Research on Microstructure Evolution in Al-9.8Zn-2.0Mg-1.8Cu Alloy during Solution Treatment

2016 ◽  
Vol 879 ◽  
pp. 2336-2341
Author(s):  
Bai Qing Xiong ◽  
Kai Wen ◽  
Yong An Zhang ◽  
Xi Wu Li ◽  
Zhi Hui Li ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Solution Treatment ◽  
Electron Back Scatter Diffraction ◽  
Solution Time ◽  
Second Phase ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Solution Treated ◽  
The Matrix

The microstructure of as-extruded Al-9.8Zn-2.0Mg-1.8Cu aluminum alloy and its evolution during solution treatment were investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), differential scanning calorimetry (DSC) analysis and electron back-scatter diffraction (EBSD). The results indicated that second phase of the as-extruded alloy mainly consisted of Mg (Zn, Cu, Al)2 and Fe-rich phases. After solution treated at 475°C for 4h, Mg (Zn, Cu, Al)2 phases were dissolved into the matrix, while Fe-rich phases still existed. Fe-rich phases cannot dissolve by prolonging solution time. The room temperature tensile strength gradually increased by prolonging solution time at 475oC. The ultimate tensile strength of the alloy reached 700MPa after both single and two-step solution treatments.

Effect of Solution Treatment on Microstructure and Mechanical Properties in an Al-9.3Zn-2.0Mg-1.8Cu Alloy

2016 ◽  
Vol 877 ◽  
pp. 606-610
Author(s):  
Kai Wen ◽  
Bai Qing Xiong ◽  
Yong An Zhang ◽  
Xi Wu Li ◽  
Zhi Hui Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Solution Treatment ◽  
Second Phase ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Residual Phase ◽  
Solution Treated ◽  
Treatment Parameter ◽  
The Matrix

The microstructure solution treated by various temperatures of 2h in as-extruded Al-9.3Zn-2.0Mg-1.8Cu alloy was investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), and differential scanning calorimetry (DSC) analysis. The mechanical properties treated at 465oC for various times were tested by room temperature tensile mechanical properties test. The results indicated that second phase of the as-extruded alloy mainly consists of Mg (Zn,Cu,Al)2 and Fe-rich phases. Mg (Zn,Cu,Al)2 phase completely dissolved into the matrix solution treated at 465oC or higher for 2h while residual phase was mainly Fe-rich phase. The mechanical properties treated at 465oC for various time were tested and optimized solution treatment parameter was chosen as 465°C/1.5h.

Effect of Solution Treatment on Second Phase Dissolution for an Al-9.2Zn-2.0Mg-1.9Cu Alloy

2020 ◽  
Vol 993 ◽  
pp. 321-326
Author(s):  
Hong Wei Liu ◽  
Kai Wen ◽  
Xi Wu Li ◽  
Zhi Hui Li ◽  
Li Zhen Yan ◽  
...  
Keyword(s):  
Electrical Conductivity ◽  
Solution Treatment ◽  
Optical Microscope ◽  
Solution Temperature ◽  
Second Phase ◽  
Dsc Analysis ◽  
Scanning Calorimetry ◽  
Phase Dissolution ◽  
Solution Treated ◽  
The Matrix

The second phase dissolution of Al-9.2Zn-2.0Mg-1.9Cu alloy conducted by various temperatures of 2h was researched with the help of optical microscope (OM), scanning electron microscope (SEM), energy dispersive spectroscopy (EDS), electrical conductivity and differential scanning calorimetry (DSC) analysis. The results gave rise to the second phase existence of Mg(Zn,Cu,Al)2 and Fe-containing phases in the as-extruded alloy. When the alloy solution treated with a temperature varied from 450°C to 470°C, a small quantity of Mg(Zn,Cu,Al)2 phase still existed in the alloy while its content exhibited a decrement trend with the solution temperature rose. For the alloy solution treated at a temperature of 475°C, Mg(Zn,Cu,Al)2 phase dissolved into the matrix completely while Fe-containing phase still remained. The electrical conductivity of quenched alloy decrease with the solution temperature increase and reached a minimum value at 470°C, and then rose slightly for the solution temperature of 475°C.

Effect of Solution Treatment on Microstructures and Hardness of Mg-Gd-Y-Zr Alloy

2014 ◽  
Vol 937 ◽  
pp. 182-186
Author(s):  
Quan An Li ◽  
Lei Lei Chen ◽  
Wen Chuang Liu ◽  
Xing Yuan Zhang ◽  
Hui Zhen Jiang
Keyword(s):  
Vickers Hardness ◽  
Cast Alloy ◽  
Solution Treatment ◽  
Hardness Measurement ◽  
Solution Temperature ◽  
X Ray Diffraction ◽  
X Ray ◽  
Solution Treated ◽  
Primary Particles ◽  
Zr Alloy

The influence of the solution treatment (at the temperature of 500-520°C for 4-12 h) on microstructures and mechanical properties of Mg-Gd-Y-Zr alloy was investigated by means of optical microscopy, scanning electron microscopy (SEM), X-ray diffraction (XRD) and Vickers hardness measurement. The as-cast alloy contains a microstructure consisting of α-Mg matrix, Mg5Gd phase and Mg24Y5phase. With increasing solution temperature and time, the quantity of the primary particles (Mg5Gd and Mg24Y5) in the alloy continually decreased, and the degree of recrystallization gradually increased, which result in the gradual decrease of the Vickers hardness of the solution-treated alloys.

Effect of Heat Treatment on the Structure and Properties of EW75 Magnesium Alloy Plate

2013 ◽  
Vol 747-748 ◽  
pp. 158-165
Author(s):  
Juan Qu ◽  
Kui Zhang ◽  
Ming Long Ma ◽  
Yong Jun Li ◽  
Xing Gang Li
Keyword(s):  
Heat Treatment ◽  
Solid Solution ◽  
Tensile Strength ◽  
Solution Process ◽  
Solution Time ◽  
Solution Temperature ◽  
Second Phase ◽  
Alloy Plate ◽  
T6 Heat Treatment ◽  
The Matrix

In this study, Mg-7Gd-5Y-1Nd-0.5Zr alloy (EW75) was produced by melting method and then press-forged into large size plate. The properties of the Mg-7Gd-5Y-1.2Nd-0.5Zr alloy were optimized through T6 heat treatment. The microstructures of alloy were observed by means of optical microscopy (OM), scanning electron microscopy (SEM). Its mechanical properties under different heat treatment conditions were determined by tensile tests. The results indicated that increasing the solid solution temperature and prolonging the solid solution time can both lead to the dissolution of second phase in the alloy back into the matrix. The solid solution temperature affects the dissolution process more than the solid solution time. Grain growth occurred during the solid solution process. The grain size of the matrix enlarges with the increase of solid solution temperature. The tensile test result showed that the tensile strength of the alloy was significantly improved after T6 heat treatment. Its tensile strength in the same direction was nearly 40% up after T6 heat treatment. The analysis shows that T6 heat treatment can effectively eliminate the larger deformed precipitates and beneficial to the formation of hard precipitates, which leads to an improvement in the alloys tensile strength.

Structure and properties of poly(3-hydroxybutyrate-co-3-hydroxyhexanoate)/poly(L-lactic acid) quasi core/sheath melt-electrospun microfibers

2018 ◽  
Vol 89 (9) ◽  
pp. 1770-1781 ◽  
Author(s):  
Huaizhong Xu ◽  
Benedict Bauer ◽  
Masaki Yamamoto ◽  
Hideki Yamane
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Lactic Acid ◽  
Tensile Tests ◽  
Processing Parameters ◽  
Structure And Properties ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Diffraction Patterns

A facile route was proposed to fabricate core–sheath microfibers, and the relationships among processing parameters, crystalline structures and the mechanical properties were investigated. The compression molded poly(3-hydroxybutyrate-co-3-hydroxyhexanoate) (PHBH)/poly(L-lactic acid) (PLLA) strip enhanced the spinnability of PHBH and the mechanical properties of PLLA as well. The core–sheath ratio of the fibers was determined by the prefab strip, while the PLLA sheath component did not completely cover the PHBH core component due to the weak interfacial tension between the melts of PHBH and PLLA. A rotational target was applied to collect aligned fibers, which were further drawn in a water bath. The tensile strength and the modulus of as-spun and drawn fibers increased with increasing the take-up velocities. When the take-up velocity was above 500 m/min, the jet became unstable and started to break up at the tip of the Taylor cone, decreasing the mechanical properties of the fibers. The drawing process facilitated the crystallization of PLLA and PHBH, and the tensile strength and the modulus increased linearly with the increasing the draw ratio. The crystal information displayed from wide-angle X-ray diffraction patterns and differential scanning calorimetry heating curves supported the results of the tensile tests.

Erucamide-Nanoclay Systems Obtained by Intercalation Process

2017 ◽  
Vol 899 ◽  
pp. 36-41 ◽  
Author(s):  
Josiane R. Silvano ◽  
J.M.M. Mello ◽  
Lucinao Luiz Silva ◽  
Humberto Gracher Riella ◽  
Márcio Antônio Fiori
Keyword(s):  
Differential Scanning Calorimetry ◽  
Reaction Medium ◽  
Film Surface ◽  
Polymeric Materials ◽  
Polymeric Films ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Intercalation Process ◽  
The Matrix

A major challenge in the manufacture of films for polymeric packaging is the definition and setting of the friction coefficient (FCO) for the film surfaces. The FCO values are established with the incorporation of additives during the processing of the polymeric films. But, the homogenization of these additives in the polymeric matrix is very difficult. The additives have different polarity that the matrix polymeric and not are mixable. So, these additives migrate for the surface of the polymeric films easily. Several molecules are used as sliding additives, but among the most efficient are the amides molecules, highlighting the erucamide. This molecule promotes the decrease of the FOC but due its quick migration for the polymeric film surface provides numerous problems for the manufacture of the polymeric packaging and during its application as the product. In this work a nanocomposite (MMT-ERU) was obtained by an intercalation process to improve the compatibility between the polymeric materials and the erucamide molecules. The results shown in this work refers to the studies about the intercalation processes of the erucamide molecules into nanoclays (montmorillonite) to obtain the nanocomposite MMT-ERU. The effect of the temperature and the percentage of the nanoclay in the intercalation processes were studied. The results of x-ray diffraction and differential scanning calorimetry shown that erucamide molecules were intercalated in the nanoclay structures and that intercalation efficiency depends positively of the temperature and percentage amount of the nanoclay in the reaction medium.

scholarly journals Impact of heating temperatures on the properties of instant cassava flour

2021 ◽  
Vol 39 (No. 5) ◽  
pp. 360-367
Author(s):  
Achmat Sarifudin ◽  
Enny Sholichah ◽  
Woro Setiaboma ◽  
Nok Afifah ◽  
Dewi Desnilasari ◽  
...  
Keyword(s):  
Heating Temperature ◽  
Ethanol Solution ◽  
Starch Granules ◽  
Dsc Analysis ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Cassava Flour ◽  
X Ray ◽  
The Matrix ◽  
The Impact

Native cassava flour can be modified to be instant flour by heating the cassava flour in ethanol solution. The impact of heating temperatures of 60, 80, and 100 °C (coded as ICF-60, ICF-80, and ICF-100) on the properties of instant cassava flour (ICF), including colour, morphological, and thermal properties, water absorption, and solubility indexes and pasting behaviour, were investigated. Results showed that ICF produced at higher temperatures exhibited lower lightness, higher redness, and yellowness values. ICF-60 and ICF-80 still displayed the granular forms and birefringence properties of native starches, while granules of ICF-100 were broken and partially lost their birefringence properties. Results of X-ray diffraction (XRD) technique and differential scanning calorimetry (DSC) analysis suggested that the amylopectin double helixes of crystalline regions within the structure of ICF orientated to more perfect conformation before they were disrupted at the highest heating temperature (100 °C). During hydration, the starch granules of ICF-60 and ICF-80 absorbed water into their granules; meanwhile, ICF-100 entrapped water within the matrix formed by the entanglements of ICF-100 particles. Results of pasting behaviour analysis indicated that ICF-60 and ICF-80 showed better thermal stability while ICF-100 exhibited the highest cold viscosity.

Microstructure and Tensile Properties of Mg-4Zn-2Sn-2Al Alloy

2013 ◽  
Vol 747-748 ◽  
pp. 398-403 ◽  
Author(s):  
Dong Qing Zhao ◽  
Xu Guang Dong ◽  
Xin En Zhang ◽  
An Jiang Gao ◽  
Ji Xue Zhou ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Ultimate Tensile Strength ◽  
Tensile Properties ◽  
Aging Process ◽  
Supersaturated Solid Solution ◽  
Cast Alloy ◽  
Solution Treatment ◽  
Solution Treated ◽  
The Matrix ◽  
Alloy Increase

The microstructures and tensile properties of as-cast, solution-treated and aged Mg-4Zn-2Sn-2Al (wt.%) alloy have been investigated. The microstructure of the as-cast alloy consists of α-Mg, Mg2Sn and Mg32(Al,Zn)49 phases. The yield tensile strength and the ultimate tensile strength of the as-cast alloy are 87.7 MPa and 241.3 MPa, respectively, and the elongation reaches to 18.8% showing excellent ductility. After solution treatment, all of the Mg32(Al,Zn)49 phase and the majority of Mg2Sn particles have dissolved into the matrix. During aging process, Mg2Sn phase precipitates from the α-Mg supersaturated solid solution. With the precipitation strengthening of Mg2Sn phase, the yield tensile strength and the ultimate tensile strength of the alloy increase to 112.5 MPa and 280.4 MPa, respectively, while, the elongation decreases to 12%.

Effect of Solution Treatment Temperature on the Microstructure of Fe-33Ni-19Cr Alloy

2020 ◽  
Vol 1010 ◽  
pp. 21-27
Author(s):  
Noraziana Parimin ◽  
Esah Hamzah
Keyword(s):  
Grain Size ◽  
Solution Treatment ◽  
Optical Microscope ◽  
Treatment Temperature ◽  
Solution Treatment Temperature ◽  
X Ray Diffraction ◽  
X Ray ◽  
Solution Treated ◽  
Average Grain Size ◽  
Different Temperatures

The effect of solution treatment temperature on the microstructure, phase present and hardness on Fe-33Ni-19Cr alloy was study in this work. The Fe-33Ni-19Cr alloy was experienced a solution treatment process at six different temperatures which are 950 °C, 1000 °C, 1050 °C, 1100 °C, 1150 °C and 1200 °C for 3 hours soaking time followed by water quench. The average grain size was measured by using linear intercept methods ASTM E112. Microstructure of solution-treated Fe-33Ni-19Cr alloy was characterized by using optical microscope and scanning electron microscope (SEM) equipped with energy dispersive x-ray (EDX) spectrometer. The phase present was analyzed using x-ray diffraction (XRD) technique. The Vickers hardness was used to measure the hardness of solution-treated Fe-33Ni-19Cr alloy. Increasing the solution treatment temperatures were increase the average grain size of solution-treated Fe-33Ni-19Cr alloy. In addition, all samples exhibited an equiaxed matrix grain with slight distribution of precipitates particles. The hardness of solution-treated Fe-33Ni-19Cr alloy was decrease as the solution treatment temperature increase.

scholarly journals The Effect of Incorporating Silica Stone Waste on the Mechanical Properties of Sustainable Concretes

Materials ◽  
2020 ◽  
Vol 13 (17) ◽  
pp. 3832 ◽  
Author(s):  
Saeid Abbasi ◽  
Mohammad Hemen Jannaty ◽  
Rabar H. Faraj ◽  
Shahriar Shahbazpanahi ◽  
Amir Mosavi
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Sustainable Construction ◽  
X Ray Diffraction ◽  
Spectroscopy Analysis ◽  
Sem Images ◽  
X Ray ◽  
Fourier Transformed Infrared Spectroscopy ◽  
The Matrix ◽  
First Time

Incorporating various industrial waste materials into concrete has recently gained attention for sustainable construction. This paper, for the first time, studies the effects of silica stone waste (SSW) powder on concrete. The cement of concrete was replaced with 5, 10, 15, and 20% of the SSW powder. The mechanical properties of concrete, such as compressive and tensile strength, were studied. Furthermore, the microstructure of concrete was studied by scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy analysis (EDX), Fourier transformed infrared spectroscopy (FTIR), and X-Ray diffraction (XRD) tests. Compressive and tensile strength of samples with 5% SSW powder was improved up to 18.8% and 10.46%, respectively. As can be observed in the SEM images, a reduced number of pores and higher density in the matrix can explain the better compressive strength of samples with 5% SSW powder.

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