Microstructure and Superconductive Property of MgB2/Al Composite Materials

2012 ◽  
Vol 706-709 ◽  
pp. 667-670
Author(s):  
Manabu Mizutani ◽  
Daisuke Tokai ◽  
Kenji Matsuda ◽  
Katsuhiko Nishimura ◽  
Tokimasa Kawabata ◽  
...  

MgB2has the higher critical temperature of superconducting transition (TC: 39K) among the intermetallic compound superconductive materials, however, MgB2is hard for practical use because of its unworkable and lower critical current density (JC) in a high magnetic field than Nb-based superconductive materials. We have developed the original method of three-dimensional penetration casting (3DPC) to fabricate the MgB2/Al composite materials. In the composite material we made, MgB2particles dispersed to the matrix uniformly. Thus, these composite materials can be processed by machining, extrusion and rolling. TheTCwas determined by electrical resistivity and magnetization to be about 37~39K. In this work, we made composite material with ground MgB2particle with the purpose of extruding thinner wires of composite material, successfully produced φ1mm wire and changed the matrix from pure Al to Al-In alloy.JCof composite materials with the matrix of Al-In alloy was calculated from the width of the magnetic hysteresis based on the extended Bean model. The result was better than that of MgB2/Al composite material without Indium. Microstructures of these samples had been confirmed by SEM observation.

2011 ◽  
Vol 409 ◽  
pp. 201-204
Author(s):  
Manabu Mizutani ◽  
Daisuke Tokai ◽  
Kenji Matsuda ◽  
Katsuhiko Nishimura ◽  
Tokimasa Kawabata ◽  
...  

MgB2has the higher critical temperature of superconducting transition (TC: 39K) among the intermetallic compound superconductive materials, however, MgB2is hard for practical use because of its unworkable and lower critical current density (JC) in a high magnetic field than Nb-based superconductive materials. We have developed the original method of three-dimensional penetration casting (3DPC) to fabricate the MgB2/Al composite materials. In the composite material we made, MgB2particles dispersed to the matrix uniformly. Thus, these composite materials can be processed by machining, extrusion and rolling. TheTCwas determined by electrical resistivity and magnetization to be about 37~39K. In this work, we made composite material with ground MgB2particle with the purpose of extruding thinner wires of composite material, successfully produced φ1mm wire and changed the matrix from pure Al to Al-In alloy.JCof composite materials with the matrix of Al-In alloy was calculated from the width of the magnetic hysteresis based on the extended Bean model. The result was better than that of MgB2/Al composite material without Indium. Microstructures of these samples had been confirmed by SEM observation.


2010 ◽  
Vol 654-656 ◽  
pp. 2759-2762
Author(s):  
Manabu Mizutani ◽  
Kenji Matsuda ◽  
Kazuya Makino ◽  
Katsuhiko Nishimura ◽  
Tokimasa Kawabata ◽  
...  

Superconducting wires have been applied for the fabrication of superconducting magnets in nuclear magneto-resonance (NMR), Magneto-resonance imaging (MRI) and so on. MgB2 has the highest critical temperature of superconducting transition (TC39K) among intermetallic compound superconductive materials. This means that MgB2 Superconductive wire doesn’t need expensive liquid He for cooling. We used the original method of the three-dimensional penetration casting (3DPC) in this laboratory to fabricate the MgB2/Al composite. Our 3DPC method for fabricating composite materials can disperse particles in the matrix homogenously without any aggregation and control volume fractions of composites within the range of 4 – 40%, even when particle size is less than 1 m. Thus, these composite materials can be processed by machining, extrusion and rolling. In the composite material we made, MgB2 particles dispersed to the Al matrix uniformly. The TC was determined by electrical resistivity and magnetization to be about 37 – 39K. We succeeded in extruding MgB2/Al composite billet to 1mm wire. Microstructures of these samples have been confirmed by SEM method. MgB2/Al composite billet and extruded wire were showed there no cracks inside the materials.


Author(s):  
O. Popoola ◽  
A.H. Heuer ◽  
P. Pirouz

The addition of fibres or particles (TiB2, SiC etc.) into TiAl intermetallic alloys could increase their toughness without compromising their good high temperature mechanical and chemical properties. This paper briefly discribes the microstructure developed by a TiAl/TiB2 composite material fabricated with the XD™ process and forged at 960°C.The specimens for transmission electron microscopy (TEM) were prepared in the usual way (i.e. diamond polishing and argon ion beam thinning) and examined on a JEOL 4000EX for microstucture and on a Philips 400T equipped with a SiLi detector for microanalyses.The matrix was predominantly γ (TiAl with L10 structure) and α2(TisAl with DO 19 structure) phases with various morphologies shown in figure 1.


2014 ◽  
Vol 918 ◽  
pp. 21-26
Author(s):  
Chen Kang Huang ◽  
Yun Ching Leong

In this study, the transport theorem of phonons and electrons is utilized to create a model to predict the thermal conductivity of composite materials. By observing or assuming the dopant displacement in the matrix, a physical model between dopant and matrix can be built, and the composite material can be divided into several regions. In each region, the phonon or electron scattering caused by boundaries, impurities, or U-processes was taken into account to calculate the thermal conductivity. The model is then used to predict the composite thermal conductivity for several composite materials. It shows a pretty good agreement with previous studies in literatures. Based on the model, some discussions about dopant size and volume fraction are also made.


Author(s):  
V. A. Kalinichenko ◽  
A. S. Kalinichenko ◽  
S. V. Grigoriev

To create friction pairs operating in severe working conditions, composite materials are now increasingly used. Composite materials obtained with the use of casting technologies are of interest due to the possibility to manufacture wide range of compositions at low price compared to powder metallurgy. Despite the fact that many composite materials have been sufficiently studied, it is of interest to develop new areas of application and give them the properties required by the consumer. In the present work the composite materials on the basis of silumin reinforced with copper granules were considered. Attention was paid to the interaction between the matrix alloy and the reinforcing phase material as determining the properties of the composite material. The analysis of distribution of the basic alloying elements in volume of composite material and also in zones of the interphases interaction is carried out. The analysis of the possibility of obtaining a strong interphase zone of contact between the reinforcing component and the matrix material without significant dissolution of the reinforcing material is carried out.


2001 ◽  
Vol 691 ◽  
Author(s):  
T. Sakakibara ◽  
Y. Takigawa ◽  
K. Kurosawa

ABSTRACTWe prepared a series of (AgBiTe2)1−x(Ag2Te)x(0≤×≤1) composite materials by melt and cool down [1]. The Hall coefficient and the electrical conductivity were measured by the standard van der Pauw technique over the temperature range from 93K to 283K from which the Hall carrier mobility was calculated. Ag2Te had the highest mobility while the mobility of AgBiTe2was the lowest of all samples at 283K. However the mobility of the (AgBiTe2)0.125(Ag2Te)0.875composite material was higher than the motility of Ag2Te below 243K. It seems that a small second phase dispersed in the matrix phase is effective against the increased mobility.


Author(s):  
V. T. Senyut

The article presents the results of a study of composite materials based on diamond-lonsdaleite abrasive (DLA) and various binders (Fe–Ti mechanocomposite, silicon carbide SiC). A metal-matrix composite material with a multimodal nano- and microlevel structure, characterized by increased adhesion of diamond grains to the binder, is obtained on the basis of impact diamonds and a Fe–Ti nano-mechanical composite. It is shown that the use of impact diamonds in comparison with synthetic diamonds makes it possible to reduce the pressure of thermobaric treatment by 30–50 % at the same sintering temperatures. The use of Fe–Ti–DLA composites in the process of magnetic-abrasive polishing (MAP) makes it possible to increase the removal rate of material based on silicon by 1.5–2 times and reduce the processing time by 30 % compared to ferroabrasive powder (FAP) based on synthetic diamonds. The effect of adding of silicon carbide on the process of obtaining a superhard composite material impact diamond – SiC is investigated. It is found that adding of SiC helps to reduce the defectiveness of the material and increase the homogeneity of its structure in comparison with the material without adding of a binder. In this case, an increase in the content of SiC and Si also leads to an inversion of the structure type of the superhard composite from polycrystalline to matrix. It is found that the additional use of amorphous soot and boron affects the refinement of the matrix structure of the composite material due to the formation of boron carbide and secondary finely dispersed silicon carbide.


2020 ◽  
pp. 121-129
Author(s):  
Андрій Володимирович Морозов

The processes occurring in composite materials are determined by differential equations in partial derivatives with variable coefficients. Most composite materials have a periodic structure, so the coefficients in the equations are rapidly oscillatory periodic functions. The most effective method for studying the stress and deformation field in structures made of composite materials is the method of finite elements, where a nonhomogeneous composite material is replaced by an equivalent homogeneous anisotropic material. To determine averaged characteristics of a composite material with a periodic structure requires a verified methodology allowing to do this. Therefore, the fundamental goal of the mechanics of composite materials is to calculate the effective elastic characteristics of the material. The paper considers the urgent issue of determining effective elastic characteristics of three-dimensional reinforced composite materials based on known elastic properties of fibers and matrix and distribution of reinforcing fibers by volume of composite material.The paper presents the mathematical modeling of the minimum three-dimensional representative volume element based on the specified reinforcement scheme and geometrical dimensions of components. Numerical experiments are performed with the ANSYS software package. A series of numerical experiments simulate six deformation cases: uniaxial tension in the X, Y, Z directions, and shear in the XY, YZ, and XZ planes. Numerical studies of the stress and strain state of the representative volume element of composite material determine the effective elastic constants of equivalent homogeneous material. Two series of calculations are performed with specifying appropriate symmetry and periodicity conditions.The results of the experimental study allow for the verification of the proposed methodology for determining the effective elastic characteristics of three-dimensional reinforced fiber composite materials. The developed numerical methodology enables us to solve the issues of the mechanics of composite materials with the help of modern software packages in the mathematical framework of which the finite element method is used.


2021 ◽  
Vol 7 (1) ◽  
pp. 085-090
Author(s):  
Sujita Darmo Darmo ◽  
Rudy Sutanto Sutanto

Fibrous composite materials continue to be researched and developed with the long-term goal of becoming an alternative to metal substitutes. Due to the nature of the fiber reinforced composite material, its high tensile strength, and low density compared to metal. In general, the composition of the composite consists of reinforcing fibers and a matrix as the binding material. The potential of natural fibers as a reinforcing composite material is still being developed and investigated. The research that has been done aims to determine the characteristics of the tensile strength of the composite strengthened with Hibiscus tiliaceust bark powder (HTBP) with alkaline NaOH and KOH treatment. The reinforcing material used is HTBP and the matrix is polyester resin, with volume fraction of 5%, 10% and 20% with an alkaline treatment of 5% NaOH and 5% KOH with immersion for 2 hours, 4 hours, 6 hours and 8 hours. Tensile testing specimens and procedures refer to ASTM D3039 standard. The results of this study showed the highest tensile strength of 34.96 MPa in the alkaline treatment of 5% KOH, soaking time of 8 hours with a volume fraction of 10% and the lowest tensile strength of 21.96 MPa of 5% KOH alkaline treatment, soaking time of 6 hours with a volume fraction of 20%. .with 10% volume fraction of 34.96 MPa and the lowest tensile strength was 5% KOH alkaline treatment at 6 hours immersion with 20% volume fraction.


2020 ◽  
Vol 2 (2) ◽  
pp. 170-174

Human health and environmental comfort are disturbed by the presence of noise, especially in cars, so that effective sound-absorbing materials are currently being developed. To answer the problem of noise in car interiors, polyester composite materials with local hemp fiber and nanocellulose reinforcement were developed. Natural fiber is biodegradable and renewable, and acts as an alternative to the use of synthetic fibers. The method used for the composite material manufacturing process was the casting method. The matrix of the composite material was polyester, while the reinforcement was a combination of local hemp fiber and nanocellulose fiber. Alkalization and non-alkalization processes have been carried out on hemp fiber. The composition of nanocellulose was 0%, 1%, and 3%. The characterization applied in this research were SEM test, FTIR test, sound transmission loss test, and density test. Optimal results were obtained on hemp fiber reinforced polyester composite materials without alkalization and without nanocellulose. Sound transmission loss (STL) was 61.91 dB up to 68.52 dB for the frequency range of 630 Hz to 125 Hz. The standard noise limit on 8-passenger passenger's four-wheeled vehicles is 77-80 dB. Based on the results obtained, the sound absorption is good. The density of this composite material was obtained at 0.989 gram/cm3. This composite material has the potential for developing dashboard material.


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