Microstructure, Texture and Inhibitors of the As-Cast and Hot Rolled Grain-Oriented Silicon Steel by Strip Casting

2016 ◽  
Vol 852 ◽  
pp. 101-104 ◽  
Author(s):  
Wen Qiang Liu ◽  
Cheng Shuai Lei ◽  
Han Mei Tang ◽  
Hong Yu Song ◽  
Hai Tao Liu

The microstructure and texture evolution of the as-cast and hot rolled grain-oriented silicon steel strips was investigated, and the precipitation of the inhibitors of the hot rolled strips was clarified. The results showed that the microstructure of the as-cast strip was characterized by coarse columnar grains with strong {001}<0vw> fiber texture. The microstructure of hot rolled strips was composed of ferrite and pearlite and the microstructure was gradually refined with increasing hot rolling reduction. In the hot rolled strips, α and γ fiber textures were enhanced at the expense of initial {001}<0vw> fiber texture and Goss texture was generated in the surface and sub-surface layer with increasing hot rolling reduction. Besides, a great number of dispersed MnS particles with the size of 20-30nm were observed in the hot rolled strips. These MnS particles could act as the effective inhibitors during the second recrystallization annealing of the grain-oriented silicon steel.

2011 ◽  
Vol 298 ◽  
pp. 203-208 ◽  
Author(s):  
Zi Li Jin ◽  
Wei Li ◽  
Yi Ming Li

With the help of orientation distribution function (ODF) analysis, experiments of different hot band grain microstructure 0.33% silicon steel were cold-rolled and annealed in the laboratory,to study the effect of the microstructure hot-rolled steel strip for cold rolled non-oriented silicon steel microstructure and texture of recrystallization annealing. The results show that hot rolled microstructure on cold rolled Non-Oriented Electrical Steel cold-rolled sheet evolution of texture and recrystallization have important influence, the quiaxed grain structure of steel by cold rolling and recrystallization annealing, the recrystallization speed than the fiber grain-based mixed crystals recrystallization fast , With the equiaxed grains made of cold rolled silicon steel after annealing the {110}<UVW> texture components was enhanced and {100}<uwv> texture components weakened. Different microstructure condition prior to cold rolling in the recrystallization annealing process the texture evolution has the obvious difference, the equiaxial grain steel belt cold rolling and annealing, has the strong crystal orientation. This shows that the equiaxed grain when hot microstructure is detrimental to the magnetic properties of cold-rolled non-oriented silicon steel to improve and increase.


2019 ◽  
Vol 116 (6) ◽  
pp. 604 ◽  
Author(s):  
Lifeng Fan ◽  
Liying Jia ◽  
Rong Zhu ◽  
Jianzhong He

The grain-oriented silicon steel was produced by medium temperature reheating and two-stage cold rolling process, and the microstructure and texture of all metallurgical processes were studied. The results shown that the microstructure of the hot rolled strip was inhomogeneous in thickness direction, the surface layer was the recrystallized microstructures with average grain size of 42.29 µm, the center layer was fiber structure, and the Goss texture appeared at surface. The primary recrystallized microstructure with average grain size of 16 µm was obtained after decarburization annealing, which characterized by a strong γ-fiber texture and a weak Goss texture. The average size of inhibitors in hot rolled strip and decarburization annealed sheet were 9.078 and 21.691 nm respectively, they were mainly compound of nitride and sulfide with spherical or lump shapes. The coarse Goss grains with average size 17.57 mm were got after secondary recrystallization, and the magnetic induction B8 and iron loss P1.7/50 were 1.885 T and 1.10 W/Kg, respectively.


2016 ◽  
Vol 2016 ◽  
pp. 1-6
Author(s):  
Zhi-chao Li ◽  
Ning Dang ◽  
Zhen-li Mi

OM (optical microscopy) and EBSD (electron backscatter diffraction) techniques were used to study microstructure and texture distribution during primary recrystallization under different intermediate annealing temperatures in CGO silicon steels. The effect of intermediate annealing temperature on texture distribution in 3% Si electrical steel was analyzed. The results indicate that the microstructure in primary recrystallization matrix of CGO silicon steel is comprised of equiaxed ferrite grains. Mean grain size of primary recrystallization increases with the rising of intermediate annealing temperature.γ-fiber texture is the dominant component in primary recrystallization matrix. With higher intermediate annealing temperature,111121texture and111110texture increase and111121texture is stronger than111110texture. Goss texture was observed to be decreased firstly and then increased. The content of high angle grain boundaries in primary recrystallization matrix are affected by intermediate annealing temperature. When intermediate annealing temperature is increased, high angle grain boundaries are increased firstly and then decreased. Misorientation distribution in primary recrystallized matrix is affected by primary recrystallization annealing temperature either. The content of high angle grain boundaries are increased owing to higher primary recrystallization annealing temperature, which can be a benefit to the abnormal growth of Goss grains in secondary recrystallization.


2011 ◽  
Vol 396-398 ◽  
pp. 1841-1845
Author(s):  
Yun Li Feng ◽  
Xue Jing Qi ◽  
Meng Song

The process of hot rolling Fe-3.15% Si steel is simulated by Gleeble-3500 thermal mechanical simulator, the influence of finishing temperature, coiling temperature and cooling rates after rolling on microstructure of Fe-3.15% Si steel are mainly researched, and the influence of hot rolled microstructure on Goss texture, secondary recrystallization and magnetic property are analysed. The results show that the nonuniform microstructures of hot rolled strip play an important role in developing the perfect secondary recrystallization. Fe-3.15% Si steel is rough rolled at 1110°C, finished rolled at 880°C, subsequently cooled to 550°C for coiling at rate of 10°C/s, then air cooled to room temperature. The above mentioned process could produce hot-rolled microstructure which are benefit to formation of Goss texture and the development of perfect secondary recrystallization.


2011 ◽  
Vol 702-703 ◽  
pp. 754-757 ◽  
Author(s):  
Ping Yang ◽  
Y.Y. Shao ◽  
W.M. Mao ◽  
Q.W. Jiang ◽  
W.X. Jin

The texture evolution in the surface and center layer of hot rolled electrical steel containing initial columnar grains with their <100> nearly along ND, RD and TD of sheets were determined by EBSD technique. The transition from Goss to Brass or Copper orientation in surface was analyzed. The difference in texture of center layers in these samples was compared. In particular, orientation evolutions within grains and at grain boundaries of different types of orientations were explored. The results are discussed in terms of the special alignments of grain boundaries among columnar grains.


2010 ◽  
Vol 146-147 ◽  
pp. 705-708
Author(s):  
Yong Mei Yu ◽  
Yun Bo Xu ◽  
Chang Sheng Li ◽  
Guo Dong Wang

The microstructure and textures of oriented silicon steel produced by Thin Slab Casting and Rolling (TSCR) were studied in laboratory. The fractions of equiaxed grains and columnar grains are close to 35% and 65% respectively in as-quenched ingot after being pulled out from the mould. The equiaxed grains and no texture gradient from surface to center can be observed for the 3-pass hot-rolled strips, and the inhomogeneities of microstructure and texture in thickness are relatively clear for the 7-pass samples. The subsurface texture of the hot-rolled sample contains of e (TD// <110>) fibers. The texture of the cold-rolled samples mainly consists of a (<110>//RD) and g (<111>//ND) fibers, and Goss texture ({110}<001>) disappears. The strong a fiber, weak g fiber and minor {001}<110>can be found in all layers in the cold-rolled condition.


2013 ◽  
Vol 712-715 ◽  
pp. 78-81 ◽  
Author(s):  
Chao Sun ◽  
Yu Hui Sha ◽  
Fang Zhang ◽  
Liang Zuo

Single pass hot rolling was adopted to form Goss texture at subsurface layer after hot rolling in twin-roll cast oriented silicon steel strip. It is found that the intensity of Goss texture is affected obviously by rolling reduction and finishing temperature. Goss texture originates from adjacent texture components, and rarely from {100}<uvw> component. An appropriate rolling temperature and reduced initial {100}<uvw> texture are beneficial for generating sharp hot rolling Goss texture at relatively low reduction.


2008 ◽  
Vol 584-586 ◽  
pp. 343-348 ◽  
Author(s):  
Somjeet Biswas ◽  
Satyaveer Singh Dhinwal ◽  
Ayan Bhowmik ◽  
Satyam Suwas

Commercially Pure Magnesium initially hot rolled and having a basal texture was deformed by Equal Channel Angular Extrusion (ECAE). ECAE was carried out upto 8 passes in a 90° die following routes A and Bc through a processing sequence involving two temperatures, namely 523 and 473 K. Texture and microstructure formed were studied using electron back scatter diffraction (EBSD) technique. In addition to significant reduction in grain size, strong <0002> fiber texture inclined at an angle ~ 45o from the extrusion axis formed in the material. Texture was also analyzed by orientation distribution function (ODF) and compared vis-à-vis shear texture. A significant amount of dynamic recrystallization occurred during ECAE, which apparently did not influence texture.


2020 ◽  
Vol 117 (5) ◽  
pp. 510
Author(s):  
Li-Feng Fan ◽  
Xing-Yuan Zhao ◽  
Li-Jun Xiao ◽  
Jiao Huang ◽  
Yuan Xiang Zhang

The medium temperature reheating and two-stage cold rolling process were adopted to produce industrialized Grain-oriented silicon steel. Results showed there were three sections (surface layer, transition layer and central layer) along the thickness direction on hot rolled sheets. Surface layer was occupied by complete recrystallization grains with average grain size 42.81 µm, while the central layer mainly consisted of fibrous microstructure. The Goss texture appeared only on surface layer with content 3.44%∼3.65%. After the first cold rolling with 72% reduction and decarburization annealing, the primary recrystallization occurred and average grains size reached 19.0 µm, simultaneously accompanied with texture rotated to λ, γ fiber texture and Goss texture dropped to 2.89%. Adopting the second cold rolling with 58% reduction, the cold rolled sheet consisted of deformed fiber microstructure and the texture maintained γ fiber texture with a peak at {111} <112>. The precipitates in hot rolled sheets comprised Cu2S and few AlN, and the average particle size was ∼14 nm. The inhibitors in the decarburization annealing sheet were mainly AlN, Cu2S, MnS and their composite precipitation, which were spherical or massive with the average particle size ∼21 nm. The single Goss oriented grains with average grain size 9.41 mm were obtained after high temperature annealing, and the intensity reached 873.30. The final magnetic properties were: B8 = 1.865 T and P1.7/50 = 1.124 W/kg, which met the requirement of 27Q120.


Metals ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 1380
Author(s):  
Sofia Papadopoulou ◽  
Athina Kontopoulou ◽  
Evangelos Gavalas ◽  
Spyros Papaefthymiou

During forming, thickness reduction and thermal treatment affect the recrystallization and evolution of the crystallographic texture of metallic materials. The present study focuses on the consequences of rolling reduction of a widespread aluminum alloy with numerous automotive, marine and general-purpose applications, namely Al 5182. Emphasis is laid on the crystallographic texture and mechanical properties on both hot and cold-rolled semi-final products. In particular, a 2.8 mm-thick hot-rolled product was examined in the as-received condition, while two cold-rolled sheets, one 1.33 mm and the other 0.214 mm thick, both originating from the 2.8 mm material, were examined in both as-received and annealed (350 °C for 1 h) conditions. Electron back-scatter diffraction indicated the presence of a large percentage of random texture as well as a weak recrystallization texture for the hot-rolled product, whereas in the case of cold rolling the evolution of β-fiber texture was noted. In addition, tensile tests showed that both the anisotropy as well as the mechanical properties of the cold-rolled properties improved after annealing, being comparable to hot-rolled ones.


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