  
Solid Ratio ◽  
Ultrasonic Assisted ◽  
Iron And Manganese

Abstract. The copper in plateau red soil was extracted by ultrasonic-assisted oxalic acid. Tessier fractional extraction method was used to evalute copper speciation. The result showed that the biggest extraction rate was 69%. Compared with oscillation extraction, the extraction rate of ultrasonic extraction was increased by 7.18% under the condition of 0.1 mol/L oxalic acid, 20:1 of liquid-solid ratio and 30 min of extraction time. Ultrasound could promote the oxalic acid extraction of copper from plateau red soil effectively, which could be attributed the success to the activation effect of ultrasound on bound to carbonates speciation and bound to iron and manganese speciation.

Ultrasound-Assisted Citric Acid Extraction of Zinc in Plateau Red Soil and Tessier Speciation Study

2013 ◽  
Vol 726-731 ◽  
pp. 4464-4467
Author(s):  
Wei Wei ◽  
Xue Jin Zhou ◽  
Yun Tao Gao
Keyword(s):  
Heavy Metal ◽  
Citric Acid ◽  
Manganese Oxides ◽  
Red Soil ◽  
Extraction Rate ◽  
Acid Extraction ◽  
Speciation Study ◽  
Ultrasonic Assisted ◽  
Ultrasound Assisted ◽  
Iron And Manganese

Taking plateau red soil as research object, using the ultrasonic-assisted organic acid extraction the heavy metal zinc in it, and analyze the form of zinc. Results showed that the extraction rate can reach 68%, with the increase of time, the extraction effect of zinc is obviously enhanced in this method. Ultrasonic-assisted citric acid extraction soil can increase the extraction rate of exchangeable, bound to carbonates and bound to iron and manganese oxides relatively.

scholarly journals Orthogonal Optimization of Polysaccharide Extraction from Millet Bran

2019 ◽  
Vol 78 ◽  
pp. 02011
Author(s):  
Songling Cai ◽  
Min Pang
Keyword(s):  
Extraction Method ◽  
Extraction Process ◽  
Orthogonal Test ◽  
Extraction Rate ◽  
Extraction Time ◽  
Alkali Concentration ◽  
Extraction Temperature ◽  
Solid Ratio ◽  
Optimum Parameters ◽  
Orthogonal Optimization

This paper investigated the effects of liquid-solid ratio, extraction time, extraction temperature and alkali concentration on the extraction rate of millet bran polysaccharides by the enzymatic hydrolysis and alkaline extraction method, then the L9 (34) orthogonal test was designed to optimize the extraction process according to the single factor experiment.The optimum parameters were obtained as follow: 15:1 liquid-solid ratio, five hours extraction time, 80° extraction temperature, and 0.7 mol/l concentration of sodium hydroxide. The extraction rate of millet bran polysaccharide reached 11.46% through the verification experiments under these conditions,and the RSD was 1.79%. Therefore, it can provide some experimental basis for the scientific research of millet bran polysaccharides in the future.

Contrastive Experimental of the Ultrasonic-Assisted Extraction and Oscillation Extraction of Lead from Soil Using EDTA

2013 ◽  
Vol 781-784 ◽  
pp. 2301-2304
Author(s):  
Wen Cao ◽  
Xue Jin Zhou ◽  
Yun Tao Gao
Keyword(s):  
Red Soil ◽  
Extraction Rate ◽  
Extraction Time ◽  
Experimental Result ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction ◽  
Optimum Extraction

Ultrasonic-assisted extraction of lead from red soil using EDTA was investigated, the experimental result was compared with that of oscillation extraction to evaluate the performance of ultrasonic-assisted extraction. The optimum extraction conditions were 0.006 mol/L of EDTA, 0.006 mol/L of EDTA and 90 min of ultrasonic-assisted extraction or 240 min of oscillation extraction. Under the optimum extraction conditions, the extraction rate of 76.33% and 74.30% was obtained for ultrasonic-assisted extraction and oscillation extraction, respectively. The ultrasonic-assisted extraction could shorter the extraction time with a improved extraction rate effectively.

Optimization of Ultrasonic-Assisted Extraction of Polysaccharides from Ottelia acuminata (Gagnep.) Dandy Using RSM

2011 ◽  
Vol 396-398 ◽  
pp. 292-296
Author(s):  
Ai Shi Zhu
Keyword(s):  
Processing Parameters ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Independent Variables ◽  
Solid Ratio ◽  
Assisted Extraction ◽  
Ultrasonic Technology ◽  
Ultrasonic Assisted ◽  
Experimental Yield ◽  
Ultrasonic Assisted Extraction

Ultrasonic technology was applied to polysaccharides extraction from Ottelia acuminata (Gagnep.) Dandy and Response Surface Methodology (RSM) was used to optimize the effects of processing parameters on polysaccharides yields. Three independent variables such as liquid-solid ratio (ml/g, X1), extraction temperature (°C, X2) and extraction time (hour, X3) were investigated respectively. The statistical analysis indicated that the three variables and the quadratic of X1 and X3 had significant effects on the yields and followed by the significant interaction effects between the variables of X1 and X3, X2 and X3 (p<0.05). A mathematical model with high determination coefficient was gained. The optimal extraction conditions of polysaccharides were determined as follows: liquid-solid ratio 43 ml/g, extraction temperature 90 °C and extraction time 3.45 hours. Under these conditions, the experimental yield of polysaccharides was 107.44 mg/g, which was agreed closely with the predicted value 108.71 mg/g.

scholarly journals Optimization of Ultrasound-Assisted Extraction of Antioxidant Polyphenols from the Seed Coats of Red Sword Bean (Canavalia gladiate (Jacq.) DC.)

Antioxidants ◽  
2019 ◽  
Vol 8 (7) ◽  
pp. 200 ◽  
Author(s):  
Yue Zhou ◽  
Xiao-Yu Xu ◽  
Ren-You Gan ◽  
Jie Zheng ◽  
Ya Li ◽  
...  
Keyword(s):  
Extraction Method ◽  
Natural Antioxidants ◽  
Extraction Time ◽  
Antioxidant Compounds ◽  
Extraction Temperature ◽  
Ultrasound Assisted Extraction ◽  
Solid Ratio ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Seed Coats

The seed coat of red sword bean (Canavalia gladiata (Jacq.) DC.) is rich in antioxidant polyphenols. It is often discarded as a byproduct with the consumption of red sword bean, since it is very thick and not consumed by people. The aim of this study was to develop an ultrasound-assisted extraction method to extract natural antioxidants from the seed coats. The extraction process was optimized by using response surface methodology. After the single-factor experiments, three key factors, including ethanol concentration, liquid/solid ratio, and extraction time, were selected and their interactions were studied using a central composite design. The optimal extraction condition was 60.2% hydroethanol, a liquid/solid ratio of 29.3 mL/g, an extraction time of 18.4 min, an extraction temperature of 50 °C, and ultrasound power of 400 W. Under the optimal conditions, antioxidant activity of the extract was 755.98 ± 10.23 μmol Trolox/g dry weight (DW), much higher than that from maceration (558.77 ± 14.42 μmol Trolox/g DW) or Soxhlet extraction (479.81 ± 12.75 μmol Trolox/g DW). In addition, the main antioxidant compounds in the extract were identified and quantified by high-performance liquid chromatography–diode array detection–tandem mass spectrometry (HPLC–DAD–MS/MS). The concentrations of digalloyl hexoside, methyl gallate, gallic acid, trigalloyl hexoside, and digallic acid were 15.30 ± 0.98, 8.85 ± 0.51, 8.76 ± 0.36, 4.27 ± 0.21, and 2.89 ± 0.13 mg/g DW. This study provides an efficient and green extraction method for the extraction of natural antioxidants from the bean coat of red sword bean. The extract of antioxidants might be added into functional foods or nutraceuticals with potential beneficial functions.

Study on Renovation of Heavy Metal Pb (II)-Contaminated Soil

2012 ◽  
Vol 518-523 ◽  
pp. 1800-1803
Author(s):  
Xiao Jiao Yu ◽  
Lin Zhu Huang ◽  
Qian Yang ◽  
Fan Zhang ◽  
Jian Zhang
Keyword(s):  
Heavy Metal ◽  
Contaminated Soil ◽  
Extraction Efficiency ◽  
Removal Rate ◽  
Polluted Soil ◽  
Extraction Rate ◽  
Extraction Time ◽  
Regeneration Medium ◽  
Solid Ratio ◽  
Edta Concentration

To remedy polluted soil, EDTA is choosen when seeing metal Pb (Ⅱ) as target pollutant. There has been a focus on discussion about the infuencs of liquid-solid ratio, EDTA concentration and extraction time on Pb (Ⅱ) extraction rate. And attention is being paid to study the effect of Na2S concentration and pH on Pb (Ⅱ) removal rate with Na2S as EDTA regeneration medium. The results obtained demonstrate that when the liquid-solid ratio is 10, EDTA concentration is 0.5 mol/L, extraction time is 24 h, extraction efficiency can reach 66.67 %. When the concentration of Na2S is 0.5 mol/L, pH is 10, the 96.67 % Pb (Ⅱ) removal rate can be achieved.

Optimization of Ultrasonic-Assisted Extraction of Flavonoids from Moringa oleifera Leaves Using Response Surface Methodology

2021 ◽  
pp. 363-367
Author(s):  
Abdelhakim Benarima ◽  
Mohamed Nasreddine Raache ◽  
Moulay Rachid Kouadri ◽  
Yassine Belaiche ◽  
Salah Eddine Laouini
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Moringa Oleifera ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Solid Ratio ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Moringa Oleifera Leaves ◽  
Ultrasonic Assisted Extraction

Moringa oleifera is considered one of the most useful plants in the world because it's rich in bioactive substances, which employing on modern medical treatment, also can be used for many fields: pharmaceutical, food and cosmetics purposes. In this study, the response surface methodology (RSM) based on a Box–Behnken design (BBD) was employed to optimize the extraction time (X1: 20–60 min), extraction temperature (X2: 15–45 °C) and solvent-solid ratio (X3: 5–7 ml/g), to obtain a high crude of flavonoids yield from Moringa oleifera Leaves by ultrasonic-assisted extraction technique (UAE). The optimum conditions were an extraction time 23 (min), extraction temperature 44 (°C) and solvent-solid ratio 5.05 (ml/g). Under these conditions, the experimental yield was 72.65 (mg ER/g), well matched with the predicted yield 74.34 (mg ER/g) with the coefficients of determination (R2= 0.9861), thus indicating the suitability of response surface methodology in optimizing the ultrasound-assisted extraction of flavonoids from Moringa oleifera Leaves.

scholarly journals Deep Eutectic Solvent-Based Ultrahigh Pressure Extraction of Baicalin from Scutellaria baicalensis Georgi

Molecules ◽  
2018 ◽  
Vol 23 (12) ◽  
pp. 3233 ◽  
Author(s):  
Hui Wang ◽  
Xiaodi Ma ◽  
Qibin Cheng ◽  
Li Wang ◽  
Liwei Zhang
Keyword(s):  
Extraction Method ◽  
Choline Chloride ◽  
Maximum Yield ◽  
Extraction Yield ◽  
Scutellaria Baicalensis ◽  
Extraction Time ◽  
Ultrahigh Pressure ◽  
Scutellaria Baicalensis Georgi ◽  
Solid Ratio ◽  
Pressure Extraction

Deep eutectic solvents (DESs), promising green solvents, and ultrahigh pressure extraction (UPE) as an effective auxiliary extraction method, have attracted wide attention. In this study, DES was coupled with UPE to efficiently extract baicalin from Scutellaria baicalensis Georgi. First, choline chloride: lactic acid (ChCl-LA, molar ratio 1:1) was selected as the most appropriate DES by comparing the extraction yield of different DESs. Second, the extraction protocol was optimized by response surface methodology (RSM) considering the impacts of ChCl-LA concentration, extraction pressure, extraction time and liquid-solid ratio on the extraction yield. Under the optimal condition (40 vol% water content, extraction pressure of 400 MPa, extraction time of 4 min and a liquid-solid ratio of 110 mL/g), a maximum yield of 116.8 mg/g was achieved, higher than that obtained by the traditional extraction method. The microstructure of the raw and extracted Scutellaria baicalensis Georgi samples according to scanning electron microscope (SEM) images revealed that the dissolution of chemical components was enhanced from the disrupted root tissues after DESs-UPE. DESs coupled with UPE could effectively extract the baicalin from Scutellaria baicalensis Georgi as a rapid and efficient extraction method.

Optimization of Ultrasonic-Assisted Extraction of Flavonols and Anthocyanins from Blueberry Using RSM

2012 ◽  
Vol 468-471 ◽  
pp. 2423-2430 ◽  
Author(s):  
Yao Tian ◽  
Yu Yang ◽  
Ping Gao ◽  
Jin Hong Wang ◽  
Ya Qin Xu ◽  
...  
Keyword(s):  
Response Surface Methodology ◽  
Extraction Time ◽  
Ultrasonic Power ◽  
Experimental Conditions ◽  
Independent Variables ◽  
Solid Ratio ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction ◽  
Predicted Values

Ultrasonic-assisted extraction (UAE) method was developed for continued extraction of flavonols and anthocyanins from Blueberry. Response surface methodology (RSM) was employed to optimize experimental conditions for extraction of flavonols and anthocyanins. Three major independent variables such as ultrasonic power (W), extraction time (min), liquid to solid ratio (mL/g) were studied. The optimal extraction conditions of flavonols and anthocyanins were determined as follows: ultrasonic power 512.7 W, extraction time 29.8 min, liquid to solid ratio 9.5:1 mL /g. Under a modified condition (ultrasonic power 510W, extraction time 30 min, liquid to solid ratio 10:1 mL /g), the experimental yields of flavonols and anthocyanins were 0.806mg/g and 2.903mg/g respectively, which were agreed closely with the predicted values (0.804mg/g and 2.899mg/g).

scholarly journals Optimization of Ultrasonic-Assisted Enzymatic Extraction of Tannic Acid from Chromolaena Odorota sp.

2021 ◽  
Vol 2129 (1) ◽  
pp. 012081
Author(s):  
AAA Kamal ◽  
M Mohamad ◽  
KA Sulaiman ◽  
NA Mohidem ◽  
NF Shoparwe ◽  
...  
Keyword(s):  
Tannic Acid ◽  
Duty Cycle ◽  
Extraction Method ◽  
Extraction Process ◽  
Enzyme Concentration ◽  
Extraction Time ◽  
Sonication Time ◽  
Chromolaena Odorata ◽  
Enzymatic Extraction ◽  
Ultrasonic Assisted

Abstract Previous study only implemented the time consuming and low amount of yield technique for extraction from Chromolaena odorata which is conventional method. Nonconventional extraction method with short extraction time and high amount of yield was applied in this study by applying ultrasound-assisted enzymatic extraction (UAEE). UAEE was used to extract tannic acid from Chromolaena odorata. The extraction parameters involved were enzyme concentration, sonication time and duty cycle at constant temperature of 50°C, solid to liquid ratio of 1:10 and sonication power at 60% amplitude. The optimum extraction process was found at cellulase enzyme concentration of 4%, sonication time of 60 minutes and duty cycle of 50% with the obtained concentration of tannic acid at 1.6152 mg/mL. The study showed that the UAEE could be employed to enhance yield of tannic acid, reduce the extraction time and ensuring green extraction method were applied in the study.

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