Deviations of Microcrack during Propagation in Thin Films of Austenitic Steel and Accompanying Accommodative Processes

2014 ◽  
Vol 627 ◽  
pp. 297-300 ◽  
Author(s):  
Tamaz Eterashvili ◽  
T. Dzigrashvili ◽  
M. Vardosanidze
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Crack Propagation ◽  
Low Cycle Fatigue ◽  
Polycrystalline Sample ◽  
Crystallographic Analysis ◽  
Cycle Fatigue ◽  
Initial Direction ◽  
Slip Bands ◽  
Transmission Electron

The work deals with the transmission electron microscopy (TEM) study of thin films of chromium-nickel Х18Н10 steel. The films were prepared from bulk samples after low cycle fatigue (LCF) tests. Focus was made on the processes accompanying propagation of small microcracks. Particularly, the microstructure changes near the crack tip were analyzed in terms of accommodation processes taking place during crack propagation, such as formation of slip bands, twins etc. The authors conducted crystallographic analysis of the defects formed during crack propagation in correlation with the reasons of their initiation and homogenous length of the slip bands. Thus, the reasons of microcrack deviation from the initial direction were determined. The research has shown that the most convenient microstructure variables in the austenitic crystals of polycrystalline sample, affecting the microcrack deviation, are microstructure, crystallography and the homogenous length of slip bands.

scholarly journals Strengthening Mechanisms and Process Controls for Super Waspaloy

1981 ◽  
Author(s):  
W. H. Couts ◽  
R. R. Biederman
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Low Cycle Fatigue ◽  
Stress Rupture ◽  
Initial Structure ◽  
Cycle Fatigue ◽  
Strengthening Mechanisms ◽  
Transmission Electron ◽  
Dislocation Movement ◽  
Process Controls

Super Waspaloy is an empirically derived thermomechanically processed version of Waspaloy. Microstructures were evaluated at steps in the hammer forge and heat treat sequence to study how the initial structure is derived. Foils taken from hot tensile, stress rupture, and elevated temperature low cycle fatigue bars were examined by transmission electron microscopy after exposure to temperature and stress. The purpose was to discover the microstructural features resistant to dislocation movement and to seek clues for further improvement of the alloy.

Low-Cycle Fatigue Behavior of an Al-Mg-Si Alloy with and without a Small Addition of Sc

2010 ◽  
Vol 654-656 ◽  
pp. 938-941 ◽  
Author(s):  
Chihiro Watanabe ◽  
Ryoichi Monzen
Keyword(s):  
Low Cycle Fatigue ◽  
Fatigue Behavior ◽  
Cyclic Hardening ◽  
Cyclic Softening ◽  
Strengthening Effect ◽  
Cycle Fatigue ◽  
Slip Bands ◽  
Transmission Electron ◽  
Peak Aging ◽  
Bearing Alloy

Low-cycle fatigue behavior of a wrought Al-0.8wt%Mg-0.7wt%Si alloy with and without 0.27wt%Sc has been investigated at room temperature under constant plastic-strain amplitudes. After peak-aging treatments, both the alloys had fine lath-shaped β' precipitates. In the Sc-containing alloy, spherical Al3Sc precipitates of about 11 nm in diameter were co-existed. The alloy with Sc exhibited cyclic hardening to saturation, while the alloy without Sc showed clear cyclic softening after initial hardening. Transmission electron microscopy observation revealed that slip band structures were developed in the Sc-free alloy. Within the slip bands, shearing of the β' precipitates by moving dislocations was often observed. The cyclic softening in the alloy without Sc can then be explained by a loss of precipitation strengthening effect through the precipitation destruction within strongly-strained slip bands. In the Sc-bearing alloy, owing to the existence of non-shearable Al3Sc precipitates, dislocations were uniformly distributed, resulting in the absence of the cyclic softening.

Dislocation Clusters and Microcracks in Thin Films of LCF-Tested Austenitic Steel

2013 ◽  
Vol 577-578 ◽  
pp. 237-240 ◽  
Author(s):  
Tamaz Eterashvili ◽  
T. Dzigrashvili ◽  
M. Vardosanidze
Keyword(s):  
Thin Films ◽  
Stainless Steel ◽  
Austenitic Steel ◽  
Low Cycle Fatigue ◽  
Cycle Fatigue ◽  
Slip Bands ◽  
Microcrack Propagation ◽  
Theoretical Assumptions ◽  
Microcrack Formation ◽  
Cylindrical Samples

Austenitic chromium-nickel stainless steel CrNiNb 18-10 was studied using TEM technique. Characterizations of thin films prepared from bulk cylindrical samples after low-cycle fatigue (LCF) tests were conducted. Focus was made on the dislocation clusters, slip bands, defects and microstructure changes taking place in the steel during LCF. It is shown that microcracks occur in slip bands. Stereographic and trace analyses revealed the microcrack propagation directions. Two types of microcracks were observed: wedge-shaped and with parallel sides. The obtained results on possible reasons and mechanisms of microcrack formation in the above places are discussed in line with the theoretical assumptions and the existing literature.

Transmission Electron Microscopy studies of the vacancy ordering in YSI2-X thin films

1991 ◽  
Vol 49 ◽  
pp. 562-563
Author(s):  
F.-R. Chen ◽  
T. L. Lee ◽  
L. J. Chen
Keyword(s):  
Crystal Structure ◽  
Electron Microscopy ◽  
Thin Films ◽  
Diffraction Pattern ◽  
Annealing Temperature ◽  
Lattice Mismatch ◽  
Si Substrate ◽  
Metal Thin Films ◽  
Transmission Electron ◽  
Vacancy Ordering

YSi2-x thin films were grown by depositing the yttrium metal thin films on (111)Si substrate followed by a rapid thermal annealing (RTA) at 450 to 1100°C. The x value of the YSi2-x films ranges from 0 to 0.3. The (0001) plane of the YSi2-x films have an ideal zero lattice mismatch relative to (111)Si surface lattice. The YSi2 has the hexagonal AlB2 crystal structure. The orientation relationship with Si was determined from the diffraction pattern shown in figure 1(a) to be and . The diffraction pattern in figure 1(a) was taken from a specimen annealed at 500°C for 15 second. As the annealing temperature was increased to 600°C, superlattice diffraction spots appear at position as seen in figure 1(b) which may be due to vacancy ordering in the YSi2-x films. The ordered vacancies in YSi2-x form a mesh in Si plane suggested by a LEED experiment.

Transmission Electron Microscopy studies of texture of Cr underlayer of magnetic recording hard disk

1991 ◽  
Vol 49 ◽  
pp. 580-581
Author(s):  
L. Tang ◽  
G. Thomas ◽  
M. R. Khan ◽  
S. L. Duan
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Transmission Electron Microscopy ◽  
Magnetic Recording ◽  
Magnetic Thin Films ◽  
Magnetic Films ◽  
Substrate Bias ◽  
Epitaxial Relationship ◽  
Transmission Electron

Cr thin films are often used as underlayers for Co alloy magnetic thin films, such as Co1, CoNi2, and CoNiCr3, for high density longitudinal magnetic recording. It is belived that the role of the Cr underlayer is to control the growth and texture of the Co alloy magnetic thin films, and, then, to increase the in plane coercivity of the films. Although many epitaxial relationship between the Cr underlayer and the magnetic films, such as ﹛1010﹜Co/ {110﹜Cr4, ﹛2110﹜Co/ ﹛001﹜Cr5, ﹛0002﹜Co/﹛110﹜Cr6, have been suggested and appear to be related to the Cr thickness, the texture of the Cr underlayer itself is still not understood very well. In this study, the texture of a 2000 Å thick Cr underlayer on Nip/Al substrate for thin films of (Co75Ni25)1-xTix dc-sputtered with - 200 V substrate bias is investigated by electron microscopy.

Transmission Electron Microscopy of Evaporated Perylene Thin Films

1990 ◽  
Vol 48 (2) ◽  
pp. 336-337
Author(s):  
C. Ewins ◽  
J.R. Fryer
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Transmission Electron Microscopy ◽  
Molecular Electronics ◽  
High Vacuum ◽  
Amorphous Layer ◽  
Electric Heater ◽  
Transmission Electron ◽  
Polycyclic Aromatic

The preparation of thin films of organic molecules is currently receiving much attention because of the need to produce good quality thin films for molecular electronics. We have produced thin films of the polycyclic aromatic, perylene C10H12 by evaporation under high vacuum onto a potassium chloride (KCl) substrate. The role of substrate temperature in determining the morphology and crystallography of the films was then investigated by transmission electron microscopy (TEM).The substrate studied was the (001) face of a freshly cleaved crystal of KCl. The temperature of the KCl was controlled by an electric heater or a cold finger. The KCl was heated to 200°C under a vacuum of 10-6 torr and allowed to cool to the desired temperature. The perylene was then evaporated over a period of one minute from a molybdenum boat at a distance of 10cm from the KCl. The perylene thin film was then backed with an amorphous layer of carbon and floated onto copper microscope grids.

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