Study on Thermal Conductivity of Polyetheretherketone/Thermally Conductive Filler Composites

2007 ◽  
Vol 124-126 ◽  
pp. 1079-1082 ◽  
Author(s):  
Sung Ryong Kim ◽  
Dae Hoon Kim ◽  
Dong Ju Kim ◽  
Min Hyung Kim ◽  
Joung Man Park
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Carbon Fiber ◽  
Conductive Filler ◽  
Laser Flash ◽  
Flash Method ◽  
Phase System ◽  
Two Phase ◽  
Nielsen Theory ◽  
Thermally Conductive

Thermal properties of PEEK/silicon carbide(SiC) and PEEK/carbon fiber(CF) were investigated from ambient temperature up to 200°C measured by laser flash method. Thermal conductivity was increased from 0.29W/m-K without filler up to 2.4 W/m-K with at 50 volume % SiC and 3.1W/m-K with 40 volume % carbon fiber. Values from Nielsen theory that predicts thermal conductivity of two-phase system were compared to those obtained from experiment.

Synergistic Effect of Hybrid Filler Contained Composites on Thermal Conductivity

2007 ◽  
Vol 544-545 ◽  
pp. 483-486 ◽  
Author(s):  
Dae Hoon Kim ◽  
Min Hyung Kim ◽  
Ji Hoon Lee ◽  
J. H. Lim ◽  
K.M. Kim ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Thermal Diffusivity ◽  
Carbon Fiber ◽  
Synergistic Effect ◽  
Laser Flash ◽  
Flash Method ◽  
Phase System ◽  
Two Phase ◽  
Hybrid Filler ◽  
Hybrid Fillers

Thermal conductivity of polyetheretherketone (PEEK) with fillers was investigated. By adding the hybrid fillers to polymer the thermal conductivity of composites was increased significantly. Thermal diffusivity of composites was measured using laser flash method. Synergistic filler effect between particulate SiC and carbon fiber (CF) was observed for thermal conductivity. In a PEEK based composite, thermal conductivity increased to 8.25 W/m-K for a 50 vol% hybrid filler (SiC+CF) system, whereas the thermal conductivity of 40 vol% CF was 3.1 W/m-K and 50 vol% of SiC was 2.4 W/m-K, respectively. The use of hybrid filler was found to be effective in increasing thermal conductivity of its composites due to formation of effective thermal conductive path. Experimental results of two-phase system were compared with Nielsen prediction.

Laser Flash Measurement of Samples With a Transparent Reference Layer

2009 ◽  
Author(s):  
Heng Ban ◽  
Zilong Hua
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Temperature Response ◽  
Front Surface ◽  
Laser Flash ◽  
Laser Flash Method ◽  
Flash Method ◽  
Thermal Diffusivity Measurement ◽  
Reference Layer

The laser flash method is a standard method for thermal diffusivity measurement. This paper reports the development of a method and theory that extends the standard laser flash method to measure thermal conductivity and thermal diffusivity simultaneously. By attaching a transparent reference layer with known thermal properties on the back of a sample, the thermal conductivity and thermal diffusivity of the sample can be extracted from the temperature response of the interface between the sample and the reference layer to a heating pulse on the front surface. The theory can be applied for sample and reference layer with different thermal properties and thickness, and the original analysis of the laser flash method becomes a limiting case of the current theory with an infinitely small thickness of the reference layer. The uncertainty analysis was performed and results indicated that the laser flash method can be used to extract the thermal conductivity and diffusivity of the sample. The results can be applied to, for instance, opaque liquid in a quartz dish with silicon infrared detector measuring the temperature of liquid-quartz interface through the quartz.

Thermal Property Measurements of Carbon Nanotube Forest Synthesized by Thermal CVD Process

2009 ◽  
Author(s):  
Qingjun Cai ◽  
Bing-chung Chen ◽  
Yuan Zhao ◽  
Julia Mack ◽  
Yanbao Ma ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Carbon Nanotube ◽  
Quartz Substrate ◽  
Laser Flash ◽  
Volume Density ◽  
Thickness Measurement ◽  
Flash Method ◽  
Thermal Cvd ◽  
3 Omega

Carbon nanotube (CNT) forest/cluster synthesized by a thermal CVD process has millimeter growth height, large porosity and nano level pore size, plus high thermal conductivity of individual CNT, thus it is potentially a good wick structure material in developing micro heat transfer devices. However, thermal properties, including effective thermal conductivity (ETC) of a bulky CNT layer, may not be as good as the common metallic wick materials. In this paper, a Netzsch DSC 404 C Pegasus is used for measurement of the CNT heat capacity. CNT volume density is obtained by measuring the ratio of a bulky CNT weight and volume. Both the laser flash and 3-omega measurement methods are employed to measure ETC for CNT wick structures synthesized by the thermal CVD processes. For the laser flash method, measurement deviations caused by reflective silicon and thin substrate are corrected by surface treatment and increased sample thickness. Measurement results of the laser flash indicate that a 600μm thick CNT layer has ETC varying from 0.7–1.2W/m.K. For the 3-omega approach, the measurement system is validated on a quartz substrate. However, the test results yield larger ETC on 250μm CNT samples. Geometric and one dimensional thermal conduction analysis indicate that the bulky CNT thermal properties are tied to CNT synthesis processes. ETC of bulky CNT layer can be enhanced by straightening CNT growth and increasing CNT growth volume density.

Thermal Characterization of IM7/8552-1 Carbon-Epoxy Composites

2014 ◽  
Author(s):  
Messiha T. Saad ◽  
Sandi G. Miller ◽  
Torrence Marunda
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Carbon Fiber ◽  
Specific Heat ◽  
High Performance ◽  
Critical Role ◽  
Flash Method ◽  
Handling Characteristics ◽  
Wide Range

Thermal properties of composite materials such as, thermal conductivity, diffusivity, and specific heat are very important in engineering design process and analysis of aerospace vehicles as well as space systems. These properties are also important in power generation, transportation, and energy storage devices including fuel cells. Thermal conductivity is the property that determines the working temperature levels of the material; it plays a critical role in the performance of materials in high temperature applications, and it is an important parameter in problems involving heat transfer and thermal structures. The objective of this paper is to develop a thermal properties data base for the carbon fiber-epoxy (IM7/8552-1) composite. The IM7 carbon fiber is a continuous, high performance, intermediate modulus, PAN based fiber. This fiber has been surface treated and can be sized to improve its interlaminar shear properties, handling characteristics, and structural properties. The 8552 is a high performance tough epoxy matrix for use in primary aerospace structures. It exhibits good impact resistance and damage tolerance for a wide range of applications. The IM7/8552-1 is an amine cured unidirectional prepreg. The manufacturer recommended cure cycle for this material was followed, which includes consolidation under vacuum and autoclave pressure. The composite has a service temperature up to 121°C (250°F). The thermal properties of IM7/8552-1 carbon-epoxy have been investigated using experimental methods. The flash method was used to measure the thermal diffusivity of the composite. This method is based on the American Society for Testing and Materials standard, ASTM E1461. In addition, the Differential Scanning Calorimeter was used in accordance with the ASTM E1269 standard to measure the specific heat. The measured thermal diffusivity, specific heat, and density data were used to compute the thermal conductivity of the IM7/8552-1 carbon-epoxy composite.

scholarly journals Исследование влияния технологических факторов на неопределенность результатов измерения теплопроводности методом лазерной вспышки

2022 ◽  
Vol 56 (2) ◽  
pp. 173
Author(s):  
Е.С. Макарова ◽  
А.В. Асач ◽  
И.Л. Тхоржевский ◽  
В.Е. Фомин ◽  
А.В. Новотельнова ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Sharp Increase ◽  
Laser Flash ◽  
Comsol Multiphysics ◽  
Flash Method ◽  
Software Environment ◽  
Conductive Materials ◽  
Measurement Results ◽  
Thermally Conductive ◽  
Graphite Coating

The estimation of the deviation in the measurements of thermal conductivity by the laser flash method for materials with different thermal conductivity coefficients, arising due to the presence of a graphite coating on the sample and the small thickness of the sample, is carried out. A computer model of the method was created in the Comsol Multiphysics software environment. For bulk samples with a graphite coating thickness of 20 μm, the deviation is 5.5 %. The thickness of bulk samples does not affect the measurement results. For materials with low thermal conductivity, a sharp increase in the deviation is observed, reaching 60%. For thermally conductive materials, the deviation is 16-18%. For thin samples less than 10 μm thick, the thickness of the graphite coating does not affect the measurement results. The decisive factor is the duration of the laser pulse.

Thermal Properties and Fracture Behavior of Compositionally Graded Al-SiCp Composites

2004 ◽  
Vol 449-452 ◽  
pp. 621-624 ◽  
Author(s):  
Kyung Mok Cho ◽  
Il Dong Choi ◽  
Ik Min Park
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Shock ◽  
Volume Fraction ◽  
Laser Flash ◽  
Fatigue Tests ◽  
Functionally Graded ◽  
Flash Method ◽  
Compositional Gradient ◽  
Infiltration Process

Compositionally graded Al-SiCp composites were fabricated using pressureless infiltration process. Microstructure was examined and thermal properties were characterized for Al-SiCp composites. Al-SiCp composites with fairly uniform distribution and compositional gradient of SiC reinforcement in the Al matrix though the thickness direction was successfully fabricated. The thermal conductivity of Al-SiCp composites was measured at room temperature, 200°C and 400°C using laser flash method. Thermal conductivity of Al-SiCp composites increases non-linearly with decreasing the volume fraction of SiC. Cyclic thermal shock fatigue tests were performed by immersing Al-SiCp functionally graded materials(FGM) into water from the various heating temperatures of 400°C , 300°C and 200°C , repeatedly. After cyclic thermal shock fatigue tests, micro-hardness was measured and formation of cracks was investigated.e fati

Highly thermally conductive UHMWPE/NG composites with the segregated structure and their application for heat spreader

2020 ◽  
pp. 089270572096564
Author(s):  
Xiao Wang ◽  
Hui Lu ◽  
Jun Chen
Keyword(s):  
Thermal Conductivity ◽  
Laser Flash ◽  
Heating Process ◽  
X Ray Diffraction ◽  
Heat Spreader ◽  
Conductive Composites ◽  
Compression Direction ◽  
Thermal Analyzer ◽  
Thermally Conductive ◽  
Plane Direction

In this work, ultra-high molecular weight polyethylene (UHMWPE)/natural flake graphite (NG) polymer composites with the extraordinary high thermal conductivity were prepared by a facile mixed-heating powder method. Morphology observation and X-ray diffraction (XRD) tests revealed that the NG flakes could be more tightly coated on the surface of UHMWPE granules by mixed-heating process and align horizontally (perpendicular to the hot compression direction of composites). Laser flash thermal analyzer (LFA) demonstrated that the thermal conductivity (TC) of composites with 21.6 vol% of NG reached 19.87 W/(m·K) and 10.67 W/(m·K) in the in-plane and through-plane direction, respectively. Application experiment further demonstrated that UHMWPE/NG composites had strong capability to dissipate the heat as heat spreader. The obtained results provided a valuable basis for fabricating high thermal conductive composites which can act as advanced thermal management materials.

Thermal Characterization of Carbon-Carbon Composites

2011 ◽  
Author(s):  
Messiha Saad ◽  
Darryl Baker ◽  
Rhys Reaves
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Specific Heat ◽  
Critical Role ◽  
Carbon Composite ◽  
Flash Method ◽  
Carbon Composites ◽  
Energy Storage Devices ◽  
Graphitized Carbon

Thermal properties of materials such as specific heat, thermal diffusivity, and thermal conductivity are very important in the engineering design process and analysis of aerospace vehicles as well as space systems. These properties are also important in power generation, transportation, and energy storage devices including fuel cells and solar cells. Thermal conductivity plays a critical role in the performance of materials in high temperature applications. Thermal conductivity is the property that determines the working temperature levels of the material, and it is an important parameter in problems involving heat transfer and thermal structures. The objective of this research is to develop thermal properties data base for carbon-carbon and graphitized carbon-carbon composite materials. The carbon-carbon composites tested were produced by the Resin Transfer Molding (RTM) process using T300 2-D carbon fabric and Primaset PT-30 cyanate ester. The graphitized carbon-carbon composite was heat treated to 2500°C. The flash method was used to measure the thermal diffusivity of the materials; this method is based on America Society for Testing and Materials, ASTM E1461 standard. In addition, the differential scanning calorimeter was used in accordance with the ASTM E1269 standard to determine the specific heat. The thermal conductivity was determined using the measured values of their thermal diffusivity, specific heat, and the density of the materials.

scholarly journals Improving the Actuation Speed and Multi-Cyclic Actuation Characteristics of Silicone/Ethanol Soft Actuators

Actuators ◽  
2020 ◽  
Vol 9 (3) ◽  
pp. 62 ◽  
Author(s):  
Boxi Xia ◽  
Aslan Miriyev ◽  
Cesar Trujillo ◽  
Neil Chen ◽  
Mark Cartolano ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Short Term Memory ◽  
Conductive Filler ◽  
Thermally Driven ◽  
Thermally Conductive ◽  
Ethanol Evaporation ◽  
Long Short Term Memory ◽  
Soft Actuators ◽  
Robotic Applications ◽  
Soft Composite

The actuation of silicone/ethanol soft composite material-actuators is based on the phase change of ethanol upon heating, followed by the expansion of the whole composite, exhibiting high actuation stress and strain. However, the low thermal conductivity of silicone rubber hinders uniform heating throughout the material, creating overheated damaged areas in the silicone matrix and accelerating ethanol evaporation. This limits the actuation speed and the total number of operation cycles of these thermally-driven soft actuators. In this paper, we showed that adding 8 wt.% of diamond nanoparticle-based thermally conductive filler increases the thermal conductivity (from 0.190 W/mK to 0.212 W/mK), actuation speed and amount of operation cycles of silicone/ethanol actuators, while not affecting the mechanical properties. We performed multi-cyclic actuation tests and showed that the faster and longer operation of 8 wt.% filler material-actuators allows collecting enough reliable data for computational methods to model further actuation behavior. We successfully implemented a long short-term memory (LSTM) neural network model to predict the actuation force exerted in a uniform multi-cyclic actuation experiment. This work paves the way for a broader implementation of soft thermally-driven actuators in various robotic applications.

scholarly journals Measurements of Aluminum-Annealed Pyrolytic Graphite Composite Baseplates with Improved Thermal Conductivity

2021 ◽  
Vol 16 (2) ◽  
pp. 042-047
Author(s):  
Yanfei Bian ◽  
SHI Jian-zhou ◽  
XIE Ming-jun ◽  
CAI Meng
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Management ◽  
Pure Aluminum ◽  
Pyrolytic Graphite ◽  
Aluminum Plate ◽  
Graphite Composite ◽  
Conductive Composites ◽  
Thermal Potential ◽  
Thermally Conductive

Annealed pyrolytic graphite (APG) is a material with thermal conductivity of about 1500 W/(m·K). This property may enable the usage of APG’s thermal potential to develop highly thermally conductive composites for devices requiring effective thermal management. In this paper, APG has been encapsulated in aluminum by brazing, and the thermal properties of Al-APG composite baseplates were measured. The results show that the thermal conductivity of the Al-APG composite baseplates is about 620 W/(m·K), which is four times higher than the pure aluminum plate (152 W/(m·K)).

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