Influence of the Mineralogical and Mortar Components on the Adherence of Some “Granites”

2013 ◽  
Vol 548 ◽  
pp. 267-274 ◽  
Author(s):  
Lizandra Nogami ◽  
Antenor B. Paraguassú ◽  
José E. Rodrigues ◽  
Rogério P. Ribeiro

Rock plate setting can be performed with metal inserts or by mortar adhesion. For mortar setting, the adhesion bond strength values, as a rule, should be above 1 MPa. In the present work, tests with eight types of “granite” tiles were performed to compare the adherence of five types of mortars. The rocks chosen were: Red Brasilia (syenogranite), Black Indian (migmatite), Green Labrador (charnockite), Black Sao Gabriel (hypersthene diorite), Rose Jacaranda (nebulitic migmatite syenogranite), Fantastic Blue (biotite monzogranite megaporphyritic serial gneissified), Grey Swallow (monzogranite) and Yellow Ornamental (garnet porphyroblastic gneiss), which do not have similar petrographic and sawability characteristics, thereby resulting in different initial roughness values of the plates obtained by breaking apart the blocks on the gangsaw machine, which use granulated steel as an abrasive element. The adherence of these rocks with the mortars was determined in the rough surface as well as in the polished surface by the pullout traction test, standardized for ceramics. The results showed that the mortar adhesion is related to roughness, to mineralogy and to the texture of these rocks. To verify this relationship, tensile bond strength tests were performed with the main mineral components of these rocks using single crystals with known optical orientation. Moreover, the microstructure study of the standard substrate/mortar/rock set was also performed.

Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4174
Author(s):  
André M. Santos ◽  
Ângelo J. Costa e Silva ◽  
João M. F. Mota ◽  
João M. P. Q. Delgado ◽  
Fernando A. N. Silva ◽  
...  

The understanding of the mechanical fixation behavior of coatings is crucial for a better comprehension of the bonding systems, especially at the interface between the mortar and the substrate. Physical adherence is related, among other things, to the contents of the materials used in the roughcast and mortar coatings, due to the colloidal water penetration into the pores of the substrate. This work evaluated the influence of different lime solution additions replacing the kneading water in the preparation of roughcast and mortar coatings. Two types of substrates were investigated:ceramic bricks and concrete blocks. Three wall masonry panels were constructed, with dimensions of 220 × 180 cm2, one of concrete block and two of ceramic bricks, followed by the application of roughcast and mortar coating with an average thickness of 5 mm and 20 mm, respectively. Direct tensile bond strength tests were performed and the results, with a 95% confidence level, showed that substrate ceramic and treatment in the roughcast exhibited a better behavior regarding the distribution of the tensile bond strength of the tested specimens. However, no significant differences of the amount of addition used (0%, 5%, 10% and 15%) on the tensile bond strength were observed.


2013 ◽  
Vol 8-9 ◽  
pp. 317-326
Author(s):  
Cosmin Sinescu ◽  
Adrian Manescu ◽  
Meda Lavinia Negrutiu ◽  
Mihai Rominu ◽  
Liviu Marşavina ◽  
...  

In orthodontics, the scientific interest regarding adhesion is focused on optimizing adherents: metallic or aesthetic bracket base conditioning, creating aesthetic brackets with improved mechanical properties, enamel conditioning and artificial surface conditioning (aesthetic veneers and crowns). In order to investigate the interfaces between adherents there are several invasive (destructive) methods such as tensile bond strength tests, shear bond strength tests and microleakage tests.


1985 ◽  
Vol 27 (1) ◽  
pp. 1-12
Author(s):  
Misaki ANZAI ◽  
Hideharu HIROSE ◽  
Takahiko IMAMURA ◽  
Tatsumasa TAKAHASHI ◽  
Masayoshi OHASHI

2007 ◽  
Vol 18 (1) ◽  
pp. 45-48 ◽  
Author(s):  
Paulo César G. Silva ◽  
Mariane Gonçalves ◽  
Telma N. do Nascimento ◽  
André Luiz B. Centola

This study evaluated the efficiency of air abrasion alone and associated with phosphoric acid etching on tensile bond strength of a single-bottle adhesive/indirect composite restorative system (Bond 1/Alert) to human enamel. Forty enamel surfaces from extracted human third molars were assigned to 4 groups (n= 10). Mach 4.1 (Kreativ Inc.) air abrasion equipment was used for 20 s. A special system of rod pairs aligned in a specific apparatus was used for tensile strength tests, according to ISO/TR 11405 standard (1994) with some modifications. Bond strength means were: G1 (air abrasion + rinsing + condensable composite resin Alert) = 3.46 ± 0.83 MPa; G2 (air abrasion + rinsing + Bond 1 adhesive system + Alert) = 4.00 ± 1.60 MPa; G3 (air abrasion + rinsing + 37% phosphoric acid + rinsing + Bond 1 + Alert) = 20.80 ± 3.95 MPa; and G4 (37% phosphoric acid + rinsing + Bond 1 + Alert) = 17.00 ± 2.74 MPa. The statistical analysis by Kruskal-Wallis test revealed that G1 and G2 presented statistically significant difference (p< 0.05) from G3 and G4 (p<0.01) and G1 and G3 did not differ significantly (p> 0.05) from G2 and G4, respectively.


2020 ◽  
Vol 10 (2) ◽  
pp. 36-43
Author(s):  
Gregor Herrmann ◽  
Susanne Reimann ◽  
Nikolaos Daratsianos ◽  
Anna Weber ◽  
Ludger Keilig ◽  
...  

Aim: The repair of restorations is an eligible method to extend the survival rates of intraoral restorations. There is a consensus that the old surface has to be removed before repair by the use of a sandblaster or rotating instruments. This study aimed to investigate whether a glycine powder can be used successfully in composite repair by measurement of shear and tensile bond strength according to dental standards. Methodology: The influence of mechanical preparation by no powder, 25 µm glycine powder or 50 µm aluminium-oxide powder and chemical conditioning by the use of bonding, phosphoric acid and bonding or bonding, phosphoric acid and a silane on the repair bond strength of an artificially aged nano-hybrid composite was tested according to the guidelines of DIN 13990 (2017), ISO 29022 (2013) and ISO/TS 11405 (2015). The fracture modes were evaluated by adhesive, cohesive or mixed failures. Results: There was no significant difference in the performance of the different mechanical and chemical treatments. The shear bond test according to DIN 13990 (2017) produces higher repair bond strengths (26.0±8.9 MPa) than the test described in ISO 29022 (17.9±6.3 MPa). The tensile bond strength according to ISO/TS 11405 (6.9±1.8 MPa) was the lowest. Most adhesive failures occurred with the shear test according to ISO 29022 (41%), followed by DIN 13990 (18%) and the tensile test (4%). Conclusion: For evaluating the bond strength of composites the test described in ISO 29022 is recommended, because it produces the highest percentage of adhesive failures. Nano-hybrid-composites are robust to different repair protocols.   How to cite this article: Herrmann GP, Reimann S, Daratsianos N, Weber A, Keilig L, Nadal J, Bourauel C. Comparison of different standardized bond strength tests and the influence of glycine powder treatment in composite resin repairs. Int Dent Res 2020;10(1):36-43. https://doi.org/10.5577/intdentres.2020.vol10.no2.2    Linguistic Revision: The English in this manuscript has been checked by at least two professional editors, both native speakers of English.


Author(s):  
M. Hibino ◽  
K. Irie ◽  
R. Autrata ◽  
P. schauer

Although powdered phosphor screens are usually used for scintillators of STEM, it has been found that the phosphor screen of appropriate thickness should be used depending on the accelerating voltage, in order to keep high detective quantum efficiency. 1 It has been also found that the variation in sensitivity, due to granularity of phosphor screens, makes the measurement of fine electron probe difficult and that the sensitivity reduces with electron irradiation specially at high voltages.In order to find out a preferable scintillator for STEM, single crystals of YAG (yttrium aluminum garnet), which are used for detecting secondary and backscattered electrons in SEM were investigated and compared with powdered phosphor screens, at the accelerating voltages of 100kV and 1 MV. A conventional electron detection system, consisting of scintillator, light guide and PMT (Hamamatsu Photonics R268) was used for measurements. Scintillators used are YAG single crystals of 1.0 to 3.2mm thicknesses (with surfaces matted for good interface to the light guide) and of 0.8mm thickness (with polished surface), and powdered P-46 phosphor screens of 0.07mm and 1.0mm thicknesses for 100kV and 1MV, respectively. Surfaces on electron-incidence side of all scintillators are coated with reflecting layers.


2014 ◽  
Vol 10 (1) ◽  
pp. 59-68
Author(s):  
H Afshar ◽  
M Ghandehari ◽  
S Amiri ◽  
Z Mirzayi ◽  
M Pourali ◽  
...  

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