Tensile Deformation of Si Single Crystals at High Temperatures

2021 ◽  
Vol 1016 ◽  
pp. 1443-1447
Author(s):  
Tubasa Suzuki ◽  
Masaki Tanaka ◽  
Tatsuya Morikawa ◽  
Yelm Okuyama ◽  
Jun Fujise ◽  
...  

Czochralski silicon single crystals were deformed in tensile tests along the direction at between 1173 K and 1373. Yield point phenomenon were observed in the specimens deformed at below 1273 K while continues yield was observed in the specimens deformed at above 1323 K. It is due to the effect of dislocation starvation in the used crystals. Work-hardening rates in stage II were consistent with those reported in fcc crystals such as copper. The onset of stage II was found to be active before the Schmid factor of the second slip system becomes larger than that of the primary slip system. Electron backscattered diffraction images indicated clear kink bands near grips and in the parallel portion. The kink bands were formed at the middle of stage I, which suggest that the formation of kink bands is a trigger of stage II.

2021 ◽  
Vol 1016 ◽  
pp. 516-521
Author(s):  
Tomohiro Hanada ◽  
Masayuki Tsushida ◽  
Hiromoto Kitahara ◽  
Shinji Ando

Tensile tests of Mg-Y single crystals with different yttrium concentrations: 0.07 and 0.3 at.% were carried out to investigate effects of yttrium on pyramidal <c+a> slip system. In Mg-0.07at%Y alloy single crystals, {11 2}< 23> second order pyramidal <c+a> slip was activated and yield stress increased, compared to pure Mg single crystals. On other hand, in Mg-0.3at%Y alloy single crystals, {10 1}< 23> first order pyramidal <c+a> slip was activated and yield stress increased, compared to Mg-0.07at%Y alloy single crystals. The change in slip system by yttrium addition would be caused by increasing critical resolved shear stress (CRSS) for second order pyramidal slip.


2010 ◽  
Vol 638-642 ◽  
pp. 2297-2302
Author(s):  
Takashi Matsuo

Through the analysis of many creep rate-time or creep rate-strain curves of -single phase Ni-20mass% Cr alloy single crystals with various stress axes, it was clarified that the creep deformation manners at lower stresses are drastically different to those at higher stresses. These creep features at lower stresses are summarized into three ones as follows. (i) The fully extended transient stage occupies the considerable ratio of rupture life. (ii) The steady state stage disappears, because the transient stage directly connected with the accelerating stage. (iii) The origin of the onset of accelerating stage is regarded as the formation of the dynamic recrystallized grain. These difference in creep deformation manner were caused by the predominant operation of the primary slip system and then the homogeneous evolution of dislocation substructures.


Single-crystal test specimens of van Arkel titanium were obtained by a modification of the strain anneal technique.The modes of slip have been identified as (101̄0) [112̄0],(101̄1) [112̄0], and (0001) [112̄0]. It has been shown that not only does the interstitial impurity affect the magnitude of the critical resolved shear stress but also the relative values for the three slip systems. (101̄0) is the principal slip system and is favoured by increasing purity. A possible mechanism for the role of oxygen and nitrogen in this effect is put forward wherein it is shown that the interstitial sites occupied are such that interstitial elements render slip more difficult on two of the three slip planes in titanium.


2007 ◽  
Vol 539-543 ◽  
pp. 3030-3035
Author(s):  
Takashi Matsuo

Through the analysis of many creep rate-strain curves of γ-single phase Ni-20mass%Cr alloy single crystals with various stress axes, it has been elucidated that the ratio of transient stage to rupture life becomes larger with decreasing the stress. And the transient stage consists of Stage I and Stage II. In Stage I, the creep rate just after loading remains constant, and in Stage II, a steep decrease in creep rate continues. It is noticeable that there is a marked difference in transient stage among single crystals with different stress axes. The aim of this study is to elucidate the mechanisms leading to the different transient stages as the function of stress axes. The deformation during transient stage in the single crystals except for the single crystals with the stress axes of the [001] and [1,–11] poles in the standard stereographic triangle, proceeds using the primary slip plane. And they are divided into two groups of the single crystals with the angle between stress axis and primary slip plane, θ, less than 45° and the single crystals with θ more than 45°. The deformations of Stage I and Stage II in these single crystals proceed using the slip system of (111)<1,–01> and the slip system of (111)<1,–10>, and in Stage I, the former slip system acts mainly except for that of single crystals with stress axis of [011]. While, in the single crystal with stress axis of [011], two slip systems above described operate at the beginning of Stage I, and the stress axis moves along [011]-[1,–11] line. And this moving gives slight increase in the Schmid factor, therefore, in Stage I slight increase in creep rate was confirmed. The {111} pole figure of the single crystal with stress axis of [1,–11] whose deformation proceeds using the plural slip planes are obtained by SEM-EBSD method. It becomes clear that the smallest strains of Stage I and Stage II derived from the increase in the torsion with creep deformation.


Author(s):  
H. P. Karnthaler ◽  
A. Korner

In f.c.c. metals slip is observed to occur generally on {111} planes. Glide dislocations on intersecting {111} planes can react with each other and form Lomer-Cottrell locks which lie along a <110> direction and are sessile since they are split on two {111} planes. Cottrell already pointed out that these dislocations could glide on {001} planes if they were not split. The first study of this phenomenon has been published recently. It is the purpose of this paper to report some interesting new details of the dislocations gliding on {001} planes in pure Ni, Cu, and Ag deformed at room temperature.Single crystals are grown with standard orientation and strained into stage II. The crystals are sliced parallel to the (001) planes. The dislocation structure is studied by TEM and the Burgers vectors ḇ and glide planes of the dislocations are determined unambiguously.In Fig.l primary P and secondary S dislocations react and form composite dislocations K.


Materials ◽  
2021 ◽  
Vol 14 (2) ◽  
pp. 252
Author(s):  
Rongchuang Chen ◽  
Shiyang Zhang ◽  
Xianlong Liu ◽  
Fei Feng

To investigate the effect of hot working parameters on the flow behavior of 300M steel under tension, hot uniaxial tensile tests were implemented under different temperatures (950 °C, 1000 °C, 1050 °C, 1100 °C, 1150 °C) and strain rates (0.01 s−1, 0.1 s−1, 1 s−1, 10 s−1). Compared with uniaxial compression, the tensile flow stress was 29.1% higher because dynamic recrystallization softening was less sufficient in the tensile stress state. The ultimate elongation of 300M steel increased with the decrease of temperature and the increase of strain rate. To eliminate the influence of sample necking on stress-strain relationship, both the stress and the strain were calibrated using the cross-sectional area of the neck zone. A constitutive model for tensile deformation was established based on the modified Arrhenius model, in which the model parameters (n, α, Q, ln(A)) were described as a function of strain. The average deviation was 6.81 MPa (6.23%), showing good accuracy of the constitutive model.


2021 ◽  
Vol 1026 ◽  
pp. 65-73
Author(s):  
Kai Zhu ◽  
Hong Wei Yan

Both microstructure inhomogeneity and mechanical property diversity along the thickness direction in rolled thick aluminum plates have been considered to have a remarkable impact on the performance and properties of the products made from the plates. In this study, scanning electron microscopy (SEM) and electron backscattered diffraction (EBSD) characterizations of microstructure and texture types along the thickness directions of Al7055 thick plate specimens prepared using two conditions, hot-rolling and solution-quenching, were performed. To examine the mechanical properties, uniaxial tensile tests were also carried out on specimens machined from both types of thick plates, using a layered strategy along the thickness direction. The results indicate that both the microstructure and mechanical properties are inhomogeneous under the two conditions. Furthermore, it is evident that there is a hereditary relationship between the mechanical properties of the two plates—areas with higher yield strength in the as-hot-rolled plate correspond to areas with the higher yield strength in the as-solution-quenched plate


Author(s):  
G. A. Stone ◽  
G. Thomas

A single crystal stressed in the [3]𝛄 direction at 185°K was transformed to 5% 𝛂 martensite and 2% Ɛ martensite by volume. The austenite slip system of maximum shear stress is the (11)𝛄 [01)𝛄. Fig. 1 shows a two surface study using the electron and optical microscopes. The a martensite is confined between £martensite plates with the (0001)Ɛ ∥ (11)𝛄. The size of the acicular martensite crystals is controlled by the spacing of the £ martensite plates. These £ martensite plates are seen in Fig. 1A as dark vertical bands. The axes of the acicular crystals lie in the (11)𝛄 plane. The £ martensite habit plane is defined as the plane perpendicular to the (11)𝛄 containing the vector defining the crystal axis.


2007 ◽  
Vol 29-30 ◽  
pp. 245-248
Author(s):  
F. Tang ◽  
B.Q. Han ◽  
Masuo Hagiwara ◽  
Julie M. Schoenung

An ultrafine-grained Al-5083 alloy reinforced with 5 vol.% nano-sized β-SiC particles was fabricated with a powder cryomilling and consolidation technique. Tensile tests were conducted at temperatures from 298 to 773 K for this composite. The mechanisms for deformation and fracture of this nanostructured composite at various temperatures are discussed.


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