Continuous Grain Refinement Using Severe Torsion Straining Process

2006 ◽  
Vol 503-504 ◽  
pp. 385-390 ◽  
Author(s):  
Katsuaki Nakamura ◽  
Koji Neishi ◽  
Kenji Kaneko ◽  
Michihiko Nakagaki ◽  
Z. Horita
Keyword(s):  
Grain Size ◽  
Grain Refinement ◽  
Uniform Elongation ◽  
Continuous Process ◽  
Longitudinal Axis ◽  
Mg Alloy ◽  
Critical Ratio ◽  
Al Alloy ◽  
Heated Zone ◽  
Wide Range

This study presents a new rapid continuous process for grain refinement in metallic materials through severe plastic deformation (SPD). The new process, designated in this study the severe torsion straining process (STSP), is applicable to a wide range of alloys based on aluminum, magnesium and copper including carbon steel. This process consists of producing a local heated zone in a rod and cooling both sides of the heated zone by spray water while rotating one end with the other. Thus, torsion strain is introduced in the local heated zone. The STSP can be continuous because the straining is achieved while the rod is shifted along the longitudinal axis of the rod. Furthermore, the process requires no die, suggesting a potential for commercialization of grain refinement through SPD. In this study, STSP was applied to an Al-Mg alloy and a Mg-Al-Zn alloy. It is shown that STSP is effective for both alloys so that the grain size is reduced to ~1.5 μm for the Al alloy and ~0.9 μm for the Mg alloy. Tensile testing showed that the strength is increased with a minimal decrease in uniform elongation. There is a critical ratio between rotation speed and moving speed, which defines the feasibility of STSP operation without breaking the rod. The grain size tends to be lowered as the ratio is close to the critical value.

Grain Refinement of Commercial Al-Mg Alloy Using Severe Torsion Straining Process

2006 ◽  
Vol 503-504 ◽  
pp. 955-960 ◽  
Author(s):  
Koji Neishi ◽  
Akihiko Higashino ◽  
Yuichi Miyahara ◽  
Katsuaki Nakamura ◽  
Kenji Kaneko ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Grain Size ◽  
Cooling Rate ◽  
Grain Refinement ◽  
Rotation Speed ◽  
Imaging System ◽  
Continuous Process ◽  
Critical Ratio ◽  
Heated Zone ◽  
Moving Speed

Severe plastic deformation (SPD) makes it possible to refine grain size in many metallic materials. Recently, we have developed a new SPD process designated the severe torsion straining process (STSP). This process requires no die but one side of a rod is rotated with respect to the other while producing a local heated zone in the rod and cooling both sides of the heated zone. Torsion strain is then introduced in the local heated zone. The STSP can be a continuous process because the rod is moved in the longitudinal direction while introducing torsion strain through the rotation. For grain refinement using the STSP, various factors may affect, which are the rotation speed, moving speed, straining temperature, cooling rate and diameter of the rod. In this study, the STSP is applied to grain refinement of an A5056 Al-Mg commercial alloy and the factors affecting the grain refinement are optimized. STSP was conducted at a temperature in the range from 573K to 723K. Microstructure was observed by optical microscopy, scanning electron microscopy with an orientation imaging system, and transmission electron microscopy. Microscopy observations revealed that the grain size was reduced to ~0.9 μm, when STSP was conducted at 573K with a rotation speed of 10 rpm and moving speed of 50 mm/min. There is a critical ratio of rotation speed to moving speed above which the rod breaks. The grain size tends to be finer as the straining temperature is lower, the cooling rate is faster and the ratio of rotation speed to moving speed is closer to the critical value.

scholarly journals Effect of Vanadium Reinforcement on the Microstructure and Mechanical Properties of Magnesium Matrix Composites

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 806
Author(s):  
Liqing Sun ◽  
Shuai Sun ◽  
Haiping Zhou ◽  
Hongbin Zhang ◽  
Gang Wang ◽  
...  
Keyword(s):  
Grain Size ◽  
Grain Refinement ◽  
Milling Process ◽  
Mg Alloy ◽  
Matrix Composites ◽  
Magnesium Matrix Composites ◽  
Pinning Effect ◽  
Average Grain Size ◽  
The Matrix ◽  
Hot Press Sintering

In this work, vanadium particles (VP) were utilized as a novel reinforcement of AZ31 magnesium (Mg) alloy. The nanocrystalline (NC) AZ31–VP composites were prepared via mechanical milling (MM) and vacuum hot-press sintering. During the milling process, the presence of VP contributed to the cold welding and fracture mechanism, resulting in the acceleration of the milling process. Additionally, increasing the VP content accelerated the grain refinement of the matrix during the milling process. After milling for 90 h, the average grain size of AZ31-X wt % Vp (X = 5, 7.5, 10) was refined to only about 23 nm, 19 nm and 16 nm, respectively. In the meantime, VP was refined to sub-micron scale and distributed uniformly in the matrix, exhibiting excellent interfacial bonding with the matrix. After the sintering process, the average grain size of AZ31-X wt % VP (X = 5, 7.5, 10) composites still remained at the NC scale, which was mainly caused by the pinning effect of VP. Besides that, the porosity of the sintered composites was no more than 7.8%, indicating a good densification effect. As a result, there was little difference between the theoretical and real density. Compared to as-cast AZ31 Mg alloy, the microhardness of sintered AZ31-X wt % VP (X = 5, 7.5, 10) composites increased by 65%, 87% and 96%, respectively, owing to the strengthening mechanisms of grain refinement strengthening, Orowan strengthening and load-bearing effects.

Significance of High Rate Superplasticity in Metallic Materials

1990 ◽  
Vol 196 ◽  
Author(s):  
Norio Furushiro ◽  
Shigenori Hori
Keyword(s):  
Grain Size ◽  
High Strain Rate ◽  
Strain Rate ◽  
Grain Refinement ◽  
Fine Particles ◽  
High Strain ◽  
High Rate ◽  
High Temperature Deformation ◽  
Temperature Deformation ◽  
Al Alloy

ABSTRACTIt has been expected that “High rate superplastic materials” will be developed for industrial applications. The Dorntype equation for high temperature deformation suggests that strain rate can be increased if the grain size is decreased. This means that grain refinement can effectively establish high strain rate superplastic materials.It is well known that a high degree of grain size refinement will result from the addition of zirconium to Al-base alloys. Powder-metallurgical processing with rapidly solidified powders is also available for the improvement of superplasticity by both the refinement of the solidified structure and the maintenance of the stable fine structure of a 7475 Al alloy during recrystallization and deformation. Therefore. P/M 7475 Al alloys containing Zr up to 0.9 wt% were selected as candidate specimens. The objective of the present paper includes the clarification of the role and the effective amount of Zr to obtain high strain rate superplastic materials. As a result, the addition of 0.3%Zr or more is effective in grain refinement of the P/M 7475 Al alloy. However, alloys containing 0.7 and 0.9 wt%Zr only show superplasticity at 793K. The optimum strain rate is shifted to a higher range with increasing Zr. The alloy of 7475 Al-0.9%Zr shows the maximum elongation of 900% at the remarkably high strain rate of 3.3×10−1 s−1.The deformation mechanism of such high stain rate superplasticity will be discussed briefly, by considering the effect of the fine particles of Zr on superplastic behavior.

Application of High-Pressure Sliding for Grain Refinement of Al and Mg Alloys

2010 ◽  
Vol 667-669 ◽  
pp. 91-96 ◽  
Author(s):  
Kiyonari Tazoe ◽  
Shuji Honda ◽  
Z. Horita
Keyword(s):  
High Pressure ◽  
Strain Rate ◽  
Grain Refinement ◽  
High Pressure Torsion ◽  
Initial Strain Rate ◽  
Mg Alloys ◽  
Initial Strain ◽  
Mg Alloy ◽  
Al Alloy ◽  
Average Grain Size

An earlier study showed that high-pressure sliding (HPS) is effective for grain refinement of pure Al in a rectangular sheet form using the principle of high-pressure torsion. In this study, the HPS is applied for grain refinement of an Al-3%Mg-0.2%Sc alloy and an AZ61 Mg alloy. HPS was conducted under a pressure of 1 GPa with sliding distances of 10 to 30 mm at room temperature for the Al alloy and at 473 K for the Mg alloy The average grain size is ~300 nm for both the Al and Mg alloys, respectively. Tensile tests showed that a superplastic elongation of ~1500% is achieved in the Al-3%Mg-0.2%Sc alloy at 573 K with an initial strain rate of 3.3x10-3 s-1 and of ~600% in the AZ61 alloy at 573 K with an initial strain rate of 1x10-3 s-1.

Grain Refinement during Superplastic Deformation of Coarse-Grained Al-Mg-Cu Alloys

2006 ◽  
Vol 509 ◽  
pp. 75-80 ◽  
Author(s):  
M.I. Cruz-Palacios ◽  
D. Hernández-Silva ◽  
L.A. Barrales-Mora ◽  
M.A. García-Bernal
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Grain Refinement ◽  
Strain Rate Sensitivity ◽  
Rate Sensitivity ◽  
Mg Alloy ◽  
Coarse Grained ◽  
Dislocation Creep ◽  
Rolled Plate ◽  
Strain Rates

In the present study the superplastic behavior of Al-6%Mg–0.5%Cu and Al–8%Mg– 0.5%Cu in a coarse grain size condition has been studied. The alloys are melted in an electrical furnace under argon atmosphere. The ingots (25 mm thick) are homogenized at 400 °C during 72 h and then rolled at 430 °C to a thickness of 5 mm. The mean grain size after rolling is 55 µm for the 6%Mg alloy and 61 µm for the 8%Mg alloy. Tensile test specimens are machined from the rolled plate in the rolling direction. Strain-rate-change tests at temperatures between 300 and 450 °C and strain rates between 1x10-4 and 1x10-1 s-1 are carried out to determine the strain rate sensitivity of the flow stress. Finally, elongation to failure tests are conducted at temperatures and strain rates where the alloys show a high strain rate sensitivity. Elongations higher than 390 % are obtained for the 8%Mg alloy. It is observed that the grip regions of the deformed samples show coarser grains than the regions near to the fracture surface. This means that grain refinement takes place during deformation, suggesting that the principal deformation mechanism is dislocation creep.

High temperature creep strength in a nanodispersion-strengthened ferritic alloy prepared by heavy plastic deformation

2011 ◽  
Vol 1298 ◽  
Author(s):  
David G. Morris ◽  
Maria Antonia Muñoz-Morris
Keyword(s):  
Plastic Deformation ◽  
Grain Size ◽  
High Temperature ◽  
Creep Strength ◽  
High Strain ◽  
Ferritic Steels ◽  
Al Alloy ◽  
Second Phase ◽  
Corrosion Properties ◽  
Wide Range

ABSTRACTProcesses of severe plastic deformation have been investigated for a wide range of ductile alloys over the past decade, generally with an objective of refining the microstructural scale, for example the grain size, but have hardly been considered for intermetallics. This presentation discusses processing of a boride-containing Fe3Al alloy using a multidirectional, high-strain and high-temperature forging technique. Iron aluminides with relatively low Al contents can be regarded as Al-rich ferritic steels with outstanding oxidation-corrosion properties. However, as for many ferritic steels, they show poor creep resistance at temperatures above about 600ºC. The deformation processing leads to a material with large grain size and refined dispersion of thermally-stable boride particles. The particles produce a large increase in creep strength under conditions of moderate stresses and low strain rates at temperatures near 700ºC. This high-strain forging technique can be seen as an intermediate processing method between conventional wrought metallurgy and mechanical-alloying powder metallurgy, whereby an initially coarse and inhomogeneous dispersion of second phase is refined and made more homogeneous, and can be considered as a useful processing technique for a wide range of particle-containing materials.

Influence of SiC Particles on the Grain Refinement of an Mg-Al Alloy

2009 ◽  
Vol 618-619 ◽  
pp. 445-448 ◽  
Author(s):  
Andreas Schiffl ◽  
Mark Easton
Keyword(s):  
Grain Size ◽  
Phase Equilibria ◽  
Grain Refinement ◽  
Al Alloys ◽  
Al Alloy ◽  
Grain Refiner ◽  
Sic Particles ◽  
Ternary Carbides

SiC particles are effective grain refiners in Mg-Al alloys. Several investigations, from different researchers, into their effect on a range of alloys with different Al contents has been undertaken and it has been found that the greatest reduction in grain size occurs in alloys having low Al contents. Performing grain refinement studies on a range of alloy contents also allows for further investigation into the mechanisms of grain refinement. It was found that the size of the SiC particles is also important in magnesium grain refinement. However, the presence of Mg2Si in the microstructure and the consideration of phase equilibria suggest that SiC can transform into other binary or ternary carbides. If such carbides are formed, they may also act as an effective grain refiner for Mg-Al alloys. In this study, the possibility of formation of new carbides (Al4C3, Al2MgC2, Mn7C3, Mg2C, Mg2C3, Al2CO etc.) and their ability to be good grain refiners for Mg-Al alloys is discussed.

Microstructures and Mechanical Properties of Mg Alloy after Severe Torsion Straining Process

2006 ◽  
Vol 503-504 ◽  
pp. 949-954 ◽  
Author(s):  
Yuichi Miyahara ◽  
N. Emi ◽  
Koji Neishi ◽  
Katsuaki Nakamura ◽  
Kenji Kaneko ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Grain Refinement ◽  
Room Temperature ◽  
Rotation Speed ◽  
Continuous Process ◽  
Mg Alloy ◽  
Compression Tests ◽  
Moving Speed ◽  
Az61 Mg Alloy

Grain refinement is attempted using severe plastic deformation (SPD) through the severe torsion straining process (STSP) which we have developed recently. The STSP is a continuous process for grain refinement without requirement of any die. In this study, an AZ61 Mg alloy was subjected to STSP at a temperature of 573 K with a rotation speed of 10 rpm and a moving speed of 200 mm/min. With this process, an initial grain size of ~20 μm was reduced to ~2~3 μm. Room temperature compression tests revealed that there were no cracks after 15% of compression for the STSP sample whereas fracture occurred for a conventionally extruded sample. For compression tests at 473 K, no cracks occurred in the STSP samples after 80% compression but compression was feasible without cracking only up to 20% for an extruded sample. It is shown that the STSP can be useful for grain refinement and ductility improvement of the AZ61 Mg alloy.

Control of Grain Size and Texture in Al Alloys Utilizing Friction Stir Processing

2007 ◽  
Vol 539-543 ◽  
pp. 3769-3774 ◽  
Author(s):  
Toshiya Shibayanagi ◽  
Masaaki Naka
Keyword(s):  
Grain Size ◽  
Aluminum Alloys ◽  
Grain Refinement ◽  
Grain Growth ◽  
Rotation Speed ◽  
Al Alloys ◽  
Abnormal Grain Growth ◽  
Texture Development ◽  
Al Alloy ◽  
Friction Stir

The present paper deals with the control of microstructure of friction stir processed aluminum alloys focusing on grain refinement, thermal stability at elevated temperature and texture development in some aluminum alloys such as 5083, 6061 and 7075 commercial aluminum alloys. 3mm thickness plates of 5083, 6061 and 7075 Al alloys were friction stir processed/welded with several rotation speeds and travelling speeds. Optical microscopy revealed the grain refinement in the stirred zone of each alloy and the average grain size decreased with decreasing rotation speed under various travelling speeds. Annealing of the joints brought about abnormal grain growth at temperatures higher than 773K for 5083 alloy. Critical temperature of the abnormal grain growth tended to decrease as the rotation speed decreased for the fixed travelling speed. Dissimilar joining of 5083 Al alloy to 6061 Al alloy also showed abnormal grain growth when annealed at 773K. A peculiar texture development of 7075 Al joint showing (111)//ND-oriented grains existing throughout the nugget was revealed by EBSP analysis.

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