Thirty Years of Superplastic Ultrafine-Grained Materials: Examining the Legacy of Oscar Kaibyshev

2018 ◽  
Vol 385 ◽  
pp. 3-8 ◽  
Author(s):  
Terence G. Langdon

The occurrence of superplasticity may be traced to the classic work of Pearson conducted in the U.K. in 1934 when an elongation of 1950% was reported in a Pb-Sn eutectic alloy. Subsequently, much attention in Russia was devoted to this scientific curiosity and this led to the first book on superplasticity written by Prof. A.A. Presnyakov and published in 1964. Later, in 1985, Oscar Kaibyshev established in Ufa the Institute of Problems of Superplasticity of Metals of the Russian Academy of Sciences and this was, and remains to this day, the only institute in the world devoted exclusively to studies of the phenomenon of superplastic flow and the development through superplastic forming of complex-shaped parts. An important development occurred in 1988 with the publication of a classic report by Kaibyshev and co-workers describing the potential for achieving low temperature superplasticity in a metallic Al-Cu-Zr alloy that had been specially processed by severe plastic deformation (SPD) to produce a remarkably small grain size of only 300 nm. This report formed the basis for the later development of SPD processing as a major tool for the production of exceptional grain refinement and as a procedure for achieving large superplastic elongations that cannot be achieved using more conventional processing. This report describes this early work, the subsequent developments and the modern status of superplastic flow in ultrafine-grained metals.

2008 ◽  
Vol 604-605 ◽  
pp. 97-111 ◽  
Author(s):  
Roberto B. Figueiredo ◽  
Megumi Kawasaki ◽  
Terence G. Langdon

Processing through the application of severe plastic deformation (SPD) provides an opportunity for achieving very significant grain refinement in bulk metals. Since the occurrence of superplastic flow generally requires a grain size smaller than ~10 µm, it is reasonable to anticipate that materials processed by SPD will exhibit superplastic ductilities when pulled in tension at elevated temperatures. This paper summarizes the fundamental principles of SPD processing and describes recent results demonstrating the occurrence of exceptional superplastic flow in these ultrafine-grained materials.


2006 ◽  
Vol 114 ◽  
pp. 7-18 ◽  
Author(s):  
Ruslan Valiev

During the last decade severe plastic deformation (SPD) has become a widely known method of materials processing used for fabrication of ultrafine-grained materials with attractive properties. Nowadays SPD processing is rapidly developing and is on the verge of a transition from lab-scale research to commercial production. This paper focuses on several new trends in the development of SPD techniques for effective grain refinement, including those for commercial alloys and presents new SPD processing routes to produce bulk nanocrystalline materials.


2007 ◽  
Vol 558-559 ◽  
pp. 1283-1294 ◽  
Author(s):  
Cheng Xu ◽  
Z. Horita ◽  
Terence G. Langdon

It is now well-established that processing through the application of severe plastic deformation (SPD) leads to a significant reduction in the grain size of a wide range of metallic materials. This paper examines the fabrication of ultrafine-grained materials using high-pressure torsion (HPT) where this process is attractive because it leads to exceptional grain refinement with grain sizes that often lie in the nanometer or submicrometer ranges. Two aspects of HPT are examined. First, processing by HPT is usually confined to samples in the form of very thin disks but recent experiments demonstrate the potential for extending HPT also to bulk samples. Second, since the strains imposed in HPT vary with the distance from the center of the disk, it is important to examine the development of inhomogeneities in disk samples processed by HPT.


Author(s):  
Mihaela Banu ◽  
Mitica Afteni ◽  
Alexandru Epureanu ◽  
Valentin Tabacaru

There are several severe plastic deformation processes that transform the material from microsized grains to the nanosized grains under large deformations. The grain size of a macrostructure is generally 300 μm. Following severe plastic deformation it can be reached a grain size of 200 nm and even less up to 50 nm. These structures are called ultrafine grained materials with nanostructured organization of the grains. There are severe plastic deformation processes like equal angular channel, high pressure torsion which lead to a 200 nm grain size, respectively 100 nm grain size. Basically, these processes have a common point namely to act on the original sized material so that an extreme deformation to be produced. The severe plastic deformation processes developed until now are empirically-based and the modeling of them requires more understanding of how the materials deform. The macrostructural material models do not fit the behavior of the nanostructured materials exhibiting simultaneously high strength and ductility. The existent material laws need developments which consider multi-scale analysis. In this context, the present paper presents a laboratory method to obtain ultrafine grains of an aluminum alloy (Al-Mg) that allows the microstructure observations and furthermore the identification of the stress–strain response under loadings. The work is divided into (i) processing of the ultrafine-grained aluminum alloy using a laboratory-scale process named in-plane controlled multidirectional shearing process, (ii) crystallographic analysis of the obtained material structure, (iii) tensile testing of the ultrafine-grained aluminum specimens for obtaining the true stress-strain behavior. Thus, the microscale phenomena are explained with respect to the external loads applied to the aluminum alloy. The proposed multi-scale analysis gives an accurate prediction of the mechanical behavior of the ultrafine-grained materials that can be further applied to finite element modeling of the microforming processes.


2012 ◽  
Vol 05 ◽  
pp. 299-306
Author(s):  
TERENCE G. LANGDON

Processing through the application of severe plastic deformation (SPD) provides a very attractive tool for the production of bulk ultrafine-grained materials. These materials typically have grain sizes in the submicrometer or nanometer ranges and they exhibit high strength at ambient temperature and, if the ultrafine grains are reasonably stable at elevated temperatures, they have a potential for use in superplastic forming operations. Several procedures are now available for applying SPD to metal samples but the most promising are Equal-Channel Angular Pressing (ECAP) and High-Pressure Torsion (HPT). This paper examines the basic principles of ECAP and HPT and describes some of the properties that may be achieved using these processing techniques.


2018 ◽  
Vol 54 (1) ◽  
pp. 46-55 ◽  
Author(s):  
Megumi Kawasaki ◽  
Terence G. Langdon

Abstract Superplasticity refers to the ability of a polycrystalline solid to exhibit a high elongation, of at least 400% or more, when testing in tension. The basic characteristics of superplastic flow are now understood and a theoretical model is available to describe the flow process both in conventional superplastic materials where the grain sizes are a few micrometers and in ultrafinegrained materials processed by severe plastic deformation where the grain sizes are in the submicrometer range. This report describes the basic characteristics of superplastic metals, gives examples of flow in ultrafine-grained materials, demonstrates the use of deformation mechanism mapping for providing a visual display of the flow processes and provides a direct comparison with the conventional model for superplastic flow. The report also describes the potential for using nanoindentation to obtain detailed information on the flow properties using only exceptionally small samples.


2015 ◽  
Vol 5 ◽  
pp. 111-126
Author(s):  
Evgeny V. Naydenkin ◽  
Galina P. Grabovetskaya ◽  
I.P. Mishin

Experimental studies on the grain boundary diffusion and processes controlled by it in the ultrafine-grained metallic materials produced by various methods of severe plastic deformation are reviewed. Correlation between the increased diffusion permeability of grain boundaries and features of recrystallization and deformation development in these materials possessing the non-equilibrium state of grain boundaries formed during severe plastic deformation in the temperature range of T < 0.35Tm is demonstrated and analyzed.


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