Effect of Nd and Y Addition on Microstructure and Mechanical Properties of Extruded Mg-Zn-Zr Alloy

2007 ◽  
Vol 546-549 ◽  
pp. 413-416 ◽  
Author(s):  
Qiang Li ◽  
Qu Dong Wang ◽  
Da Quan Li ◽  
Wen Jiang Ding

The effect of Nd and Y addition on the microstructure and mechanical properties of as-extruded Mg-Zn-Zr magnesium alloy has been investigated in this study. The Mg-Zn-Zr alloy had 11 μm average grain size due to dynamic recrystallization during hot extrusion; but the average grain sizes of the Mg-Zn-Nd-Y-Zr alloys were markedly reduced to 4 μm by Nd and Y additions. The lamellar α-Mg + T phase or α-Mg + W phase eutectics at grain boundaries in as-cast Mg-Zn-Nd-Y-Zr alloys were broken up and MgZn2 precipitates in the matrix are obtained during hot extrusions. The mechanical properties of as-extruded Mg-Zn-Zr alloy were improved significantly by Nd and Y additions, especially the elevated temperature strength, which was above 150 MPa in ultimate tensile strength at 250 °C. These may be ascribed to the very fine grain size, the dispersed T phase or W phase and the MgZn2 type Laves phase precipitating during hot extrusion.

2005 ◽  
Vol 488-489 ◽  
pp. 385-388
Author(s):  
Qiang Li ◽  
Qu Dong Wang ◽  
Xiao Qing Zeng ◽  
Wen Jiang Ding ◽  
Quanbo Tang ◽  
...  

Nd, Y and Ca containing Mg-Zn-Zr alloys are produced by electromagnetic direct-chilling casting process, and extruded at a temperature of 643K with two extrusion ratios of 38:1 and 22:1, respectively. The grain size is markedly reduced from 80µm in as-cast alloy to 2~5µm in as-extruded alloy due to dynamic recrystallization, and lamellar eutectics at grain boundaries in as-cast alloy are broken up and fine precipitates in the matrix come forth during hot extrusions. Mechanical properties of the alloys are measured by tensile test from room temperature to 523K. Nd, Y and Ca are favorable to the strength of the hot-extruded alloy, especially the elevated-temperature strength, which is above 200MPa in ultimate tensile strength at 523K.


2008 ◽  
Vol 141-143 ◽  
pp. 713-718 ◽  
Author(s):  
Jun Xu ◽  
Shao Ming Zhang ◽  
Bi Cheng Yang ◽  
Li Kai Shi ◽  
Z. Fan

A new rheo-extrusion technique has been developed to produce extruded profiles. The AZ31 slurry is fabricated by a twin-screw mechanism, and has spheroidal solid particles with a grain size of about 50 to 80μm. The slurry was introduced into an extrusion container with an inner diameter of 95mm, and then squeezed to a billet before extruding into a round bar with a diameter of 22mm using a 500kN extrusion machine. It is found that the new technique has a lower deformation resistance than that of the conventionally hot extrusion technique in the same extrusion velocity. The microstructure and mechanical properties of the rheo-extruded bars were examined in detail. The results illustrated that grains of the bar were very fine with the average grain size about 2.3μm,and the mechanical properties were improved substantially compared with those of the same alloy produced by the conventional hot extrusion.


2007 ◽  
Vol 546-549 ◽  
pp. 105-108 ◽  
Author(s):  
Qu Dong Wang ◽  
Da Quan Li ◽  
Qiang Li ◽  
Wen Jiang Ding

Microstructure and mechanical properties of Mg-Zn-Er-Zr alloys were characterized in detail. The grain size of as-cast Mg-Zn-Er-Zr alloy was greatly decreased by the Mg-Zn-Er phases formed at grain boundaries. The addition of Er can increase the yield strength (YS) but decrease the ultimate tensile strength (UTS) and elongation of as-cast Mg-Zn-Zr alloy. The thermally stable Mg-Zn-Er phases were just partially dissolved into the matrix during solution treatment. And the addition of Er can prolong the precipitation process of Mg-Zn-Zr alloy. Solution-plus-ageing treatment can increase the strength of both the Mg-Zn-Zr and Mg-Zn-Er-Zr alloys, but the strengthening effect of Mg-Zn-Er-Zr alloy was greatly weakened, for the incompletely solution of Mg-Zn-Er phases. Er can greatly enhance the high temperature elongation of Mg-Zn-Zr alloy, but the increase of high temperature tensile strength was just a little.


2013 ◽  
Vol 774-776 ◽  
pp. 791-794
Author(s):  
Dong Mei Jiang ◽  
Liang Guo ◽  
Zhan Yi Cao ◽  
Xu Sun ◽  
Feng Xiao Huang

The microstructure and mechanical properties of the as-cast Mg-Zn-Ca-Zr alloys were investigated in this study. The results showed that the alloy was mainly composed of α-Mg solid solution and the secondary phases of Ca2Mg6Zn3. The grain size of alloys decreased from 82 μm to 38 μm with Zr content from 0.1% to 0.5%. The addition of Zr greatly improved the ultimate tensile strength (σb) and elongation (ε), while slightly improved the tensile yield strength (σ0.2). The σb, ε and σ0.2 of the Mg-4Zn-0.5Ca-0.5Zr were 196MPa, 85MPa and 16.1% compared with the other two alloys. The reason was that grain size refinement strengthening enhanced the mechanical properties.


2010 ◽  
Vol 667-669 ◽  
pp. 457-461
Author(s):  
Wei Guo ◽  
Qu Dong Wang ◽  
Man Ping Liu ◽  
Tao Peng ◽  
Xin Tao Liu ◽  
...  

Cyclic channel die compression (CCDC) of AZ31-1.7 wt.% Si alloy was performed up to 5 passes at 623 K in order to investigate the microstructure and mechanical properties of compressed alloys. The results show that multi-pass CCDC is very effective to refine the matrix grain and Mg2Si phases. After the alloy is processed for 5 passes, the mean grain size decreases from 300 μm of as-cast to 8 μm. Both dendritic and Chinese script type Mg2Si phases break into small polygonal pieces and distribute uniformly in the matrix. The tensile strength increases prominently from 118 MPa to 216 MPa, whereas the hardness of alloy deformed 5 passes only increase by 8.4% compared with as-cast state.


2011 ◽  
Vol 683 ◽  
pp. 103-112 ◽  
Author(s):  
B. Yang

The evolution of the microstructure and mechanical properties of electrodeposited nanocrystalline Ni with different annealing procedures was studied systematically. For the annealed specimens hardness decreases with increasing average grain size but the dependence changes at different grain size ranges. The specimens annealed at a low temperature show higher hardness compared to the as-deposited nanocrystalline Ni, despite an increased measured average grain size. In association with this hardening an increase in elastic modulus and a decrease in microstrain was observed after annealing. With increasing annealing temperature both the tensile strength and the fracture strain were observed to decrease, this is companied with a transition from ductile to brittle in the fracture surfaces. These results indicated that the mechanical behaviour of nanocrystalline Ni depends not only on the average grain size but also on the grain boundary structure. A change in the grain boundary state arising from annealing may be responsible for the observed increase in hardness and elastic modulus as well as the deterioration of tensile properties.


2018 ◽  
Vol 37 (1) ◽  
pp. 97-103 ◽  
Author(s):  
Hansong Xue ◽  
Xinyu Li ◽  
Weina Zhang ◽  
Zhihui Xing ◽  
Jinsong Rao ◽  
...  

AbstractThe effects of Bi on the microstructure and mechanical properties of AZ80-2Sn alloy were investigated. The results show that the addition of Bi within the as-cast AZ80-2Sn alloy promotes the formation of Mg3Bi2 phase, which can refine the grains and make the eutectic phases discontinuous. The addition of 0.5 % Bi within the as-extruded AZ80-2Sn alloy, the average grain size decreases to 12 μm and the fine granular Mg17Al12 and Mg3Bi2 phases are dispersed in the α-Mg matrix. With an increase in Bi content, the Mg17Al12 and Mg3Bi2 phases become coarsened and the grain size increases. The as-extruded AZ80-2Sn-0.5 %Bi alloy has the optimal properties, and the ultimate tensile strength, yield strength and elongation are 379.6 MPa, 247.1 MPa and 14.8 %, respectively.


2011 ◽  
Vol 391-392 ◽  
pp. 32-36 ◽  
Author(s):  
Bin Liu ◽  
Jing Huai Zhang ◽  
Zhong Yi Niu ◽  
Jun Qing Li

The as-cast Mg-14Li-3Al-(0-0.9)RE alloys were prepared with vacuum melting method, then processed by hot extrusion. The microstructure and tensile properties were investigated. The results show that both addition of RE and extrusion deformation can refine the grain size. Al3La compounds are formed with addition of La-rich misch metal. The as-extruded Mg-14Li-3Al-0.6RE alloy obtains the finest grain size (4.28 μm) and the highest mechanical properties (σb=222.75 MPa, δ=23.8%), which is related to the grain refinement and the formation of Al3La.


2012 ◽  
Vol 724 ◽  
pp. 481-485
Author(s):  
Kuk Hyun Song ◽  
Kazuhiro Nakata

This study evaluated the microstructure and mechanical properties of friction stir welded lap joints. Inconel 600 and SS 400 as experimental materials were selected, and friction stir welding was carried out at tool rotation speed of 200 rpm and welding speed of 100 mm/min. Applying the friction stir welding was notably effective to reduce the grain size of the stir zone, as a result, the average grain size of Inconel 600 was reduced from 20 μm in the base material to 8.5 μm in the stir zone. Joint interface between Inconel 600 and SS 400 showed a sound weld without voids and cracks. Also, the hook, along the Inconel 600 alloy from SS 400, was formed at advancing side, which directly affected an increase in peel strength. In this study, we systematically discussed the evolution on microstructure and mechanical properties of friction stir lap jointed Inconel 600 and SS 400.


2021 ◽  
Vol 40 (1) ◽  
pp. 300-309
Author(s):  
Sheng Huang ◽  
Changrong Li ◽  
Zhiying Li ◽  
Zeyun Zeng ◽  
Yongqiang Zhai ◽  
...  

Abstract HRB500E seismic steel bars are mainly used in high-rise buildings near the seismic zone. The influence of different niobium contents (0–0.023%) on the microstructure and mechanical properties of HRB500E seismic reinforcement was studied. Results showed that the grain size of ferrite was between 3.6 and 8.3 μm when only V was added. Meanwhile, as the niobium content increases, the ferrite particles are further refined. After adding niobium, the grain contribution increased by 9%. The addition of niobium significantly refined the grain size of HRB500E seismic reinforcement. The second-phase nano-elliptic precipitate is NbC. The precipitated phase is dispersed on the grain boundary and the matrix, and the dislocation density on the matrix promotes the precipitation of NbC particles along the dislocation line. The second-phase precipitation of niobium can form an effective pinning effect and then refine the pearlite spacing. The microhardness and the tensile strength also significantly improved. The yield strength increased from 509 to 570 MPa.


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