scholarly journals Effect of an Ionic Liquid on the Flexural and Fracture Mechanical Properties of EP/MWCNT Nanocomposites

2017 ◽  
Vol 885 ◽  
pp. 19-24 ◽  
Author(s):  
Gábor Szebényi ◽  
Levente Ferenc Tóth ◽  
József Karger-Kocsis
Keyword(s):  
Ionic Liquid ◽  
Interfacial Adhesion ◽  
Bending Strength ◽  
Mechanical Tests ◽  
Critical Force ◽  
Electron Microscopic ◽  
Adhesion Promoter ◽  
Multiwalled Carbon ◽  
Three Point Bending ◽  
Bending Modulus

The improvement of interfacial adhesion between multiwalled carbon nanotubes (MWCNTs) and epoxy resin (EP) was investigated in nanocomposites with the addition of an ionic liquid (IL, 1-Ethyl-3-methyl imidazolium tetrafluoroborate - EMIM BF4) as interfacial adhesion promoter. MWCNT (0, 0.3 and 0.5 weight%) was dispersed in EP through diluting an MWCNT-rich masterbatch prepared in presence and absence of IL. Three point bending and compact tension (CT) fracture mechanical tests were performed on specimens with different MWCNT contents with and without IL surfactant. IL addition resulted in easier dispersion of MWCNT in the EP masterbatch. With the addition of the IL the three point bending strength, the bending modulus of elasticity and the critical force required for crack propagation have increased significantly at the optimal, 0.3 weight% MWCNT content. Scanning electron microscopic (SEM) investigation of the fracture surfaces of the CT specimens revealed that incorporation of MWCNTs and its IL-assisted dispersion produced rougher surfaces suggesting higher fracture toughness than the reference EP.

Bending Properties and Failure Mechanisms of Tapered 3D Braided Composites

2011 ◽  
Vol 332-334 ◽  
pp. 1468-1471 ◽  
Author(s):  
Can Can Cheng ◽  
Zhao Lin Liu ◽  
Li Fang Liu ◽  
Jian Yong Yu
Keyword(s):  
Failure Modes ◽  
Bending Strength ◽  
Failure Mechanisms ◽  
Reduction Technique ◽  
Braided Composites ◽  
Bending Properties ◽  
Bending Tests ◽  
Three Point Bending ◽  
Bending Modulus ◽  
3D Braided Composites

Tapered 3D braided composites are prepared by column yarn-reduction technique, unit yarn-reduction technique and cutting, respectively. Bending properties in the tapered regions of the composites are obtained by three-point bending tests, and SEM photographs of the fracture surfaces are observed to analyze the failure mechanisms. Results show that bending modulus and bending strength of the yarn-reduction composites are significantly higher than those of the cut composites, and the unit yarn-reduction composites are slightly stronger than the column yarn-reduction composites. The saw-tooth propagation of matrix crackings and interfacial debondings are the primary failure mechanisms of the yarn-reduction composites, while yarn breakages and yarn pulling-outs are the main failure modes of the cut composites.

Preparation and Characterization of Polyurethane/Multiwalled Carbon Nanotube Composites

2008 ◽  
Vol 16 (8) ◽  
pp. 501-507 ◽  
Author(s):  
Shuzhong Guo ◽  
Chao Zhang ◽  
Weizhi Wang ◽  
Tianxi Liu ◽  
Wuiwui Chauhari Tjiu ◽  
...  
Keyword(s):  
Carbon Nanotube ◽  
Interfacial Adhesion ◽  
In Situ Polymerization ◽  
Stress Transfer ◽  
Mechanical Analysis ◽  
Mechanical Tests ◽  
Multiwalled Carbon Nanotube ◽  
Multiwalled Carbon ◽  
The Matrix ◽  
Nanotube Composites

Multiwalled carbon nanotube (MWNT)/polyurethane (PU) nanocomposites have been prepared by the combination of in-situ polymerization and solution-casting approach. A homogeneous dispersion of MWNTs throughout PU matrix is observed by scanning electron microscopy on the fracture surfaces of the composites. Strong interfacial adhesion between the MWNTs and the PU matrix, as evidenced by the presence of broken but strongly embedded MWNTs in the matrix, is favorable to stress transfer from polymer matrix to the nanotubes. Mechanical tests (by tensile testing and dynamic mechanical analysis) show that, compared with neat PU, both the Young's modulus and the tensile strength of the composites are significantly improved by about 90%, with incorporating only 1 wt.% MWNTs. And most importantly, the elongation-at-break of PU/carbon nanotube (CNT) composites is greatly improved by about 500%, indicating that the toughness of neat PU is remarkably enhanced by adding CNTs into the matrix. The fine dispersion of CNTs and strong interfacial adhesion between the CNTs with the matrix are responsible for the simultaneous and significant enhancement in the strengthening and toughening of PU matrix. In addition, the thermal stability of PU was also improved after incorporating CNTs into the matrix.

The Mechanical Properties of Organic Modified Epoxy Resin

2020 ◽  
Vol 43 (3) ◽  
pp. 10-14
Author(s):  
Georgel MIHU ◽  
Claudia Veronica UNGUREANU ◽  
Vasile BRIA ◽  
Marina BUNEA ◽  
Rodica CHIHAI PEȚU ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Composite Materials ◽  
Epoxy Resin ◽  
Epoxy Matrix ◽  
Epoxy Resins ◽  
Mechanical Tests ◽  
Organic Modification ◽  
Three Point Bending ◽  
Modified Epoxy

Epoxy resins have been presenting a lot of scientific and technical interests and organic modified epoxy resins have recently receiving a great deal of attention. For obtaining the composite materials with good mechanical proprieties, a large variety of organic modification agents were used. For this study gluten and gelatin had been used as modifying agents thinking that their dispersion inside the polymer could increase the polymer biocompatibility. Equal amounts of the proteins were milled together and the obtained compound was used to form 1 to 5% weight ratios organic agents modified epoxy materials. To highlight the effect of these proteins in epoxy matrix mechanical tests as three-point bending and compression were performed.

Mechanical and thermal characterization of grafted PP-NCC nanocomposites

2019 ◽  
pp. 089270571987822
Author(s):  
Saud Aldajah ◽  
Mohammad Y Al-Haik ◽  
Waseem Siddique ◽  
Mohammad M Kabir ◽  
Yousef Haik
Keyword(s):  
Thermal Properties ◽  
Interfacial Adhesion ◽  
Thermal Characterization ◽  
Mechanical And Thermal Properties ◽  
Screw Extruder ◽  
Scanning Calorimetry ◽  
Three Point Bending ◽  
Twin Screw ◽  
Thermal Stability Of

This study reveals the enhancement of mechanical and thermal properties of maleic anhydride-grafted polypropylene (PP- g-MA) with the addition of nanocrystalline cellulose (NCC). A nanocomposite was manufactured by blending various percentages of PP, MA, and NCC nanoparticles by means of a twin-screw extruder. The influence of varying the percentages of NCC on the mechanical and thermal behavior of the nanocomposite was studied by performing three-point bending, nanoindentation, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), and Fourier-transform infrared (FTIR) spectroscopy tests. The novelty of this study stems on the NCC nanoparticles and their ability to enhance the mechanical and thermal properties of PP. Three-point bending and nanoindentation tests revealed improvement in the mechanical properties in terms of strength, modulus, and hardness of the PP- g-MA nanocomposites as the addition of NCC increased. SEM showed homogeneity between the mixtures which proved the presence of interfacial adhesion between the PP- g-MA incorporated with NCC nanoparticles that was confirmed by the FTIR results. DSC and TGA measurements showed that the thermal stability of the nanocomposites was not compromised due to the addition of the coupling agent and reinforced nanoparticles.

Effects of hostile solutions on the static and dynamic behavior of carbon/epoxy composites

2021 ◽  
pp. 002199832110200
Author(s):  
H Ersen Balcıoğlu ◽  
Raif Sakin ◽  
Halit Gün
Keyword(s):  
Bending Strength ◽  
Laminated Composites ◽  
Fatigue Behavior ◽  
Laminated Composite ◽  
Test Sample ◽  
Solution Concentration ◽  
Static Stability ◽  
Three Point Bending ◽  
Sem Image ◽  
Solution Type

Fiber-reinforced laminated composite is often used in harsh environments that may affect their static stability and long-term durability as well as residual strength. In this study, the effect of heavy chemical environments such as acid and alkaline and retaining time for these environments on flexural strength and flexural fatigue behavior of carbon/epoxy laminated composites were investigated. In this context, carbon/epoxy was retained into an acidic and alkaline solution having 5%, 15%, and 25% concentration by weight for 1–4 months. Fatigue behavior of carbon/epoxy was determined under dynamic flexural load, which corresponds to 80%, 70%, 60%, 50%, and 40% of static three-point bending strength of the test sample. SEM image of damaged specimens was taken to describe the failure mechanism of damage which occurs after fatigue. Also, to better understand environmental condition on the fatigue life, results were compared with results of carbon/epoxy laminated composites, which were not retained into any environments (unretained). The test results showed that the solution type, solution concentration, and retaining time caused noticeable changes in the static and dynamic strengths of carbon/epoxy laminated composites.

scholarly journals Chlorine-Functional Silsesquioxanes (POSS-Cl) as Effective Flame Retardants and Reinforcing Additives for Rigid Polyurethane Foams

Molecules ◽  
2021 ◽  
Vol 26 (13) ◽  
pp. 3979
Author(s):  
Anna Strąkowska ◽  
Sylwia Członka ◽  
Karolina Miedzińska ◽  
Krzysztof Strzelec
Keyword(s):  
Flame Retardants ◽  
Elevated Temperatures ◽  
Bending Strength ◽  
Reaction System ◽  
Fire Retardant ◽  
Polyurethane Foams ◽  
Polymerization Reaction ◽  
Three Point Bending ◽  
One Step

The subject of the research was the production of silsesquioxane modified rigid polyurethane (PUR) foams (POSS-Cl) with chlorine functional groups (chlorobenzyl, chloropropyl, chlorobenzylethyl) characterized by reduced flammability. The foams were prepared in a one-step additive polymerization reaction of isocyanates with polyols, and the POSS modifier was added to the reaction system in an amount of 2 wt.% polyol. The influence of POSS was analyzed by performing a series of tests, such as determination of the kinetics of foam growth, determination of apparent density, and structure analysis. Compressive strength, three-point bending strength, hardness, and shape stability at reduced and elevated temperatures were tested, and the hydrophobicity of the surface was determined. The most important measurement was the determination of the thermal stability (TGA) and the flammability of the modified systems using a cone calorimeter. The obtained results, after comparing with the results for unmodified foam, showed a large influence of POSS modifiers on the functional properties, especially thermal and fire-retardant, of the obtained PUR-POSS-Cl systems.

scholarly journals Properties of AlSi9Cu3 metal matrix micro and nano composites produced via stir casting

2018 ◽  
Vol 16 (1) ◽  
pp. 726-731 ◽  
Author(s):  
Tennur Gülşen Ünal ◽  
Ege Anıl Diler
Keyword(s):  
Mechanical Properties ◽  
Metal Matrix ◽  
Weight Fraction ◽  
Stir Casting ◽  
Mechanical Tests ◽  
Matrix Composites ◽  
Casting Method ◽  
Porosity Formation ◽  
Three Point Bending ◽  
Hardness Values

AbstractThe effects of micro and nano sized reinforcement particles on microstructure and mechanical properties of aluminium alloy-based metal matrix composites were investigated in this study. AlSi9Cu3 alloy was reinforced with micro and nano sized ceramic reinforcement particles at different weight fractions by using a stir casting method. The mechanical tests (hardness, three point bending) were performed to determine the mechanical properties of AlSi9Cu3 alloy-based microcomposites (AMMCs) and nanocomposites (AMMNCs). The experimental results have shown that the size and weight fraction of reinforcement particles have a strong influence on the microstructure and the mechanical properties of AlSi9Cu3 alloy-based microcomposites and nanocomposites. The relative densities of all AMMC and AMMNC samples are lower than unreinforced AlSi9Cu3 alloy due to porosity formation with the increase of weight fraction of reinforcement particles. As weight fraction increases, hardness values of AMMCs and AMMNCs increase. Maximum flexural strength can be obtained at 3.5wt.% for the AMMC sample with microsized Al2O3 particles and at 2wt.% for the AMMNC sample with nano-sized Al2O3 particles. After the weight fractions exceed these values, flexural strengths of both AMMCs and AMMNCs decrease due to clustering of Al2O3 particles.

scholarly journals Knitted Meshes for Reinforcing Building Composites

2019 ◽  
Vol 27 (4(136)) ◽  
pp. 102-111
Author(s):  
Zbigniew Mikołajczyk ◽  
Katarzyna Pieklak ◽  
Aleksandra Roszak
Keyword(s):  
Concrete Beam ◽  
Bending Strength ◽  
Relative Elongation ◽  
Testing Machine ◽  
Strength Analysis ◽  
Knitted Fabrics ◽  
Three Point Bending ◽  
Concrete Mass ◽  
Frp Composites ◽  
Technical Textiles

Modern technical textiles, including knitted fabrics, are widely used in the construction industry. Regarding textiles in concrete reinforcement, methods based on shredded fibres, meshes, reinforcing mats, woven textiles and knitted DOStapes are frequently used as underlays of concrete constructions. Textiles are also used in the reinforcement of fibrous FRP composites. The research presented focused on producing composites made of MapeiMapefill concrete mass with reinforcement in the form of three variants of knitted meshes made of 228 tex polyamide threads, polypropylene threads of 6.3 tex and 203 tex glass threads, as well as identification of their mechanical properties. The mesh variant made of glass fibre is especially noteworthy, as its strength is more than three times higher than that of polyamide meshes. At the same time, a very small relative elongation of 3% is observed for this variant of knitted fabric, which is a desired property regarding the comparatively low stretching extension of concrete. In the process of making the composites, the adhesion of the concrete mass to the surface of the threads was analyzed. For this purpose, a "Sopro HE449" type agent was used. Composite beams were subjected to a three-point bending strength analysis on a testing machine. The results of strength measurements of the composites obtained prove that those with glass fibres demonstrate a threefold increase in strength compared to the original concrete beam.

scholarly journals Effect of Gamma Radiation on the Mechanical Properties of Natural Fabric Reinforced Polyester Composites

2019 ◽  
Vol 27 (4(136)) ◽  
pp. 88-93
Author(s):  
K.Z.M. Abdul Motaleb ◽  
Md Shariful Islam ◽  
Rimvydas Milašius
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Impact Strength ◽  
Gamma Radiation ◽  
Bending Strength ◽  
Polyester Resin ◽  
Radiation Doses ◽  
Elongation At Break ◽  
Bending Modulus ◽  
Polyester Composites

Two types of composites:(1) pineapple fabric reinforced polyester resin (Pineapple/PR) and (2) jute fabric reinforced polyester resin (Jute/PR) were prepared and the mechanical properties investigated for various gamma radiation doses ranging from 100-500 krad. Properties like tensile strength, Young’s modulus, elongation-at-break, bending strength, bending modulus and impact strength were increased significantly by 19%, 32%, 45%, 32%, 47% and 20%, respectively, at a dose of 300 krad for Pineapple/PR, and by 47%, 49%, 42%, 45%, 52% and 65%, respectively, at a dose of 200 krad for the Jute/PR composite in comparison to the non-irradiated composite. Gamma radiation improved the mechanical properties, but overdoses of radiation even caused a reduction in them.

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