Controlling the Ferrite/Austenite Phase Balance of SAF 2707HD Hyperduplex Stainless Steel Weldment

2013 ◽  
Vol 748 ◽  
pp. 138-143
Author(s):  
Muhammad Anis ◽  
Rini Riastuti ◽  
Permana Hariansyah ◽  
Mohammad Fadli ◽  
Fisca Sunandar Arif ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Weld Metal ◽  
Stainless Steels ◽  
Heat Input ◽  
Volume Fraction ◽  
Nitrogen Addition ◽  
Limited Range ◽  
Austenite Phase ◽  
Shielding Gas ◽  
Phase Balance

Hyperduplex, as a new class of duplex stainless steels, having high Cr and Mo present excellent combination of mechanical and corrosion resistance, due to their strict composition control and ferrite/austenite phase balance. This balance may, however, be disturbed during welding in both the weld metal and the Heat Affected Zone (HAZ) due to the rapid cooling rates. Those may lead to loss of the good corrosion and mechanical properties of the weldments. The present investigation is to establish the effect of heat input and the nitrogen addition in the argon shielding gas, for controlling the microstructure of hyperduplex stainless steels welded by the Gas Tungsten Arc Welding (GTAW) technique autogeneously. Hyperduplex stainless steel in the form of tube having outside diameter of 32 mm and thickness of 2 mm, was welded using limited range of heat input to control the microstructure in the HAZ, and using the nitrogen addition of 2-5% into argon shielding gas to control the ferrite/austenite phase balance of the weld metal. The microstructure of the weldment was examined by calculating the volume fraction of ferrite and austenite phases. The result shows that the heat input of 0,6 kJ/mm gives the optimum ferrite/austenite phase balance in the HAZ. The addition of 2% nitrogen into argon shielding gas is recommended to give the optimum balance of ferrite/austenite phases in weld metal in addition to the heat input employed. The heat input higher than 0,6 kJ/mm promoted sigma phase at the HAZ as well as at the weld metal particularly when welded with addition of more than 2% nitrogen in the argon shielding gas.

Influence of Argon-Nitrogen Gas to Balance the Microstructure in the Welding of Super Duplex Stainless Steel

2016 ◽  
Vol 836 ◽  
pp. 165-172
Author(s):  
Suheni
Keyword(s):  
Stainless Steel ◽  
Weld Metal ◽  
Duplex Stainless Steel ◽  
Heat Input ◽  
Oil And Gas ◽  
Austenite Phase ◽  
Super Duplex Stainless Steel ◽  
Shielding Gas ◽  
Input Variables ◽  
Protective Gas

Super duplex stainless steel is steel that has a corrosion resistance and good mechanical strength so that used in industry especially in oil and gas and petrochemical industry. In use in the field is often used for the connection process by welding methods. To produce good welds, it should be noted that the welding procedures and parameters used , especially the heat input. In this study is used the heat input variables shielding gas composition to determine how much influence on the balance of ferrite - austenite phase structure in the weld stainless steels SAF 2507 super duplex with tungsten inert gas welding method (TIG). Heat input varied by applying different welding speed 1,3,4 and 5 mm /sec while the shielding gas is used 100 % argon, 98 % argon + 2 % nitrogen and 95 % argon + 5 % nitrogen. The result showed that at different welding speeds generated depth and width of the weld metal which is different. Likewise the use of protective gas will produce a different ratio wide and deep of weld metal which is different. By using protective gas 95 % argon + 5 % nitrogen squeak - ausenit phase, resulting in weld metal that is relatively balanced than others. On a slow welding in addition to produce a large heat input also produces weld metal hardness at high and affect the growth of the austenite phase. The higher the heat input ( 2,280 kJ / mm ) , the lower the austenite phase in the weld metal.

Structure and mechanical properties of laser-MIG hybrid welded SAF 2507 super duplex stainless steel joints

2019 ◽  
Vol 33 (01n03) ◽  
pp. 1940037 ◽  
Author(s):  
Kai Qi ◽  
Ruifeng Li ◽  
Guangjin Wang ◽  
Zhe Sun
Keyword(s):  
Mechanical Properties ◽  
Stainless Steel ◽  
Weld Metal ◽  
Duplex Stainless Steel ◽  
Phase Distribution ◽  
Welding Process ◽  
Austenite Phase ◽  
Welding Parameters ◽  
Super Duplex Stainless Steel ◽  
Phase Balance

Joining of super duplex stainless steel (SDSS) is still a challenge, in particular, the need to control the phase balance in the weld metal. In this paper, laser-MIG hybrid welding process was used to join SAF 2507 SDSS plates. The effects of welding parameters on weld appearance, microstructure and phase distribution and mechanical properties were studied systematically. Results showed that the arc/laser hybrid effect was more significant when the arc led the laser with 2 mm distance. It was indicated that arc current mainly affected the weld width while laser power mainly affected weld penetration depth. The composition and microstructure varied a lot at different positions in the weld due to the differences in peak temperature and cooling rate. From top to root, the content of ferrite phase increased and austenite phase decreased. With optimized welding parameters, due to the increase of heat input and the introduction of welding wire, the ferrite/austenite phase balance in the weld metal was obtained. Mechanical property tests showed that the joints exhibited higher tensile strength but lower toughness compared to base metal.

scholarly journals Physical and Theoretical Modeling of the Nitrogen Content of Duplex Stainless Steel Weld Metal: Shielding Gas Composition and Heat Input Effects

Metals ◽  
2019 ◽  
Vol 9 (7) ◽  
pp. 762 ◽  
Author(s):  
Balázs Varbai ◽  
Kornél Májlinger
Keyword(s):  
Weld Metal ◽  
Nitrogen Content ◽  
Heat Input ◽  
Large Scale ◽  
Nitrogen Addition ◽  
Industrial Applications ◽  
Gas Composition ◽  
Shielding Gas ◽  
Corrosion Properties ◽  
Dissolved Nitrogen

Duplex stainless steels (DSSs) are gaining more and more attention in corrosion-resistant applications and also in the transport and automotive industry. The outstanding mechanical and corrosion properties of DSSs highly depends on the austenite-to-ferrite phase balance (A/F). This phase ratio can shift in a large scale during welding. Thus, the heat input and the shielding gas composition should be optimized. Nitrogen addition to argon shielding is frequently used in DSS welding, because it is a potent austenite former. The dissolved nitrogen content in the heat-affected zone and the weld metal (WM) predetermines the A/F. To determine the effect of heat input and nitrogen content in shielding gas, two different heat inputs and six different gas compositions were used in autogenous tungsten inert gas welding. An improved theoretical model was established in order to simulate the WM dissolved nitrogen content, which calculates it with less error than the initial models. The correlation between nitrogen content and arc voltage was also determined. This improved model delivers the basics for shielding gas selection and the subsequent weld design for optimal A/F for industrial applications.

scholarly journals Surface Modification of a Nickel-Free Austenitic Stainless Steel by Low-Temperature Nitriding

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1845
Author(s):  
Francesca Borgioli ◽  
Emanuele Galvanetto ◽  
Tiberio Bacci
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Austenitic Stainless Steel ◽  
Low Temperature ◽  
Stainless Steels ◽  
Volume Fraction ◽  
Surface Hardness ◽  
Austenitic Stainless Steels ◽  
Surface Layers ◽  
Modified Surface

Low-temperature nitriding allows to improve surface hardening of austenitic stainless steels, maintaining or even increasing their corrosion resistance. The treatment conditions to be used in order to avoid the precipitation of large amounts of nitrides are strictly related to alloy composition. When nickel is substituted by manganese as an austenite forming element, the production of nitride-free modified surface layers becomes a challenge, since manganese is a nitride forming element while nickel is not. In this study, the effects of nitriding conditions on the characteristics of the modified surface layers obtained on an austenitic stainless steel having a high manganese content and a negligible nickel one, a so-called nickel-free austenitic stainless steel, were investigated. Microstructure, phase composition, surface microhardness, and corrosion behavior in 5% NaCl were evaluated. The obtained results suggest that the precipitation of a large volume fraction of nitrides can be avoided using treatment temperatures lower than those usually employed for nickel-containing austenitic stainless steels. Nitriding at 360 and 380 °C for duration up to 5 h allows to produce modified surface layers, consisting mainly of the so-called expanded austenite or gN, which increase surface hardness in comparison with the untreated steel. Using selected conditions, corrosion resistance can also be significantly improved.

Effect of Ar-N2 Mixed Gas on Morphology and Microstructure of Type 316L Stainless Steel TIG Weld Metal

2011 ◽  
Vol 295-297 ◽  
pp. 1919-1924 ◽  
Author(s):  
Kuang Hung Tseng ◽  
Kai Chieh Hsien
Keyword(s):  
Stainless Steel ◽  
Weld Metal ◽  
316L Stainless Steel ◽  
Welding Process ◽  
Ferrite Content ◽  
Shielding Gas ◽  
Mixed Gas ◽  
Nitrogen Gas ◽  
Type 316L ◽  
Type 316L Stainless Steel

The aim of the present work was to investigate the effects of specific nitrogen gas additions to argon shielding gas on morphology and microstructure of austenitic stainless steel TIG welds. An autogenous TIG welding process was applied on type 316L stainless steel to produce a bead-on-plate weld. The ferrite content of weld metal was measured using a Feritscope. The results indicated that the arc voltage increase as the amount of nitrogen gas added to the argon atmosphere increases. The retained ferrite content of type 316L stainless steel TIG weld metal decreased rapidly as nitrogen gas addition to the argon shielding gas was increased.

High Heat Input Welding of 12Cr-6Ni-2.5Mo Supermartensitic Stainless Steel

2003 ◽  
Author(s):  
Ragnhild Aune ◽  
Hans Fostervoll ◽  
Odd Magne Akselsen
Keyword(s):  
Weld Metal ◽  
Stainless Steels ◽  
Heat Affected Zone ◽  
Heat Input ◽  
High Heat ◽  
Maximum Heat ◽  
Final Microstructure ◽  
Girth Welding ◽  
High Heat Input ◽  
Longitudinal Seam

In conventional welding of 13% Cr supermartensitic stainless steels, the normal microstructure that forms on cooling is martensite. Although high heat input tends to give a certain coarsening of the final microstructure, the eventual accompanying loss in toughness is not known. The present study was initiated to examine the effect of heat input on weld metal and heat affected zone mechanical properties of a 12Cr-6Ni-2.5Mo grade. The results obtained showed that the notch toughness is low (25 J) and independent of heat input for the weld metal, while it is reduced with increasing heat input for fusion line and the heat affected zone locations. Subsequent post weld heat treatment gave a substantial increase in toughness for all notch locations. Based on these results, indications are that a specified maximum heat input is not applicable in welding of supermartensitic stainless steels, allowing more production efficient techniques to be used, both in longitudinal seam and girth welding.

scholarly journals Microstructure of laser metal deposited duplex stainless steel: Influence of shielding gas and heat treatment

2020 ◽  
Author(s):  
Maria Asuncion Valiente Bermejo ◽  
Karthikeyan Thalavai Pandian ◽  
Björn Axelsson ◽  
Ebrahim Harati ◽  
Agnieszka Kisielewicz ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Duplex Stainless Steel ◽  
Nitrogen Loss ◽  
Steel Wire ◽  
Research Work ◽  
Shielding Gas ◽  
Austenite Content ◽  
Heat Treated ◽  
Phase Balance

AbstractThis research work is the first step in evaluating the feasibility of producing industrial components by using Laser Metal Deposition with duplex stainless steel Wire (LMDw). The influence of Ar and N2 shielding gases was investigated in terms of nitrogen loss and in the microstructure and austenite content of different deposited geometries. The evolution of the microstructure in the build-up direction of the Ar and N2-shielded blocks was compared in the heat-treated and as-deposited conditions. The susceptibility for oxygen pick-up in the LMDw deposits was also analyzed, and oxygen was found to be in the range of conventional gas-shielded weldments. Nitrogen loss occurred when Ar-shielding was used; however, the use of N2-shielding prevented nitrogen loss. Austenite content was nearly doubled by using N2-shielding instead of Ar-shielding. The heat treatment resulted in an increase of the austenite content and of the homogeneity in the microstructure regardless of the shielding gas used. The similarity in microstructure and the low spread in the phase balance for the as-deposited geometries is a sign of having achieved a stable and consistent LMDw process in order to proceed with the build-up of more complex geometries closer to industrial full-size components.

Effect of post-weld heat treatment on thermal diffusivity in UNS S32304 duplex stainless steel welds

2017 ◽  
Vol 2 (88) ◽  
pp. 49-58
Author(s):  
E.G. Betini ◽  
C.S. Mucsi ◽  
T.S. Luz ◽  
M.T.D. Orlando ◽  
M-N. Avettand-Fènoël ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Thermal Diffusivity ◽  
Duplex Stainless Steel ◽  
Welding Process ◽  
Austenite Phase ◽  
Shielding Gas ◽  
Heat Treated ◽  
Steel Welds ◽  
Weld Heat

Purpose: The thermal diffusivity variation of UNS S32304 duplex stainless steel welds was studied after pulsed GTA welding autogenous process without filler addition. This property was measured in the transverse section of thin plates after welding process and post-heat treated at 750°C for 8 h followed by air-cooling. Design/methodology/approach: The present work reports measurements of thermal diffusivity using the laser-flash method. The thermal cycles of welding were acquired during welding by means of k-type thermocouples in regions near the weld joint. The used shielding gas was pure argon and 98% argon plus 2% of nitrogen. The temperature profiles were obtained using a digital data acquisition system. Findings: It was found an increase of thermal diffusivity after welding process and a decrease of these values after the heat treatment regarding the solidified weld pool zone, irrespective of the welding protection atmosphere. The microstructure was characterized and an increase of austenite phase in the solidified and heat-affected zones was observed for post-weld heat-treated samples. Research limitations/implications: It suggests more investigation and new measurements about the influence of the shielding gas variation on thermal diffusivity in the heat-affected zone. Practical implications: The nuclear industry, especially, requests alloys with high thermal stability in pipes for power generation systems and safe transportation equipment’s for radioactive material. Thus, the duplex stainless steel grades have improved this stability over standard grades and potentially increase the upper service temperature reliability of the equipment. Originality/value: After heat treatment, the welded plate with 98%Ar plus 2%N2 as shielding gas presented a thermal diffusivity closer to the as received sample. By means of 2%-nitrogen addition in shielding gas during GTAW welding of duplex stainless steel may facilitate austenite phase reformation, and then promotes stability on the thermal diffusivity of duplex stainless steels alloys.

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