Study of Microstructure, Texture and Residual Stress in Asymmetrically Rolled Titanium

2014 ◽  
Vol 777 ◽  
pp. 1-6 ◽  
Author(s):  
Marcin Wronski ◽  
Krzysztof Wierzbanowski ◽  
Lucjan Pytlik ◽  
Brigitte Bacroix ◽  
Mirosław Wróbel ◽  
...  
Keyword(s):  
Residual Stress ◽  
X Ray Diffraction ◽  
Asymmetric Rolling ◽  
Rolling Mills ◽  
X Ray ◽  
Wide Range ◽  
Strong Shear ◽  
Angular Velocities ◽  
Ebsd Technique ◽  
Titanium Grade

Asymmetric rolling is a promising forming technique offering numerous possibilities of material properties modification and the improvement of technological process parameters. This geometry of deformation is relatively easy to implement on existing industrial rolling mills. Moreover, it can provide large volume of a material with modified properties. The study of microstructure, crystallographic texture and residual stress in asymmetrically rolled titanium (grade 2) is presented in this work. The above characteristics were examined using EBSD technique and X-ray diffraction. The rolling asymmetry was realized using two identical rolls, driven by independent motors, rotating with different angular velocities ω1 and ω2. This ensured a wide range of rolling asymmetry: A=ω1/ω2. It was found that a strong shear stress induced in the asymmetrically rolled material allowed to obtain a microstructure refinement, texture homogenization and lowering of residual stress.

scholarly journals Modification of Stress and Texture Distributions in Asymmetrically Rolled Titanium

2014 ◽  
Vol 996 ◽  
pp. 688-693 ◽  
Author(s):  
Marcin Wronski ◽  
Krzysztof Wierzbanowski ◽  
Andrzej Baczmański ◽  
Sebastian Wroński ◽  
Brigitte Bacroix ◽  
...  
Keyword(s):  
Residual Stress ◽  
Crystallographic Texture ◽  
Material Properties ◽  
X Ray Diffraction ◽  
Asymmetric Rolling ◽  
Rolling Mills ◽  
X Ray ◽  
Angular Velocities ◽  
Ebsd Technique ◽  
Titanium Grade

Asymmetric rolling can be used in order to modify material properties and to decrease forces and torques applied during deformation. This geometry of deformation is relatively easy to implement on existing industrial rolling mills and it can provide large volumes of a material. The study of microstructure, crystallographic texture and residual stress in asymmetrically rolled titanium (grade 2) is presented in this work. The above characteristics were examined using EBSD technique and X-ray diffraction. The rolling asymmetry was realized using two identical rolls, driven by independent motors, rotating with different angular velocities w1 and w2. It was found that asymmetric rolling leads to microstructure refinement, texture homogenization and lowering of residual stress.

scholarly journals Statistical analysis of the reproducibility of residual stress measurements in cold extruded parts

2021 ◽  
Author(s):  
Fabian Jaeger ◽  
Alessandro Franceschi ◽  
Holger Hoche ◽  
Peter Groche ◽  
Matthias Oechsner
Keyword(s):  
Residual Stress ◽  
Statistical Analysis ◽  
Stress Measurement ◽  
Industrial Applications ◽  
Cold Extrusion ◽  
X Ray Diffraction ◽  
Forming Process ◽  
X Ray ◽  
Stress States ◽  
Key Aspects

AbstractCold extruded components are characterized by residual stresses, which originate from the experienced manufacturing process. For industrial applications, reproducibility and homogeneity of the final components are key aspects for an optimized quality control. Although striving to obtain identical deformation and surface conditions, fluctuation in the manufacturing parameters and contact shear conditions during the forming process may lead to variations of the spatial residual stress distribution in the final product. This could lead to a dependency of the residual stress measurement results on the relative axial and circumferential position on the sample. An attempt to examine this problem is made by the employment of design of experiments (DoE) methods. A statistical analysis of the residual stress results generated through X-Ray diffraction is performed. Additionally, the ability of cold extrusion processes to generate uniform stress states is analyzed on specimens of austenitic stainless steel 1.4404 and possible correlations with the pre-deformed condition are statistically examined. Moreover, the influence of the coating, consisting of oxalate and a MoS2 based lubricant, on the X-Ray diffraction measurements of the surface is investigated.

scholarly journals Multidimensional Ln-Aminophthalate Photoluminescent Coordination Polymers

Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1786
Author(s):  
Carla Queirós ◽  
Chen Sun ◽  
Ana M. G. Silva ◽  
Baltazar de Castro ◽  
Juan Cabanillas-Gonzalez ◽  
...  
Keyword(s):  
Water Content ◽  
Coordination Polymers ◽  
Metal Ion ◽  
Low Cost ◽  
Microwave Assisted Synthesis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Wide Range ◽  
Ft Ir ◽  
Ft Ir Spectroscopy

The development of straightforward reproducible methods for the preparation of new photoluminescent coordination polymers (CPs) is an important goal in luminescence and chemical sensing fields. Isophthalic acid derivatives have been reported for a wide range of applications, and in addition to their relatively low cost, have encouraged its use in the preparation of novel lanthanide-based coordination polymers (LnCPs). Considering that the photoluminescent properties of these CPs are highly dependent on the existence of water molecules in the crystal structure, our research efforts are now focused on the preparation of CP with the lowest water content possible, while considering a green chemistry approach. One- and two-dimensional (1D and 2D) LnCPs were prepared from 5-aminoisophthalic acid and Sm3+/Tb3+ using hydrothermal and/or microwave-assisted synthesis. The unprecedented LnCPs were characterized by single-crystal X-ray diffraction (SCRXD), powder X-ray diffraction (PXRD), Fourier transform infrared (FT-IR) spectroscopy and scanning electron microscopy (SEM), and their photoluminescence (PL) properties were studied in the solid state, at room temperature, using the CPs as powders and encapsulated in poly(methyl methacrylate (PMMA) films, envisaging the potential preparation of devices for sensing. The materials revealed interesting PL properties that depend on the dimensionality, metal ion, co-ligand used and water content.

Simulation and Experiment on the Residual Stress in Super-High Speed Grinding

2010 ◽  
Vol 135 ◽  
pp. 238-242
Author(s):  
Yue Ming Liu ◽  
Ya Dong Gong ◽  
Wei Ding ◽  
Ting Chao Han
Keyword(s):  
Residual Stress ◽  
High Speed ◽  
Element Model ◽  
Residual Stress Distribution ◽  
X Ray Diffraction ◽  
Machined Surface ◽  
X Ray ◽  
High Speed Grinding ◽  
Simulation And Experiment ◽  
Cylindrical Workpiece

In this paper, effective finite element model have been developed to simulation the plastic deformation cutting in the process for a single particle via the software of ABAQUS, observing the residual stress distribution in the machined surface, the experiment of grinding cylindrical workpiece has been brought in the test of super-high speed grinding, researching the residual stress under the machined surface by the method of X-ray diffraction, which can explore the different stresses from different super-high speed in actual, and help to analyze the means of reducing the residual stresses in theory.

Problems Associated with Kα Doublet in Residual Stress Measurements

1979 ◽  
Vol 23 ◽  
pp. 333-339
Author(s):  
S. K. Gupta ◽  
B. D. Cullity
Keyword(s):  
Residual Stress ◽  
Silicon Powder ◽  
Lattice Parameter ◽  
Diffraction Peak ◽  
Parameter Determination ◽  
X Ray Diffraction ◽  
X Ray ◽  
Analysis Techniques ◽  
The Difference ◽  
Similar Accuracy

Since the measurement of residual stress by X-ray diffraction techniques is dependent on the difference in angle of a diffraction peak maximum when the sample is examined consecutively with its surface at two different angles to the diffracting planes, it is important that these diffraction angles be obtained precisely, preferably with an accuracy of ± 0.01 deg. 2θ. Similar accuracy is desired in precise lattice parameter determination. In such measurements, it is imperative that the diffractometer be well-aligned. It is in the context of diffractometer alignment with the aid of a silicon powder standard free of residual stress that the diffraction peak analysis techniques described here have been developed, preparatory to residual stress determinations.

Service Loading Analysis of Wind Turbine Gearbox Rolling Bearings Based on X-Ray Diffraction Residual Stress Measurements

2013 ◽  
Vol 768-769 ◽  
pp. 723-732 ◽  
Author(s):  
Jürgen Gegner ◽  
Wolfgang Nierlich
Keyword(s):  
Residual Stress ◽  
Wind Turbine ◽  
Rolling Contact Fatigue ◽  
Contact Fatigue ◽  
Rolling Contact ◽  
X Ray Diffraction ◽  
Rolling Bearings ◽  
Wind Turbine Gearbox ◽  
X Ray ◽  
Stress Measurements

Rolling bearings in wind turbine gearboxes occasionally fail prematurely by so-called white etching cracks. The appearance of the damage indicates brittle spontaneous tensile stress induced surface cracking followed by corrosion fatigue driven crack growth. An X-ray diffraction based residual stress analysis reveals vibrations in service as the root cause. The occurrence of high local friction coefficients in the rolling contact is described by a tribological model. Depth profiles of the equivalent shear and normal stresses are compared with residual stress patterns and a relevant fracture strength, respectively. White etching crack failures are reproduced on a rolling contact fatigue test rig under increased mixed friction. Causative vibration loading is evident from residual stress measurements. Cold working compressive residual stresses are an effective countermeasure.

2D X-ray diffraction and molecular modelling of the crystalline structure of polyesters under uniaxial stress

2021 ◽  
pp. 096739112199822
Author(s):  
Ahmed I Abou-Kandil ◽  
Gerhard Goldbeck
Keyword(s):  
Crystalline Structure ◽  
Molecular Modelling ◽  
Three Dimensional ◽  
Uniaxial Stress ◽  
X Ray Diffraction ◽  
X Ray ◽  
Wide Range ◽  
Modelling Techniques ◽  
Diffraction Patterns

Studying the crystalline structure of uniaxially and biaxially drawn polyesters is of great importance due to their wide range of applications. In this study, we shed some light on the behaviour of PET and PEN under uniaxial stress using experimental and molecular modelling techniques. Comparing experiment with modelling provides insights into polymer crystallisation with extended chains. Experimental x-ray diffraction patterns are reproduced by means of models of chains sliding along the c-axis leading to some loss of three-dimensional order, i.e. moving away from the condition of perfect register of the fully extended chains in triclinic crystals of both PET and PEN. This will help us understand the mechanism of polymer crystallisation under uniaxial stress and the appearance of mesophases in some cases as discussed herein.

Revision and extension of the standard laboratory technique for X-ray diffraction measurement of residual stress gradients

2007 ◽  
Vol 40 (4) ◽  
pp. 675-683 ◽  
Author(s):  
Cristy L. Azanza Ricardo ◽  
Mirco D'Incau ◽  
Paolo Scardi
Keyword(s):  
Residual Stress ◽  
Hole Drilling ◽  
Al Alloy ◽  
Diffraction Measurement ◽  
X Ray Diffraction ◽  
Surface Residual Stress ◽  
X Ray ◽  
Stress Gradients ◽  
Layer Removal ◽  
Removal Technique

A new procedure is proposed to determine sub-surface residual stress gradients by laboratory X-ray diffraction measurements at different depths using a chemical layer-removal technique. The standard correction algorithm for stress relaxation due to layer removal is improved by including corrections for X-ray absorption, and by the addition of constraints imposed by the mechanical equilibrium conditions. Besides correcting the data,i.e.providing more reliable through-thickness residual stress trends, the proposed procedure also provides an elastically compatible and plausible estimate of the residual stress inside the component, well beyond the measured region. The application of the model is illustrated for a set of Al-alloy components shot-peened at different Almen intensities. Results are compared with those given by `blind hole drilling', which is an independent and partly destructive method.

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