Metrological Analysis of the Relationship Model between the Properties of Piezoelectric Materials

The properties of piezoelectric materials due to the effect of electrical, mechanical, thermal, radiation, and chemical parameters are systematized. On the basis of Maxwell's relations (obtained from expressions for thermodynamic functions) and the application of the system analysis methodology, it made it possible to develop an analytical model of the relationship between the parameters and properties of piezoelectrics in the form of a system of equations. The results of the metrological analysis of an analytical model, which made it possible to identify the sources of additional errors in the measurement of parameters, to derive formulas for their calculation, which in turn contributes to an increase in the accuracy of measurements of the piezoelectrics parameters and products based on them, are presented.

VISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA

Проведен анализ основных источников методических погрешностей магнитного ротационного вискозиметра, позволивший усовершенствовать конструкцию и исключить критические режимы исследований. Теоретическая оценка систематической погрешности прибора показала, что значение относительной ошибки измерений можно довести до значения менее 1%. Наибольший вклад в систематическую погрешность прибора вносит нестабильность температурного режима исследуемой наножидкости и неточность определения высоты слоя жидкости, контактирующего с измерительным цилиндром. Измерение вязкости эталонных жидкостей на магнитном вискозиметре показало, что экспериментальные значения незначительно, примерно на 0,9% завышены. Тарировка прибора на различных эталонных жидкостях позволила снизить суммарную ошибку измерений до десятых долей процента. Магнитный ротационный вискозиметр может найти применение при нестандартных научных исследованиях структуры и реологических характеристик наножидкостей, для оперативного контроля процессов синтеза магнитных жидкостей и аттестации магнитных наножидкостей, предназначенных для технического применения. An analysis is carried out of the main sources of methodological errors of the magnetic rotary viscometer. The analysis allowed to improve design and to eliminate critical modes of the research. Theoretical evaluations of the systematic error of the device showed that the value of the relative measurement error can be brought to a value of less than 1%. The greatest contribution to the systematic error of the device is made by the instability of the temperature regime of the nanofluid under study and by the inaccuracy of determining the height of the liquid layer in contact with the measuring cylinder. The measurement of the viscosity of the reference liquids on the magnetic viscometer showed that experimental values are slightly, by about 0.9% overestimated. Calibration of the device on various reference liquids allowed reducing the total measurement error down to tenths of a percent. The magnetic rotary viscometer can be used in non-standard scientific studies of the structure and rheological characteristics of nanofluids, for operational control of the processes of synthesis of magnetic liquids and certification of magnetic nanofluids intended for technical use.

Application of an automated complex resistance and phase difference measuring method for rheographic studies of human cardiovascular system

The structure of an automated system for measuring the complex resistance of the human body and the phase difference is proposed. It is used in the rheographic method for diagnosing human cardiovascular system diseases using a multilevel microcontroller structure. The metrological analysis of the automated system made it possible to achieve an increase in the measurement accuracy both by reducing the methodological and instrumental components of measurement errors. The relative basic measurement error does not exceed ± 0.5%.

Metrological aspects of an automated method for measuring electrophysical parameters of soft magnetic materials

The structure of an automated system for measuring magnetic-hysteresis loops, normal magnetization curve, magnetic permeability with an error of no more than ± 1% is proposed. The measuring principle is based on the inferential measurements of the magnetic induction and the coercive force by integrating the secondary voltage and the excitation current. As a result of metrological analysis, an increase in the measurements accuracy is achieved both by improving the hardware implementation and calibrating the measuring channels, by introducing a correction for the systematic component of the error.

Application of Brillouin scattering in optic-fiber sensors

The article analyses possible applications for Brillouin scattering in optic-fiber sensors. They make it possible to do temperature and physical strain measurements with high accuracy for long line sections. The functional dependences of the output signals characteristics on parameters measured by the sensors are studied. Of particular interest are the results of the analysis of the spectral component shifts in the Brillouin light scattering depending on the fiber elongation and temperature. After a brief review of the basic theoretical principles the results of some researches aimed to expand the dynamic range and to increase spatial resolution. The results of simulation in professional design software environment OptiSystem 17.1. are described. The results are obtained by experimental research based on Brillouin reflectometer AQ8603 manufactured by “ANDO” (Japan). They show that it is possible to implement optic-fiber sensors based on Brillouin scattering in telecommunication systems, oil and gas industry, in electric-power industry, construction, aviation and space industry. The objectives for further research are to perform metrological analysis at all stages of the method implementation, to complete the base of Brillouin spectrograms for optical fiber of various types and to improve algorithms for automated processing spectra in order to expand functionality of the systems.

A portable calorimeter for measuring the calorific value of natural gas

Natural gas quality assessment is a relevant issue. A critical analysis of calorimeter designs for measuring the calorific value of natural gas was carried out. The most common methods for determining the calorific value of natural gas are as follows: direct by gas calorimeters; indirect by gas chromatographs; indirect, based on correlations. The advantages of isoperibolic calorimeters of measuring calorific value of natural gas directly in the consumer’s conditions are substantiated. The design of a portable calorimeter containing a thermostated shell, calorimetric tank, Peltier element with tank, circulating pump, gas burner, thermostat systems, metered supply of natural gas and air, fuel ignition, sensors, combustion analyzer and control and measurement unit, was developed. The geometric dimensions of the calorimetric tank are optimized, materials and technologies of manufacturing parts are specified. The metrological analysis of the developed portable calorimeter was carried out. A method for measuring the calorific value of natural gas directly in the conditions of household consumers and transport enterprises was developed. The results of testing the prototype calorimeter in the laboratory confirmed its high performance and metrological characteristics, and the deviation of the measurement of the calorific value of natural gas from that determined using a gas chromatograph was 0.6%.

PARAMETERS OF CASTLE FORTIFICATIONS ON THE TERRITORY OF THE WESTERN REGIONS OF UKRAINE OF THE MIDDLE OF THE 16TH - BEGINNING OF THE 18TH CENTURIES

A comparative typological and metrological analysis of defensive structures of 53 castles in the western regions of Ukraine is carried out. Fortification lines of castles are classified, based on the division of fortresses by their dimensions, proposed in the treatise on fortification in 1659 by J. Naronovich-Naronsky. The reasons for the functioning of castle fortifications with different levels of defense in one period are explained.

Preliminary Research: Validation of the Method of Evaluating Resistance to Surface Wetting with Liquid of Protective Materials Intended for Polymer Protective Gloves

The article presents validation argumentation of the novel method of evaluating resistance to surface wetting with different liquids of protective materials intended for polymer protective gloves based on the three parameters: water permeability index, non-wettability index and absorption index. Using our own method of evaluating resistance to surface wetting, it was shown that the knurled structure of the palm part of polymer protective gloves may inhibit transport of harmful and hazardous liquids outside the area of the protective glove. Currently, there is lack of objectifying methods for evaluation of surface wettability focused on the mentioned aspects. In view of the above facts, an original method for evaluating the resistance of protective materials to surface wetting with mineral oils and water has been invented and validated. It was assumed that the non-wettability index will be subjected to metrological analysis. Consequently, the validation process refers to this index. A precise assessment of the uncertainty budget of the individual components was obtained. On the basis of the obtained results, the measurement errors that may affect the quality and reliability of the test result performed in the laboratory were identified.

Application of GIS Tools in the Measurement Analysis of Urban Spatial Layouts Using the Square Grid Method

The principal aim of this paper is to present the capabilities of newly developed GIS tools for measurement analysis of urban spatial layouts, using the square grid method. The study of urban morphology and metrology is a multistage process, which involves the metrological analysis of town plans. The main research step is the determination of measurement modules of town layouts, using the square grid. By using GIS software, the authors developed a new tool, named HGIS Tools, which allow to create any number of modular grids with the selected cell size that corresponds to urban units of distance and surface area. When investigating a large number of towns and cities, this offers a significant improvement of the research procedure. The paper presents a test of the tool’s potential on the example of regular medieval towns from the area of the former Teutonic Order state (currently the territory of Poland), diversified in terms of size, genesis and morphometrics. The obtained results confirmed that HGIS Tools allowed to determine the hypothetical measurement module of the layout of the cities studied. The results were consistent with the analyses of other authors carried out with the traditional grid-square methods. The test of the HGIS Tools showed their significant potential in conducting morphometric analyses of spatial arrangements of urban spatial layout on a larger scale.