Employment of DC Sputtering for Synthesizing Nano Cadmium Oxide for Sevoflurane Anesthetic Gas Sensor

2021 ◽  
Vol 1039 ◽  
pp. 406-415
Author(s):  
Asmaa S.J.M. Al-Ragehey ◽  
Osama Abdul Azeez Dakhil ◽  
Hussein Saadoun ◽  
Asmaa Hadi Mohammed ◽  
Marwa Hassan
Keyword(s):  
Silver Nanoparticles ◽  
Gas Sensor ◽  
Cadmium Oxide ◽  
Metal Plate ◽  
Content Increase ◽  
Sem Images ◽  
Dc Sputtering ◽  
Silver Nps ◽  
Cadmium Metal ◽  
Quartz Substrates

Thin films of CdO doped with AgNPs were deposited on ITO quartz substrates using DC sputtering protocol. The films were characterized using different techniques like XRD pattern for both undoped and doped one CdO NPs with silver nanoparticles, with various doping concentrations (0.4, 1.04, and 1.20) at%. It has been noticed from X-ray pattern that the nanostructured films possessed polycrystalline reflection patterns and the Prevailing orientation plane (111) on 2θ=33.35o in addition the reflection intensity increases with increasing of the doping concentration (1chip, 2chips and 3 chips) of Silver nanoparticles that chipped to the surface cadmium plate. Microstructures characterization of synthesized samples was studied using SEM. Images of SEM demonstrated that the particle size increases directly along with the number of implanting Silver NPs with three chips (1, 2 and 3) to the essential plate of Cd metal. EDXS spectroscopy counting the elemental composition using the atomic percentage, it has been demonstrated existence of silver in doped once. More, the percentage of silver content increase with increasing the number of Ag chips increases as follows The Ag content in the doped films of the cadmium metal plate with 1 attached is (1.39 wt. % for one Ag chip, 2.02 wt. % for two Ag chips while, the concentration has been increased further for three Ag chips to 3.24 at. %. Sensitivity of the manufactured device to Sevoflurane Anesthetic Gas Sensor indicates that the resistance decreases with the increase in the number of silver chips, and this is due to an increase of the pure charge carriers of the current. Keywords: Cadmium Oxide, Sliver, Structural Properties, DC reactive magnetron sputtering method, Sevoflurane Anesthetic Gas.

Green and Simple Synthesis of Silver Nanoparticles by Aqueous Extract of Perovskia abrotanoides: Characterization, Optimization and Antimicrobial Activity

2020 ◽  
Vol 21 (11) ◽  
pp. 1129-1137 ◽  
Author(s):  
Somayeh Mirsadeghi ◽  
Masoumeh F. Koudehi ◽  
Hamid R. Rajabi ◽  
Seied M. Pourmortazavi
Keyword(s):  
Antimicrobial Activity ◽  
Silver Nanoparticles ◽  
Minimum Inhibitory Concentration ◽  
Plant Extract ◽  
Inhibitory Concentration ◽  
Minimum Bactericidal Concentration ◽  
Extraction Temperature ◽  
Silver Particles ◽  
Silver Nps ◽  
Perovskia Abrotanoides

Background: Herein, we report the biosynthesis procedure to prepare silver nanoparticles as reduction and capping agents with the aqueous plant extract of Perovskia abrotanoides. Methods: The therapeutic application of silver nanoparticles entirely depends on the size and shape of the nanoparticles therefore, their control during the synthesis procedure is so important. The effects of synthesis factors, for example, silver ion concentration, the mass of plant extract, reaction time and extraction temperature, on the size of silver particles were considered and optimized. Several analytical methods were used for the characterization of silver NPs including FT-IR and UV–Vis spectrophotometer, XRD and SEM. Results: The results showed that the mean size of the silver particles was about 51 nm. Moreover, the antibacterial properties of biosynthesized silver NPs were investigated by the minimum inhibitory concentration, minimum bactericidal concentration, and Well-diffusion tests. The minimum inhibitory concentration/ minimum bactericidal concentration values of silver NPs and aqueous plant extract versus Gram-positive bacteria (Staphylococcus aureus and Bacillus cereus) and Gram-negative bacteria (E. coli) were 3.03/0.00, 1.20/0.01, 3.06/0.00, 0.98/1.04, 1.00/0.05 and 1.30/0.03 (mg/mL), respectively. Conclusion: The antimicrobial activity study displayed that the synthesized silver nanoparticles by plant extract have better antimicrobial properties compared to aqueous plant extract of Perovskia abrotanoides.

Graphene Decorated with Silver Nanoparticles as a Low-Temperature Methane Gas Sensor

2019 ◽  
Vol 11 (24) ◽  
pp. 21795-21806 ◽  
Author(s):  
Rezvan Ghanbari ◽  
Rosa Safaiee ◽  
Mohammad H. Sheikhi ◽  
Mohammad M. Golshan ◽  
Z. Karami Horastani
Keyword(s):  
Silver Nanoparticles ◽  
Low Temperature ◽  
Gas Sensor ◽  
Methane Gas

Antimicrobial Activities of Coriander Seed Essential Oil and Silver Nanoparticles

2021 ◽  
Author(s):  
Kadriye Ozlem saygi ◽  
Birgul Kacmaz ◽  
Serdar Gul
Keyword(s):  
Silver Nanoparticles ◽  
Essential Oil ◽  
Bacterial Infections ◽  
Materials Science ◽  
Antimicrobial Properties ◽  
Antimicrobial Activities ◽  
Elemental Distribution ◽  
Sem Images ◽  
X Ray ◽  
Coriander Seed

Abstract Bacterial infections are one of the most serious health problems all over the world, which cause need for the discovery of new drug. Since antibiotic resistance is a major threat to both humans and the environment, there is a need for studies on the antimicrobial properties of different forms of traditionally used plants. Herein, the seeds of coriander were used to isolate essential oil (EO) and to synthesise silver nanoparticles (C-AgNPs). The major oil constituents were characterized by GC-MS as Linalool (79.12%), Camphor (6.16%), γ-Terpinene (2.82%) and α-Pinene (2.67%). The synthesized AgNPs were characterized by UV-Visible spectrophotometry, Scanning Electron Microscopy (SEM), Energy Dispersive X-ray (EDX), X-ray difraction (XRD) and Fourier Tranmission Infrared (FTIR). The surface plasmon resonance (SPR) of C-AgNPs at 437 nm was recorded on the UV-Vis spectrometer. The spherical and homogenous of AgNPs was presented in SEM images. EDX showed elemental distribution and confirmed AgNPs. A characteristic intense peak was at 3.0 keV. The antibacterial activities of the essential oil and AgNPs form of coriander seed against Staphylococcus aureus ATCC 29213 and Escherichia coli ATCC 25922 bacteria were investigated by broth microdilution test. AgNPs and essential oil of coriander can be expected to provide future opportunities in nanomedicine and materials science. AgNPs can be displayed synergistic antimicrobial effect when used in combination with essential oil.

SERS Tags Derived from Silver Nanoparticles and Aryl Diazonium Salts for Cell Raman Imaging

Nanoscale ◽  
2022 ◽  
Author(s):  
Da Li ◽  
Philippe Nizard ◽  
Delphine Onidas ◽  
Aazdine Lamouri ◽  
Jean Pinson ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Silver Nanoparticles ◽  
Surface Functionalization ◽  
Surface Enhanced Raman Spectroscopy ◽  
Raman Imaging ◽  
Diazonium Salts ◽  
Surface Enhanced ◽  
Surface Enhanced Raman ◽  
Silver Nps ◽  
Sers Tags

The surface functionalization of silver nanoparticles (NPs) by Raman reporters has stimulated a wide interest in recent years for the design of Surface-Enhanced Raman Spectroscopy (SERS) labels. However, silver NPs...

scholarly journals Inhibitory Activity of Silver Nanoparticles Synthesized Using Lycopersicon Esculentum against Biofilm Formation in Candida Species

Nanomaterials ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1512 ◽  
Author(s):  
Jeong Su Choi ◽  
Ji Woong Lee ◽  
Un Chul Shin ◽  
Min Woo Lee ◽  
Dae Jin Kim ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Lycopersicon Esculentum ◽  
Candida Species ◽  
Normal Growth ◽  
Antibiofilm Activity ◽  
Sem Images ◽  
X Ray ◽  
Natural Extracts ◽  
Particle Characteristics ◽  
Ft Ir

This paper investigated the antifungal and antibiofilm activity of silver nanoparticles synthesized with Lycopersicon esculentum extracts against Candida species. Lycopersicon esculentum extracts obtained by homogenization were mixed with silver nitrate to synthesize silver nanoparticles. Analysis of the particle characteristics by UV–Vis spectrophotometry, scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDAX), dynamic light scattering (DLS), and Fourier transform infrared spectroscopy (FT-IR) confirmed that the Lycopersicon esculentum extracts effectively served as reductants and capping agents. Minimum inhibitory concentration (MIC) tests were conducted to confirm antifungal activity against Candida species. In all the tested species, the silver nanoparticles inhibited the growth of Candida. Moreover, the SEM images of Candida species treated with silver nanoparticles synthesized using natural extracts of Lycopersicon esculentum showed that silver nanoparticles adhered to the surface of Candida, which induced pore formation in the membranes and prevented their normal growth. Ultimately, these abnormal forms of Candida were thought to be less able to form biofilms than normal Candida. The antifungal and antibiofilm activities of silver nanoparticles against Candida are expected to be utilized in various fields and contribute in particular to developments in nanomedicine.

scholarly journals Green Synthesis of Silver Nanoparticles in the Presence of Polysaccharide: Optimization and Characterization

2020 ◽  
Vol 2020 ◽  
pp. 1-10 ◽  
Author(s):  
Margarita I. Skiba ◽  
Victoria I. Vorobyova ◽  
Alexander Pivovarov ◽  
Natalya P. Makarshenko
Keyword(s):  
Silver Nanoparticles ◽  
Sodium Alginate ◽  
Xrd Analysis ◽  
Face Centered Cubic ◽  
Colloidal Solutions ◽  
Ag Nps ◽  
Sem Images ◽  
Spherical Powder ◽  
Stabilizing Agent ◽  
Vis Spectroscopy

The process of obtaining aqueous solutions of silver nanoparticles with the use of a low-temperature nonequilibrium contact plasma and stabilizing agent—polysaccharide (sodium alginate)—has been examined. The synthesized Ag NPs were characterized by using UV-Vis spectroscopy, dynamic light scattering (DLS), scanning electron microscope (SEM), and XRD analysis. The effect of concentration of Ag+, sodium alginate, duration of processing by plasma discharge, and pH of liquid on the production of silver nanoparticles has been studied. The results demonstrated that synthesis provides the formation of silver nanoparticles for investigated concentrations of Ag+ (0.3-3.0 mmol/l) and 5.0 g/l Na-Alg (pH=7–10) within 1–5 minutes. From the SEM images, the silver nanoparticles are found to be almost spherical. Powder XRD results reveal that Ag nanoparticles have a face-centered cubic crystal structure. Zeta potential of plasma-chemically obtained colloidal solutions at various concentrations of Ag+ ions and stabilizing agent varies from −32.8 to −39.3 mV, indicating the moderate stability of synthesized nanoparticles.

scholarly journals Femtosecond laser fabrication of silver nanostructures on glass for surface enhanced Raman spectroscopy

2019 ◽  
Vol 9 (1) ◽  
Author(s):  
Mark MacKenzie ◽  
Haonan Chi ◽  
Manoj Varma ◽  
Parama Pal ◽  
Ajoy Kar ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Silver Nanoparticles ◽  
Silica Surface ◽  
Microfluidic Channel ◽  
Surface Enhance Raman Spectroscopy ◽  
Surface Enhanced Raman Spectroscopy ◽  
Fused Silica ◽  
Microfluidic Channels ◽  
Silver Nanostructures ◽  
Sem Images

AbstractWe report on an optimized fabrication protocol for obtaining silver nanoparticles on fused silica substrates via laser photoreduction of a silver salt solution. We find that multiple scans of the laser over the surface leads to a more uniform coverage of densely packed silver nanoparticles of approximately 50 nm diameter on the fused silica surface. Our substrates yield Raman enhancement factors of the order of 1011 of the signal detected from crystal violet. We use a theoretical model based on scanning electron microscope (SEM) images of our substrates to explain our experimental results. We also demonstrate how our technique can be extended to embedding silver nanoparticles in buried microfluidic channels in glass. The in situ laser inscription of silver nanoparticles on a laser machined, sub-surface, microfluidic channel wall within bulk glass paves the way for developing 3D, monolithic, fused silica surface enhance Raman spectroscopy (SERS) microfluidic sensing devices.

scholarly journals New Relevant Descriptor of Linear QNAR Models for Toxicity Assessment of Silver Nanoparticles

Nanomaterials ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 1459
Author(s):  
Alexey Kudrinskiy ◽  
Pavel Zherebin ◽  
Alexander Gusev ◽  
Olga Shapoval ◽  
Jaeho Pyee ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Biological Activity ◽  
Colloidal Stability ◽  
Chemical Nature ◽  
Equilibrium Concentration ◽  
Toxicity Assessment ◽  
Yeast Cells ◽  
Wide Range ◽  
Silver Nps ◽  
Living Organisms

The use of silver nanoparticles (NPs) in medical, industrial and agricultural fields is becoming more widespread every year. This leads to an increasing number of experimental toxicological and microbiological studies of silver NPs aimed at establishing the risk–benefit ratio for their application. The following key parameters affecting the biological activity of silver dispersions are traditionally taken into consideration: mean diameter of NPs, surface potential of NPs and equilibrium concentration of Ag+. These characteristics are mainly predetermined by the chemical nature of the capping agent used for stabilization. However, the extent to which they influence the biological activity and the toxicity of silver NPs varies greatly. In this work, dispersions of silver NPs stabilized with a wide array of substances of different chemical nature were used for quantitative evaluation of whether the various measurable properties of silver NPs fit as descriptors of linear QNAR (quantitative nanostructure–activity relationship) models for silver NP toxicity evaluation with respect to a model eukaryotic microorganism—Saccharomyces cerevisiae yeast cells. It was shown that among the factors that determine silver NP toxicity, the charge of particles, their colloidal stability and the ability to generate Ag+ ions carry more importance than the descriptors related to the particle size. A significant synergistic effect between the ζ-potential and the colloidal stability of silver NPs on their toxicity was also discovered. Following this, a new descriptor has been proposed for the integral characterization of the silver dispersion colloidal stability. According to the obtained data, it can be considered applicable for building QNAR models of higher efficacy. The validity testing of the proposed model for theoretical prediction of silver NP toxicity using a wide range of living organisms has shown that this new descriptor correlates with toxicity much better compared to most traditionally used descriptors. Consequently, it seems promising in terms of being used not only in situations involving the rather narrow array of the objects tested, but also for the construction of silver NP toxicity models with respect to other living organisms.

Time resolved growth of membrane stabilized silver NPs and their catalytic activity

RSC Advances ◽  
2014 ◽  
Vol 4 (103) ◽  
pp. 59379-59386 ◽  
Author(s):  
Sabyasachi Patra ◽  
Debasis Sen ◽  
Ashok K. Pandey ◽  
J. Bahadur ◽  
S. Mazumder ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Catalytic Activity ◽  
Growth Kinetics ◽  
Nanocomposite Membranes ◽  
Time Resolved ◽  
Catalytic Application ◽  
Silver Nps ◽  
First Time ◽  
Kinetics Of

Growth kinetics of membrane stabilized silver nanoparticles have been studied for the first time with time resolved in situ SAXS. The catalytic application of nanocomposite membranes thus formed has also been explored.

scholarly journals FDTD Modelling of Silver Nanoparticles Embedded in Phase Separation Interface of H-PDLC

2015 ◽  
Vol 2015 ◽  
pp. 1-7 ◽  
Author(s):  
Kun Gui ◽  
Jihong Zheng ◽  
Kangni Wang ◽  
Daoping Li ◽  
Songlin Zhuang
Keyword(s):  
Silver Nanoparticles ◽  
Phase Separation ◽  
Incident Angle ◽  
Incident Light ◽  
Near Field ◽  
Double Resonance ◽  
Blue Shift ◽  
Resonance Peak ◽  
Localized Surface Plasmon ◽  
Silver Nps

We report localized surface plasmon resonance (LSPR) of silver nanoparticles (NPs) embedded in interface of phase separation of holographic polymer-dispersed liquid crystal (H-PDLC) gratings using Finite-Difference Time Domain method. We show that silver NPs exhibit double resonance peak at the interface, and these peaks are influenced by the angle of incident light. We observe a blue shift of the wavelength of resonance peak as the incident angle increases. However, the location of silver NPs at the interface has nearly no effect on the wavelength of resonance peak. Also we show near-field and far-field properties surrounding silver NPs and find that field distribution can be controlled through rotation of incident angle. Therefore, LSPR properties of silver NPs within H-PDLC gratings can be excited by appropriate wavelength and angle of the incident light.

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