Primary Study on the Improvement and Application of Formulation Optimization of 2116# Rosin Modified Phenolic Resin

2020 ◽  
Vol 837 ◽  
pp. 168-173
Author(s):  
Qing Zhang ◽  
Li Li Huang ◽  
Mei Ye Wu ◽  
Xiao Zhang Yu

2116# Rosin Modified Phenolic Resin is synthesized by means of one-step process taking calcium hydroxide as catalyst and Rosin, Bisphenol A, solid formaldehyde and glycerol as main raw materials. The formulation and process are improved and characterized. The result shows that it satisfies technical performance indicators. And, it is preliminarily applied to ink. This resin is expected to be applied to printing ink and coating industry.

e-Polymers ◽  
2003 ◽  
Vol 3 (1) ◽  
Author(s):  
Bernd Bruchmann ◽  
Wolfgang Schrepp

Abstract Synthesizing hyperbranched polyurethanes in a one step process using commercially available raw materials: these were the primary conditions for this work. By taking advantage of intramolecular reactivity differences of isocyanate groups in diisocyanates in combination with reactivity differences of OH and NH groups in alkanolamines, it is possible to generate in situ AB2 molecules by controlling reactions of specific functional groups towards each other. This AA* + B*B2 approach works without protecting groups and opens up a simple and versatile strategy towards hyperbranched aromatic as well as aliphatic polyureaurethanes. Preferential diisocyanates for this synthesis were 2,4-toluylene diisocyanate and isophorone diisocyanate, whereas diethanolamine and diisopropanolamine were used as isocyanate-reactive counterparts.


Author(s):  
D. V. Andreev

The article describes experiments on the reconstruction of the technology of the one-step process of obtaining iron-carbon alloys in furnaces based on archaeological sources. It contains the description of furnace design, metallurgical process technology and raw materials preparation. The process of refining the iron bloom by forging is described. Scientifically grounded assumptions are made about possible technological methods of obtaining steels in the pre-industrial period on the territory of modern Belarus.


2021 ◽  
Author(s):  
Hu-Lin Liu ◽  
Feng-Zhen DANG ◽  
De-Wei NI ◽  
Chang-Qing LIU ◽  
Yun-Long XUE ◽  
...  

Abstract We developed a new method to synthesize single-phase transition metal carbide powders by combining citric acid complexing method and ball-milling dispersion. High-entropy carbides (Zr0.25Ti0.25Ta0.25Nb0.25)C (4TmC), (Zr0.2Ti0.2Ta0.2Nb0.2Hf0.2)C (5TmC-H) and (Zr0.2Ti0.2Ta0.2Nb0.2Mo0.2)C (5TmC-M) were successfully fabricated by this method using low-cost raw materials. The element and phase composition and microstructures of the obtained carbide powders were investigated. The relationships of synthesis process and temperature with chemical composition were also discussed. (Zr0.25Ti0.25Ta0.25Nb0.25)C can be obtained by a one-step process at 1550 °C, while (Zr0.2Ti0.2Ta0.2Nb0.2Hf0.2)C and (Zr0.2Ti0.2Ta0.2Nb0.2Mo0.2)C are fabricated by a two-step process of carbothermal reduction followed by solid solution at the temperatures not lower than 1850 °C and 1650 °C. The higher synthesis temperatures of the five-component carbides are attributed to the obvious sluggish diffusion effect induced by the larger lattice distortions. The particle sizes of (Zr0.25Ti0.25Ta0.25Nb0.25)C, (Zr0.2Ti0.2Ta0.2Nb0.2Hf0.2)C and (Zr0.2Ti0.2Ta0.2Nb0.2Mo0.2)C powders are 118.2±26.1 nm (at 1550 °C), 284.8±73.7 nm (at 1850 °C) and 65.5±13.9 nm (at 1750 °C), respectively.


2013 ◽  
Vol 821-822 ◽  
pp. 1122-1125
Author(s):  
Xiao Mei Wang ◽  
Yan Ming Zhang

Taking cassava starch as the raw materials and hydrochloric acid (HCL) as the catalyst, the acidolysis modification of starch was performed combining with the size mixture blending process. The results show that when the concentration of cassava starch is in the range of 8%~12%, the dosage of 6% hydrochloride acid for 1000g starch milk is about 0.8g~1.2g, and the viscosity of acidolysis starch decreases with the increase of hydrochloric acid dosage. The viscosity can reach the stable level when the reaction time is about 2 hours for the size mixture of low viscosity, and is about 3 hours for that of the high viscosity. Also, the viscosity thermal stability of size mixture is verified to be good.


Nanoscale ◽  
2021 ◽  
Author(s):  
Wipakorn Jevasuwan ◽  
Naoki Fukata

Vertical Al-catalyzed SiNW arrays with shaped surfaces were synthesized by a one-step process and NW-based solar cells were demonstrated with optimized NW surface defects through surface modification and length reduction.


2017 ◽  
Vol 101 (4) ◽  
pp. 1780-1789 ◽  
Author(s):  
Giuliana Taglieri ◽  
Valeria Daniele ◽  
Claudia Mondelli

2017 ◽  
Vol 5 (2) ◽  
pp. 110 ◽  
Author(s):  
Adebayo Fashina ◽  
Salifu Azeko ◽  
Joseph Asare ◽  
Chukwuemeka Ani ◽  
Vitalis Anye ◽  
...  

This paper presents the results of a study on the reliability and performance of the solar-powered street lighting systems installed at the African University of Science and Technology (AUST) in Nigeria, a hot and humid environment. The technical performance of the systems was studied using the following performance indicators: system energy yield, capture loss, as well as the system performance ratio while the reliability of the systems was examined using a model developed from the findings from the maintenance and fault diagnosis of the systems. The model was used to predict the total failure and survival probability of the systems using the Weibull distribution. The performance evaluation during the monitored period (February 2012 to January 2015) indicated that the performance ratios of the systems vary from 70% to 89% and the energy yields of the systems ranging from 2.87 h/day to 5.57 h/day. The results from the reliability analysis also showed that when the stress concentration factor around the notch between the cable terminals in the charge controller increases, the charge controller will become overheated, which in turn affected other components of the systems. The implications of this study are also discussed for the design and development of future solar-powered street lighting systems.


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