Effect of a New Coupling Agent on Mechanical Properties of Domestic High-Modulus Carbon Fiber/Cyanate Composites

2013 ◽  
Vol 873 ◽  
pp. 411-416
Author(s):  
Wei Qiang Chen ◽  
De Qun Peng ◽  
Wei Qin
Keyword(s):  
Mechanical Properties ◽  
Carbon Fiber ◽  
Coupling Agent ◽  
Interlaminar Shear Strength ◽  
Raw Material ◽  
Bend Strength ◽  
High Modulus ◽  
Overall Performance ◽  
Interlaminar Shear ◽  
Properties Of Composites

To improve the overall performance of the domestic high-modulus carbon fiber/cyanate composites, a macromolecular coupling agent (SCC) based on the raw material styrene, methyl acrylate and γ-methyl (acryloyl) trimethoxysilane was synthesized. It also studies the effect of coupling agent content on the mechanical properties of composites. The results show that the dosage of macromolecular coupling agent with 3%, the performance of the composite materials has been notable improved, its bend strength and interlaminar shear strength are 1100Mpa and 63.5Mpa, which has been raised 6.0% and 16.1%, respectively. SEM micrographs show that the addition of a coupling agent effectively improve the interface compatibility between the resin and fibers in composite.

Epoxy Modified Polyurethanes Coated High Modulus Carbon Fiber: Synthesis and Properties Studies

2011 ◽  
Vol 217-218 ◽  
pp. 728-733 ◽  
Author(s):  
Yan Hong Tian ◽  
Zhan Qing Liu ◽  
Su Mei Kang ◽  
Xue Jun Zhang
Keyword(s):  
Carbon Fiber ◽  
Raw Materials ◽  
Crosslinking Agent ◽  
Epoxy Composites ◽  
High Modulus ◽  
Coating Agent ◽  
Interlaminar Shear ◽  
Carbon Fiber Epoxy ◽  
Thermal Stability Of ◽  
Properties Of Composites

With toluene 2, 4-diisocyanate (TDI), polyethylene glycol (PEG) and 2,3-Epoxy-1-prop -anol (glycidol) used as the raw materials, two epoxy terminated polyurethanes (EPU) was synthesized by prepolymerization and closed end. Moreover, EPU with high toughhess is chosen as a coating agent for carbon fiber with three ethylene tetramine (TETA) as curing agen. The influence of the content of crosslinking agent in the coating layer on properties of composites and the mechanism of interface toughness are investigated. The chemical structure and thermal property of the EPU were studied with FTIR, 1HNMR and TGA, respectively. It proves that the thermal stability of EPU is more stable than epoxy coating. The interlaminar shear strength (ILSS) of the sized high modulus carbon fiber/epoxy composites is improved to 71MPa, which increased by 19.4% compared with the composites reinforced by unsized high modulus carbon fiber, and DMTA show that using EPU as a new kind of polymer coating for carbon fiber is a feasible method to improve the interfacial performance of high modulus carbon fiber/epoxy composites.

scholarly journals Effect of Graphene Additive on Flexural and Interlaminar Shear Strength Properties of Carbon Fiber-Reinforced Polymer Composite

2020 ◽  
Vol 4 (4) ◽  
pp. 162
Author(s):  
Mohamed Ali Charfi ◽  
Ronan Mathieu ◽  
Jean-François Chatelain ◽  
Claudiane Ouellet-Plamondon ◽  
Gilbert Lebrun
Keyword(s):  
Mechanical Properties ◽  
Shear Strength ◽  
Carbon Fiber ◽  
Flexural Strength ◽  
Interlaminar Shear Strength ◽  
Fiber Reinforced Polymer ◽  
Carbon Fiber Reinforced Polymer ◽  
Adhesion Properties ◽  
Reinforced Polymer ◽  
Interlaminar Shear

Composite materials are widely used in various manufacturing fields from aeronautic and aerospace industries to the automotive industry. This is due to their outstanding mechanical properties with respect to their light weight. However, some studies showed that the major flaws of these materials are located at the fiber/matrix interface. Therefore, enhancing matrix adhesion properties could significantly improve the overall material characteristics. This study aims to analyze the effect of graphene particles on the adhesion properties of carbon fiber-reinforced polymer (CFRP) through interlaminar shear strength (ILSS) and flexural testing. Seven modified epoxy resins were prepared with different graphene contents. The CFRP laminates were next manufactured using a method that guarantees a repeatable and consistent fiber volume fraction with a low porosity level. Short beam shear and flexural tests were performed to compare the effect of graphene on the mechanical properties of the different laminates. It was found that 0.25 wt.% of graphene filler enhanced the flexural strength by 5%, whilst the higher concentrations (2 and 3 wt.%) decreased the flexural strength by about 7%. Regarding the ILSS, samples with low concentrations (0.25 and 0.5 wt.%) demonstrated a decent increase. Meanwhile, 3 wt.% slightly decreases the ILSS.

Effect of Ozone Treatment on the Interfacial Properties of High Modulus Carbon Fiber/Epoxy Composites

2007 ◽  
Vol 546-549 ◽  
pp. 1547-1550 ◽  
Author(s):  
Xiao Jin Zhao ◽  
Wei Qin ◽  
Ben Li Wang
Keyword(s):  
Shear Strength ◽  
Carbon Fiber ◽  
Fiber Surface ◽  
Interlaminar Shear Strength ◽  
Epoxy Composites ◽  
Ozone Treatment ◽  
High Modulus ◽  
Surface Impregnation ◽  
Interlaminar Shear ◽  
Carbon Fiber Epoxy

High modulus carbon/epoxy composites have been attached more and more importance in the aeronautic field. Because chemical inert of high modulus carbon fiber surface and its poor impregnation for resin, it is essential to improve its polarity in order to enhance the interfacial performances of high modulus carbon/epoxy composites. In this paper, high modulus carbon fiber was treated by ozone oxidation method to modify its surfacial properties. AFM and SEM were used to observe the surface of the carbon fiber, as well as interlaminar shear strength of high modulus carbon fiber/epoxy composite was tested. The impregnation and the interfacial performances of the high modulus carbon/epoxy composites were studied. The results show that after ozone treatment, the surface impregnation of high modulus carbon fiber and the interlaminar shear strength property of high modulus carbon/epoxy composites can be improved obviously.

Mechanical properties of multiwall carbon nanotubes/unidirectional carbon fiber-reinforced epoxy hybrid nanocomposites in transverse and longitudinal fiber directions

2021 ◽  
pp. 096739112098651
Author(s):  
Saeedeh Saadatyar ◽  
Mohammad Hosain Beheshty ◽  
Razi Sahraeian
Keyword(s):  
Mechanical Properties ◽  
Shear Strength ◽  
Epoxy Resin ◽  
Interlaminar Shear Strength ◽  
Lap Shear Strength ◽  
Transverse Tensile ◽  
Lap Shear ◽  
Longitudinal Fiber ◽  
Interlaminar Shear ◽  
Multiwall Carbon

Unidirectional carbon fiber-reinforced epoxy (UCFRE) is suffering from weak transverse mechanical properties and through-thickness properties. The effect of different amount (0.1, 0.3 and 0.5 phr which is proportional to 0.09, 0.27 and 0.46 wt%, respectively) of multiwall carbon nanotube (MWCNT), on transverse tensile properties, flexural strength, fracture toughness in transverse and longitudinal fiber directions, interlaminar shear strength and lap shear strength of UCFRE has been investigated. Dicyandiamide was used as a thermal curing agent of epoxy resin. MWCNT was dispersed in the epoxy resin by ultrasonic instrument and their dispersion state was investigated by scanning electron microscopy (SEM). The curing behavior of epoxy resin and its nanocomposites was assessed by differential scanning calorimetry. Results show that transverse tensile strength, modulus and strain-at-break were increased by 28.5%, 25% and 14%, respectively by adding 0.1 phr of MWCNT. Longitudinal flexural properties of UCFRE was not changed by adding different amount of MWCNT. Although longitudinal flexural strength was increased by 5% by adding 0.1 phr of MWCNT. Fracture toughness in transverse and longitudinal fiber directions was increased by 39% and 9%, respectively at 0.3 phr of MWCNT. Results also show that interlaminar shear strength and lap shear strength were increased at 0.3 phr of MWCNT by 8% and 5%, respectively. These increases in mechanical properties were due to the good adhesion of fibers to the matrix, interlocking and toughening action of MWCNT as revealed by SEM.

Surface and Composite Interface of Carbon Fiber Modified by Grafting of Diethanolamine

2009 ◽  
Vol 79-82 ◽  
pp. 497-500 ◽  
Author(s):  
Lei Chen ◽  
Zhi Wei Xu ◽  
Jia Lu Li ◽  
Xiao Qing Wu ◽  
Li Chen
Keyword(s):  
Shear Strength ◽  
Carbon Fiber ◽  
Functional Groups ◽  
Carbon Fibers ◽  
Irradiation Dose ◽  
Interlaminar Shear Strength ◽  
Epoxy Composites ◽  
Composite Interface ◽  
Γ Ray ◽  
Interlaminar Shear

The γ-ray co-irradiation method was employed to study the effect of diethanolamine modification on the surface of carbon fiber (CF) and the interfacial properties of CF/epoxy composites. Compared with the original carbon fiber, the surface of modified fibers became rougher. The amount of oxygen-containing functional groups was increased and the nitrogen element was detected after irradiation grafting. The interlaminar shear strength (ILSS) of composites reinforced by carbon fibers irradiated in diethanolamine solution was increased and then decreased as the irradiation dose increased. The ILSS of CF/epoxy composites was enhanced by 16.1% at 200kGy dose, compared with that of untreated one. The γ-ray irradiation grafting is expected to be a promising method for the industrialized modification of carbon fibers.

scholarly journals Mechanical properties of Gelatin –Hydroxyapatite composite for bone tissue engineering

2015 ◽  
Vol 50 (1) ◽  
pp. 15-20 ◽  
Author(s):  
MJ Hossan ◽  
MA Gafur ◽  
MM Karim ◽  
AA Rana
Keyword(s):  
Mechanical Properties ◽  
Bone Tissue ◽  
Composite Scaffold ◽  
Testing Machine ◽  
Casting Process ◽  
Raw Material ◽  
Potential Candidate ◽  
Oven Drying ◽  
Hydroxyapatite Composite ◽  
Properties Of Composites

In this study, hydroxyapatite (HAp) and gelatin (GEL) scaffolds were prepared to mimic the mineral and organic component of natural bone. The raw material was first compounded and resulting composite were molded into the petridishes. Using Solvent casting process, it is possible to produce scaffolds with mechanical and structural properties close to natural trabecular bone.The mechanical properties of composites were investigated by Thermo-mechanical analyzer (TMA), Vickers microhardness tester, Universal testing machine. It was observed that the composite has maximum tensile strength of 37.13MPa ( oven drying) and % elongation of 7.68 (Oven drying) and 2.04 (Natural drying) at 15% of Hap respectively. These results demonstrate that the prepared composite scaffold is a potential candidate for bone tissue engineering.Bangladesh J. Sci. Ind. Res. 50(1), 15-20, 2015

Microstructure optimizations for improving interlaminar shear strength and self-healing efficiency of spread carbon fiber/epoxy laminates containing microcapsules

2020 ◽  
Vol 55 (1) ◽  
pp. 27-38
Author(s):  
Yasuka Nassho ◽  
Kazuaki Sanada
Keyword(s):  
Shear Strength ◽  
Carbon Fiber ◽  
Optical Microscope ◽  
Interlaminar Shear Strength ◽  
Self Healing ◽  
Short Beam ◽  
Healing Efficiency ◽  
Beam Shear ◽  
Interlaminar Shear ◽  
Carbon Fiber Epoxy

The purpose of this study is to improve interlaminar shear strength and self-healing efficiency of spread carbon fiber (SCF)/epoxy (EP) laminates containing microcapsules. Microencapsulated healing agents were embedded within the laminates to impart a self-healing functionality. Self-healing was demonstrated on short beam shear specimens, and the healing efficiency was evaluated by strain energies of virgin and healed specimens. The effects of microcapsule concentration and diameter on apparent interlaminar shear strength and healing efficiency were discussed. Moreover, damaged areas after short beam shear tests were examined by an optical microscope to investigate the relation between the microstructure and the healing efficiency of the laminates. The results showed that the stiffness and the apparent interlaminar shear strength of the laminates increased as the microcapsule concentration and diameter decreased. However, the healing efficiency decreased with decreasing the microcapsule concentration and diameter.

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