Acrylic fiber is one of the earliest developed chemical fiber species in China. Acrylic products are fluffy, warm, soft to the touch, and have good weather resistance and anti-mildew and anti-moth properties. Acrylic fiber has a wide range of applicability, but the wastewater generated during its production is a major problem facing the world. The complex composition and high toxicity of acrylic wastewater pollutants, the presence of many oligomers and other difficult to biodegrade, as well as the presence of sulfate, sulfite and other bioinhibitory components, make the biochemical properties of acrylic wastewater very low, making it very difficult to treat. In this paper, we propose an acrylic wastewater treatment method based on deep oxidation technology to solve this problem, which can effectively carry out wastewater treatment and make it meet the national discharge standards.