Microstructure and Mechanical Properties of 6013 Aluminium Alloy Processed by a Combination of ECAP and Preaging Treatment

2016 ◽  
Vol 877 ◽  
pp. 437-443
Author(s):  
Jia Wei Jiang ◽  
Man Ping Liu ◽  
Yang Liu ◽  
Kai Tang ◽  
Zi Bo Wang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Dislocation Density ◽  
Average Length ◽  
High Strength ◽  
Tensile Tests ◽  
Tem Analysis ◽  
Average Dislocation Density ◽  
Angular Pressing ◽  
Microstructure And Mechanical Properties ◽  
Peak Aging

Microstructure and mechanical properties of a 6013 Al-Mg-Si-Cu aluminum alloy processed by a combination of equal channel angular pressing (ECAP) and preaging treatment were comparatively investigated using quantitative X-ray diffraction (XRD) measurements, transmission electron microscopy (TEM) and tensile tests. In addition, the precipitation sequences were obtained by thermodynamic calculations using the FactSage software package. Average grain sizes measured by XRD are in the range 211–501 nm while the average dislocation density is in the range 0.35-1.0 × 1014 m-2 in the deformed alloy. TEM analysis reveals that fine needle β′′ precipitates with an average length of 4-10 nm are uniformly dispersed in the preaging ECAPed alloy. The local dislocation density in this sample is as high as 2.2×1017 m-2. The strength is significantly increased in the preaging-ECAPed samples as compared to that of the undeformed counterparts. The highest yield strength among the preaging ECAPed alloys is 322 MPa. This value is about 1.25 times higher than that (258 MPa) of the static peak-aging sample. The high strength in the preaging ECAPed alloy is suggested to be related to grain size strengthening and dislocation strengthening, as well as precipitation strengthening contributed from both preaging treatment and ECAP deformation.

Microstructure and Mechanical Properties of AA5483 after Combination of ECAP and Hydrostatic Extrusion SPD Processes

2014 ◽  
Vol 59 (1) ◽  
pp. 163-166 ◽  
Author(s):  
M. Kulczyk ◽  
J. Skiba ◽  
W. Pachla
Keyword(s):  
Mechanical Properties ◽  
Salt Water ◽  
True Strain ◽  
High Strength ◽  
Tensile Tests ◽  
Hydrostatic Extrusion ◽  
Angular Pressing ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size ◽  
Marine Applications

Abstract Al-Mg alloys of the 5xxx series are strain hardenable and have moderately high strength, excellent corrosion resistance even in salt water, and very high toughness even at cryogenic temperatures to near absolute zero, which makes them attractive for a variety of applications, e.g. in systems exploited at temperatures as low as -270°C, and marine applications. The present study is concerned with the effect of a combination of 2 processes, which generate serve plastic deformation (SPD), equal channel angular pressing (ECAP) and hydrostatic extrusion (HE), on the microstructure and mechanical properties of an alloy that contain Al and Mg. The alloy was subjected to multi-pass ECAP followed by cumulative HE with a total true strain of 5.9. The microstructure of SPD samples was evaluated by transmission and scanning electron microscopy. The mechanical properties were determined by tensile tests and microhardness measurements. The combination of the two processes gave a uniform nanostructure with an average grain size of 70nm. The grain refinement taking place during the SPD processing resulted in the increase of the mechanical strength by 165% (YS) with respect to that of the material in the as- received state. The experiments have shown that the combination of HE and ECAP permits producing homogeneous nanocrystalline materials of large volumes.

scholarly journals Effect of Intercritical Annealing and Austempering on the Microstructure and Mechanical Properties of a High Silicon Manganese Steel

Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1448 ◽  
Author(s):  
Mattia Franceschi ◽  
Luca Pezzato ◽  
Claudio Gennari ◽  
Alberto Fabrizi ◽  
Marina Polyakova ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Intercritical Annealing ◽  
High Strength ◽  
Xrd Analysis ◽  
Tensile Tests ◽  
Manganese Steel ◽  
Microstructure And Mechanical Properties ◽  
Martensitic Microstructure ◽  
Steel Grades ◽  
High Silicon

High Silicon Austempered steels (AHSS) are materials of great interest due to their excellent combination of high strength, ductility, toughness, and limited costs. These steel grades are characterized by a microstructure consisting of ferrite and bainite, accompanied by a high quantity retained austenite (RA). The aim of this study is to analyze the effect of an innovative heat treatment, consisting of intercritical annealing at 780 °C and austempering at 400 °C for 30 min, on the microstructure and mechanical properties of a novel high silicon steel (0.43C-3.26Si-2.72Mn wt.%). The microstructure was characterized by optical and electron microscopy and XRD analysis. Hardness and tensile tests were performed. A multiphase ferritic-martensitic microstructure was obtained. A hardness of 426 HV and a tensile strength of 1650 MPa were measured, with an elongation of 4.5%. The results were compared with those ones obtained with annealing and Q&T treatments.

Effect of Cold Deformation on Microstructure and Mechanical Properties of Mg-8Gd-3Y-0.5Zr Alloy

2012 ◽  
Vol 706-709 ◽  
pp. 1297-1302
Author(s):  
De Jiang Li ◽  
Xiao Qin Zeng ◽  
Xin Su ◽  
Yan Cai Xie ◽  
Wen Jiang Ding
Keyword(s):  
Mechanical Properties ◽  
Cold Rolling ◽  
Cold Deformation ◽  
Tensile Tests ◽  
Age Hardening ◽  
Boundary Structure ◽  
Microstructure Observation ◽  
Microstructure And Mechanical Properties ◽  
Peak Aging ◽  
State 1

Pre-cold rolling with the reduction of 15% was employed on Mg-8Gd-3Y-0.5Zr (wt.%) (GW83K) alloy in different initial states: as-extruded (state 1) and extruded followed by annealing (state 2) with the aim to investigate the effects on microstructure and mechanical properties. Microstructure observation revealed that there are more amounts of mechanical twins in the alloy in state 2 than that of the alloy in state 1 after cold rolling, which indicates the different deformation mechanisms. Further investigation through EBSD has elucidated the grain boundary structure and types of twins in the alloys. Pre-cold deformation greatly promotes the age hardening response and the peak aging time at 200°C was found to be nearly 12h for the alloy in both state 1 and state 2, which were about 24h and 80h less than that of their non-deformed counterparts, respectively. Tensile tests at temperatures lower than 250°C showed that the alloy in state 1 has a predominant mechanical property than that of the alloy in state 2, while at 300°C, it displayed a reverse tendency.

scholarly journals Effect of ECAP on the Microstructure and Mechanical Properties of a Rolled Mg-2Y-0.6Nd-0.6Zr Magnesium Alloy

Crystals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 586 ◽  
Author(s):  
Shi ◽  
Li ◽  
Hu ◽  
Tan ◽  
Zhang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Room Temperature ◽  
High Strength ◽  
Electron Backscattered Diffraction ◽  
Bar Rolling ◽  
Fine Grained ◽  
Angular Pressing ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

A fine-grained Mg-2Y-0.6Nd-0.6Zr alloy was processed by bar-rolling and equal-channel angular pressing (ECAP). The effect of ECAP on the microstructure and mechanical properties of rolled Mg-2Y-0.6Nd-0.6Zr alloy was investigated by optical microscopy, scanning electron microscopy, electron backscattered diffraction and a room temperature tensile test. The results show that the Mg-2Y-0.6Nd-0.6Zr alloy obtained high strength and poor plasticity after rolling. As the number of ECAP passes increased, the grain size of the alloy gradually reduced and the texture of the basal plane gradually weakened. The ultimate tensile strength of the alloy first increased and then decreased, the yield strength gradually decreased, and the plasticity continuously increased. After four passes of ECAP, the average grain size decreased from 11.2 µm to 1.87 µm, and the alloy obtained excellent comprehensive mechanical properties. Its strength was slightly reduced compared to the as-rolled alloy, but the plasticity was greatly increased.

Dislocation study of ARMCO iron processed by ECAP

2016 ◽  
Vol 1818 ◽  
Author(s):  
Jairo Alberto Muñoz ◽  
Oscar Fabián Higuera ◽  
José María Cabrera
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Grain Size ◽  
Dislocation Density ◽  
Deformation Behavior ◽  
Armco Iron ◽  
Tensile Tests ◽  
Grain Sizes ◽  
Angular Pressing ◽  
Cylindrical Samples

ABSTRACTThe aim of this work was to study the deformation behavior of an Armco iron after severe plastic deformation by equal channel angular pressing (ECAP). Particular attention was paid to predict the dislocation density by different approaches like the model proposed by Bergström. Experimental measures of dislocation density by different techniques are used in the discussion. Cylindrical samples of ARMCO iron (8mm of diameter, 60mm of length) were subjected to ECAP deformation using a die with an intersecting channel of Φ=90° and outer arc of curvature of ψ= 37° die. Samples were deformed for up to 16 ECAP passes following route Bc. The mechanical properties of the material were measured after each pass by tensile tests. The original grain size of the annealed iron (70 μm) was drastically reduced after ECAP reaching grain sizes close to 300nm after 16 passes.

scholarly journals Characterization of the Role of Squeeze Casting on the Microstructure and Mechanical Properties of the T6 Heat Treated 2017A Aluminum Alloy

2019 ◽  
Vol 2019 ◽  
pp. 1-9 ◽  
Author(s):  
S. Souissi ◽  
N. Souissi ◽  
H. Barhoumi ◽  
M. ben Amar ◽  
C. Bradai ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Aluminum Alloy ◽  
Squeeze Casting ◽  
Applied Pressure ◽  
High Strength ◽  
Casting Process ◽  
Tensile Tests ◽  
Scanning Calorimetry ◽  
Microstructure And Mechanical Properties

In this study, the effects of squeeze casting process and T6 heat treatment on the microstructure and mechanical properties of 2017A aluminum alloy were investigated with scanning electron microscopy (SEM), energy dispersive X-ray spectrometry (EDS), differential scanning calorimetry (DSC), and microhardness and tensile tests. The results showed that this alloy contained α matrix, θ-Al2Cu, and other phases. Furthermore, the applied pressure and heat treatment refines the microstructure and improve the ultimate tensile strength (UTS) to 296 MPa and the microhardness to 106 HV with the pressure 90 MPa after ageing at 180°C for 6 h. With ageing temperature increasing to 320°C for 6 h, the strength of the alloy declines slightly to 27 MPa. Then, the yield strength drops quickly when temperature reaches over 320°C. The high strength of the alloy in peak-aged condition is caused by a considerable amount of θ′ precipitates. The growth of θ′ precipitates and the generation of θ phase lead to a rapid drop of the strength when temperature is over 180°C.

MILLING TIME — DEPENDENT MICROSTRUCTURE AND MECHANICAL PROPERTIES OF NANOSTRUCTURED Al–Si ALLOY

2013 ◽  
Vol 27 (11) ◽  
pp. 1350036 ◽  
Author(s):  
A. A. EBNALWALED ◽  
M. ABOU ZIED
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Dislocation Density ◽  
Milling Time ◽  
Time Dependent ◽  
Average Dislocation Density ◽  
Microstructure And Mechanical Properties ◽  
Drastic Increase ◽  
Median Diameter ◽  
Ball Milling Technique

Al –7% Si alloys were prepared by ball milling technique under different milling time. The effect of milling time on the microstructure and mechanical properties were studied. The results indicate that the grain size decrease with increasing the milling time, the average dislocation density, ρ, was found to exhibit a drastic increase by increasing the milling time, the median diameter, μ decreases, while the value of width parameter, σ is approximately constant with increasing the milling time. The value of Vickers hardness (HV) increases by increasing milling time, this increase was attributed to the refinement of grains with increasing milling time.

Microstructure and Mechanical Properties of Pure Nickel Processed by Severe Plastic Deformation

2006 ◽  
Vol 503-504 ◽  
pp. 579-584 ◽  
Author(s):  
G.V. Nurislamova ◽  
Rinat K. Islamgaliev ◽  
Ruslan Valiev
Keyword(s):  
Mechanical Properties ◽  
High Pressure Torsion ◽  
High Strength ◽  
Pure Nickel ◽  
Angular Pressing ◽  
Microstructure And Mechanical Properties ◽  
Transmission Electron ◽  
Back Scattering ◽  
Misorientation Angles ◽  
Strength And Ductility

Microstructure and mechanical properties of pure nickel processed by high pressure torsion (HPT) and equal channel angular pressing (ECAP) have been investigated in the present paper. The uniformity of microstructure and misorientation angles in the SPD samples were studied using transmission electron microscopy and electron back scattering diffraction. Microstructural requirements for achivement of high strength and ductility in SPD metals are discussed.

scholarly journals Comparative Study of Two Aging Treatments on Microstructure and Mechanical Properties of an Ultra-Fine Grained Mg-10Y-6Gd-1.5Zn-0.5Zr Alloy

Metals ◽  
2018 ◽  
Vol 8 (9) ◽  
pp. 658 ◽  
Author(s):  
Huan Liu ◽  
He Huang ◽  
Ce Wang ◽  
Jia Ju ◽  
Jiapeng Sun ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Magnesium Alloys ◽  
Aging Treatment ◽  
High Strength ◽  
Tensile Tests ◽  
Aged Alloy ◽  
Fine Grained ◽  
Peak Aging ◽  
Peak Aged ◽  
Strength And Ductility

Developing high strength and high ductility magnesium alloys is an important issue for weight-reduction applications. In this work, we explored the feasibility of manipulating nanosized precipitates on LPSO-contained (long period stacking ordered phase) ultra-fine grained (UFG) magnesium alloy to obtain simultaneously improved strength and ductility. The effect of two aging treatments on microstructures and mechanical properties of an UFG Mg-10Y-6Gd-1.5Zn-0.5Zr alloy was systematically investigated and compared by a series of microstructure characterization techniques and tensile test. The results showed that nano γ’’ precipitates were successfully introduced in T5 peak aged alloy with no obvious increase in grain size. While T6 peak aging treatment stimulated the growth of α-Mg grains to 4.3 μm (fine grained, FG), together with the precipitation of γ’’ precipitates. Tensile tests revealed that both aging treatments remarkably improved the strengths but impaired the ductility slightly. The T5 peak aged alloy exhibited the optimum mechanical properties with ultimate strength of 431 MPa and elongation of 13.5%. This work provided a novel strategy to simultaneously improve the strength and ductility of magnesium alloys by integrating the intense precipitation strengthening with ductile LPSO-contained UFG/FG microstructure.

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