Strength and Plasticity of Ultra-Fine Grained Zirconium at Low Temperatures

2008 ◽  
Vol 584-586 ◽  
pp. 452-457
Author(s):  
Elena D. Tabachnikova ◽  
Aleksey V. Podolskiy ◽  
Vladimir Z. Bengus ◽  
S.N. Smirnov ◽  
V.D. Natsik ◽  
...  
Keyword(s):  
Considerable Increase ◽  
Activation Volume ◽  
Mutual Influence ◽  
Large Strain ◽  
Coarse Grained ◽  
Simultaneous Action ◽  
Fine Grained ◽  
Grain Sizes ◽  
Strength And Plasticity ◽  
Two Stages

Plasticity of ultra-fine grained (UFG) zirconium (grain size ~ 0.4 µm), produced by intensive plastic deformation (IPD) - a combination of extrusion, annealing, and drawing, have been studied within the temperature range 300 – 4.2 K in uniaxial compression. It was found that decrease of grain sizes in the result of IPD leads to considerable increase of strength characteristics for the UFG zirconium in comparison with coarse-grained (CG) zirconium (in 6 times at 300 K and 4 times at 77 K); and plasticity of the UFG zirconium keeps rather large (strain > 0.15). Two stages of the strain-hardening and decrease of the activation volume for plastic flow with deformation have been registered. A conclusion was made about the identity of basic deformation mechanisms in the UFG and CG zirconium: simultaneous action and mutual influence of intragrain dislocation gliding and twinning.

scholarly journals Sintering of a fine-grained BaCeO3 powder obtained from a co-precipitation method

2018 ◽  
Author(s):  
Roberto Köferstein
Keyword(s):  
Precursor Powder ◽  
Coarse Grained ◽  
Precipitation Method ◽  
Fine Grained ◽  
Grain Sizes ◽  
Three Phase ◽  
Sintering Behaviour ◽  
Co Precipitation ◽  
Precursor Powders ◽  
Powder Compacts

The formation of BaCeO3 by a co-precipitation method is described herein. The coprecipitationroute leads to an orange (BaCe)-precursor powder (1). To improve the sinteringbehaviour, a small amount of Ge4+ was incorporated, leading to a (BaCe0.95/Ge0.05)-precursor(2). Both precursor powders results in fine-grained preceramic powders (1A, 2A) aftercalcination. The shrinkage and sintering behaviour of resulting powder compacts were studiedin comparison to a coarse-grained mixed-oxide BaCeO3 powder (3). Compacts of 2A reach arelative density of 90 % after sintering at 1350 °C with grain-sizes between 0.9−3.2 μm. Onthe other hand ceramics of 1A and 3 have, after sintering at 1500 °C (10 h), relative densitiesof 85 % and 76 %, respectively. Ceramic bodies of 1A consisted of phase-pure orthorhombicBaCeO3, whereas bodies of 2A show reflections of BaCeO3 and a Ba2GeO4 phase. DTAinvestigations of samples 1A and 2A reveal three phase transitions at 255 °C (1A) and 256 °C (2A) as well as 383 °C (1A) and 380 °C (2A). A very weak one can be obtained in the range880−910 °C

Finite Element Simulation of Cyclic Channel Die Compression with Route A

2010 ◽  
Vol 44-47 ◽  
pp. 1300-1304
Author(s):  
Feng Jian Shi ◽  
Tao Xu ◽  
Sheng Lu ◽  
Lei Gang Wang
Keyword(s):  
Finite Element ◽  
Large Strain ◽  
Effective Strain ◽  
Central Zone ◽  
Peripheral Zone ◽  
Linear Increase ◽  
Rigid Plastic ◽  
Compression Load ◽  
Fine Grained ◽  
Two Stages

In this paper, effective strain and load were simulated by rigid-plastic finite element method (FEM) during cyclic channel die compression (CCDC) with route A, and the optical microstructure was observed. The results show that large strain can be accumulated in the material by CCDC. The load variation includes two stages, slowly linear increase and rapid increase. At the end of the CCDC, the compression load rises rapidly. Apart from the edges of the specimen, the effective strain is higher in the central region and lower at the surrounding region. The effective strain gradient increases with the number of compression. Grain refinement at the central zone is faster due to the strain inhomogeneity. But the peripheral zone is also refined with the number of CCDC. This illustrates CCDC is a promising method for producing bulk ultra-fine grained materials.

Studies with the intraruminal selenium pellet. 2. The effect of grain size of selenium on the functional life of pellets in sheep

1981 ◽  
Vol 32 (6) ◽  
pp. 935 ◽  
Author(s):  
DR Hudson ◽  
RA Hunter ◽  
DW Peter
Keyword(s):  
Grain Size ◽  
Progressive Increase ◽  
Coarse Grained ◽  
Elemental Selenium ◽  
Average Composition ◽  
Plasma Selenium ◽  
Iron Selenide ◽  
Fine Grained ◽  
Grain Sizes

Grain size of elemental selenium is a major factor controlling the long-term effectiveness of intraruminal selenium pellets. Microscope studies of polished sections of new and used selenium pellets showed that two commercially manufactured pellets contained selenium with average grain sizes about 4 and 40 �m respectively. Plasma selenium concentrations in sheep treated with pellets containing the coarse-grained selenium were maintained at higher levels over longer periods of time than those measured for sheep treated with pellets with fine-grained selenium. Pellets removed from sheep after 2, 4, 8, 16 and 28 days showed a progressive increase in the degree of alteration of selenium to a compound of average composition (g/100 g) iron, 33.7; selenium, 51.3 ; oxygen, 15.0. After 28 days only a small percentage of elemental selenium remained in pellets with fine-grained selenium, whereas about 50% remained in pellets with coarse-grained selenium. CSIRO prototype pellets, for which long-term effectiveness had been established, also contained coarse-grained selenium, and remnants of selenium were found in pellets that had been in sheep for periods up to 3 years. Selenium, administered in gelatin capsules or as sachets containing glass-selenium mixtures, was stable under the pH-Eh conditions of the rumen, but was rendered unstable in selenium pellets or iron-selenium mixtures by the presence of iron. It is probable that the most rapid release of selenium to the sheep occurs as a result of a chemical reaction involving the oxidation of iron and concomitant alteration of elemental selenium to iron selenide.

Effect of Grain Size on Mechanical Properties of Dual Phase Steels Composed of Ferrite and Martensite

MRS Advances ◽  
2016 ◽  
Vol 1 (12) ◽  
pp. 811-816 ◽  
Author(s):  
Myeong-heom Park ◽  
Akinobu Shibata ◽  
Nobuhiro Tsuji
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
Tensile Test ◽  
Coarse Grained ◽  
Dual Phase ◽  
Fine Grained ◽  
Grain Sizes ◽  
Dp Structure ◽  
Dp Steels

ABSTRACTIt is well-known that dual phase (DP) steels composed of ferrite and martensite have good ductility and plasticity as well as high strength. Due to their excellent mechanical properties, DP steels are widely used in the industrial field. The mechanical properties of DP steels strongly depend on several factors such as fraction, distribution and grain size of each phase. In this study, the grain size effect on mechanical properties of DP steels was investigated. In order to obtain DP structures with different grain sizes, intercritical heat treatment in ferrite + austenite two-phase region was carried out for ferrite-pearlite structures having coarse and fine ferrite grain sizes. These ferrite-pearlite structures with coarse and fine grains were fabricated by two types of heat treatments; austenitizing heat treatment and repetitive heat treatment. Ferrite grain sizes of the specimens heat-treated by austenitizing and repetitive heat treatment were 47.5 µm (coarse grain) and 4.5 µm (fine grain), respectively. The ferrite grain sizes in the final DP structures fabricated from the coarse-grained and fine-grained ferrite-pearlite structures were 58.3 µm and 4.1µm, respectively. The mechanical behavior of the DP structures with different grain sizes was evaluated by an uniaxial tensile test at room temperature. The local strain distribution in the specimens during tensile test was obtained by a digital image correlation (DIC) technique. Results of the tensile test showed that the fine-grained DP structure had higher strength and larger elongation than the coarse-grained DP structure. It was found by the DIC analysis that the fine-grained DP structure showed homogeneous deformation compared with the coarse-grained DP structure.

Combined In Situ Neutron Diffraction and Acoustic Emission of Twin Nucleation & Twin Growth in Extruded ZM20 Mg Alloy

2010 ◽  
Vol 652 ◽  
pp. 149-154 ◽  
Author(s):  
Ondrej Muránsky ◽  
Matthew R. Barnett ◽  
David G. Carr ◽  
Sven C. Vogel ◽  
E.C. Oliver
Keyword(s):  
Acoustic Emission ◽  
Neutron Diffraction ◽  
Room Temperature ◽  
Coarse Grained ◽  
Fine Grained ◽  
Grain Sizes ◽  
Twin Nucleation ◽  
Twin Growth ◽  
In Situ Neutron Diffraction

In the present work in situ neutron diffraction and acoustic emission were used concurrently to study deformation twinning in two ZM20 Mg alloys with significantly different grain sizes at room temperature. The combination of these techniques allows differentionation between the twin nucleation and the twin growth mechanisms. It is shown, that yielding and immediate post-yielding plasticity in compression is governed primarily by twin nucleation, whereas the plasticity at higher strains is governed by twin growth. The current results further suggest that yielding by twinning happens in a slightly different manner in the fine-grained as compared to the coarse-grained alloy.

Grain Size Dependence of the Flow Stress of TWIP Steel

2010 ◽  
Vol 654-656 ◽  
pp. 294-297 ◽  
Author(s):  
Ghasem Dini ◽  
Rintaro Ueji ◽  
Abbas Najafizadeh
Keyword(s):  
Grain Size ◽  
Flow Stress ◽  
Twip Steel ◽  
Strengthening Mechanism ◽  
Mechanical Twinning ◽  
Coarse Grained ◽  
Strengthening Effect ◽  
Fine Grained ◽  
Hardening Behavior ◽  
Grain Sizes

The effect of grain size on the flow stress in TWinning Induced Plasticity (TWIP) steel was investigated via the X-ray diffraction (XRD) measurements of dislocation density. The results indicated that the hardening behavior of fine grained samples (mean grain sizes in the range of 2.1-3.8μm) can be described as typical dislocation interactions. However in coarse grained samples (mean grain sizes in the range of 4.7-38.5μm) where extensive mechanical twinning occurs, another strengthening mechanism is required. Consequently, the effect of grain size on the flow stress parameters of the proposed equation was considered and it was found that in the fine grained samples, the Holloman analysis can describe the hardening behavior. However, in coarse grained samples, a second hardening term due to the strengthening effect of mechanical twin boundaries needs to be added to the Holloman equation.

scholarly journals Pliocene–Pleistocene basin evolution along the Garlock fault zone, Pilot Knob Valley, California

Geosphere ◽  
2020 ◽  
Vol 16 (5) ◽  
pp. 1208-1224
Author(s):  
William M. Rittase ◽  
J. Douglas Walker ◽  
Joe Andrew ◽  
Eric Kirby ◽  
Elmira Wan
Keyword(s):  
Volcanic Field ◽  
Coarse Grained ◽  
Fine Grained ◽  
Grain Sizes ◽  
The North ◽  
Source Regions ◽  
Provenance Data ◽  
Garlock Fault ◽  
Depositional Patterns ◽  
Fourth Member

Abstract Exposed Pliocene–Pleistocene terrestrial strata provide an archive of the spatial and temporal development of a basin astride the sinistral Garlock fault in California. In the southern Slate Range and Pilot Knob Valley, an ∼2000-m-thick package of Late Cenozoic strata has been uplifted and tilted to the northeast. We name this succession the formation of Pilot Knob Valley and provide new chronologic, stratigraphic, and provenance data for these rocks. The unit is divided into five members that record different source areas and depositional patterns: (1) the lowest exposed strata are conglomeratic rocks derived from Miocene Eagle Crags volcanic field to the south and east across the Garlock fault; (2) the second member consists mostly of fine-grained rocks with coarser material derived from both southern and northern sources; and (3) the upper three members are primarily coarse-grained conglomerates and sandstones derived from the adjacent Slate Range to the north. Tephrochronologic data from four ash samples bracket deposition of the second member to 3.6–3.3 Ma and the fourth member to between 1.1 and 0.6 Ma. A fifth tephrochronologic sample from rocks south of the Garlock fault near Christmas Canyon brackets deposition of a possible equivalent to the second member of the formation of Pilot Knob Valley at ca. 3.1 Ma. Although the age of the base of the lowest member is not directly dated, regional stratigraphic and tectonic associations suggest that the basin started forming ca. 4–5 Ma. By ca. 3.6 Ma, the northward progradation fanglomerate sourced in the Eagle Crags region waned, and subsequent deposition occurred in shallow lacustrine systems. At ca. 3.3 Ma, southward progradation of conglomerates derived from the Slate Range began. Circa 1.1 Ma, continued southward progradation of fanglomerate with Slate Range sources is characterized by a shift to coarser grain sizes, interpreted to reflect uplift of the Slate Range. Overall, basin architecture and the temporal evolution of different source regions were controlled by activity on three regionally important faults—the Garlock, the Marine Gate, and the Searles Valley faults. The timing and style of motions on these faults appear to be directly linked to patterns of basin development.

scholarly journals Error annotation in the COPLE2 corpus

2018 ◽  
pp. 225-239
Author(s):  
Iria Del Rio ◽  
Amália Mendes
Keyword(s):  
Second Language Acquisition ◽  
Coarse Grained ◽  
Computer Assisted ◽  
Learner Corpus ◽  
Fine Grained ◽  
Error Annotation ◽  
Level Information ◽  
New Research ◽  
Two Stages ◽  
General Architecture

We present the general architecture of the error annotation system applied to the COPLE2 corpus, a learner corpus of Portuguese implemented on the TEITOK platform. We give a general overview of the corpus and of the TEITOK functionalities and describe how the error annotation is structured in a two-level system: first, a fully manual token-based and coarse-grained annotation is applied and produces a rough classification of the errors in three categories, paired with multi-level information for POS and lemma; second, a multi-word and fine-grained annotation in standoff is then semi-automatically produced based on the first level of annotation. The token-based level has been applied to 47% of the total corpus. We compare our system with other proposals of error annotation, and discuss the fine-grained tag set and the experiments to validate its applicability. An inter-annotator (IAA) experiment was performed on the two stages of our system using Cohen’s kappa and it achieved good results on both levels. We explore the possibilities offered by the tokenlevel error annotation, POS and lemma to automatically generate the fine-grained error tags by applying conversion scripts. The model is planned in such a way as to reduce manual effort and rapidly increase the coverage of the error annotation over the full corpus. As the first learner corpus of Portuguese with error annotation, we expect COPLE2 to support new research in different fields connected with Portuguese as second/foreign language, like Second Language Acquisition/Teaching or Computer Assisted Learning.

scholarly journals Provenance signals in metaturbidites of the Paleoproterozoic greenstone belt of the Guiana Shield in Suriname

2016 ◽  
Vol 95 (4) ◽  
pp. 467-489 ◽  
Author(s):  
R. Naipal ◽  
S.B. Kroonenberg
Keyword(s):  
Greenstone Belt ◽  
Factor Score ◽  
Coarse Grained ◽  
Turbidity Currents ◽  
Mafic Mineral ◽  
Source Areas ◽  
Fine Grained ◽  
Grain Sizes ◽  
Wide Range ◽  
Characteristic Features

AbstractThe sedimentological, metamorphic, petrographic and geochemical characteristics of the Armina Formation, part of the Paleoproterozoic Greenstone Belt of Suriname in South America, are described, based on field, geochemical and petrographic evidence obtained through fieldwork along the Marowijne River and study of diamond drill cores from Rosebel Gold Mine (RGM). The metagreywackes show characteristic features of deposition by turbidity currents: coarse-grained, poorly sorted graded greywackes, covered by fine-grained, parallel-laminated phyllitic beds, often with convolute structures and climbing ripples. Their immature character and composition suggest deposition in an arc-trench environment. In the Marowijne River three different facies of metagreywackes are distinguished: (1) the greyish Bonnidoro Falls facies, characterised by common red millimetre-sized pseudomorphs after siderite in the finer beds, (2) the green Paroe Tabiki metagreywacke facies, with decimetre-sized calcsilicate nodules, both metamorphosed in the lower greenschist facies with chlorite as the main mafic mineral, and (3) the grey Armina Falls metagreywacke facies, geochemically similar to the Bonnidoro type but of higher metamorphic grade with biotite as the main mafic mineral. The metagreywackes from the Marowijne River show a predominance of quartz, plagioclase and lithic (tonalitic) clasts, suggesting exhumation of tonalite–trondhjemite–granodiorite plutons before deposition of the turbidites. There is a slight increase in maturity from (1) to (3), suggesting increasing weathering in the source areas. The metagreywackes of the RGM (JZone) have a predominantly metavolcanic origin, suggesting that they have a different provenance area than the Marowijne metagreywackes. Geochemically the spread in composition within each facies is larger than between the facies because of the wide range in grain sizes in each turbidite sequence. A large part of the rocks from the RGM, classified by previous authors as arenites, are geochemically and petrographically metagreywackes. Only a few RGM samples are real arenites, and plot as a separate cluster in geochemical factor score plots because of their low Fe and Na contents.

Effect of Grain Size and Grain Boundary on Mechanical Yielding Behavior of Fully Stabilized Zirconia

2006 ◽  
Author(s):  
Jie Lian ◽  
Javier Garay ◽  
Junlan Wang
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Boundary ◽  
Boundary Effect ◽  
Coarse Grained ◽  
Stabilized Zirconia ◽  
Fine Grained ◽  
Grain Sizes ◽  
Reduced Modulus ◽  
Grain Boundary Effect

Mechanical properties of fully yttria stabilized zirconia (F-YSZ) with different grain sizes were investigated using instrumented indentation. While the grain size effect on the yield strength was performed on both the coarse-grained and fine-grained F-YSZ, the grain boundary effect was studied on the coarse-grained F-YSZ by performing nanoindentation within the grains and on/near the grain boundaries. Little variations were observed on mechanical properties such as hardness and reduced modulus, interesting results were obtained on the grain boundary effect on the yielding load for the course-grained F-YSZ.

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