The effect of microtexture on the liquid flow over the sheets

This work considers the method of the corrugated sheet arrangement near the column wall with the aim to limit liquid fall on the wall and increase liquid concentration in the near-wall area. Experiments were carried out at the corrugated Koch 1Y packing sheets for various liquid flow rates. This report presents experimental results on the character of liquid flow near the edge of corrugated sheets and the effect of the middle sheet shift from the edge of the packing. The ribs of this sheet are directed downward to the edge of the packing. Test was performed for two positions of the middle sheet: to study the effect of microtexture orientation at the sheet, whose ribs are directed downward to the packing edge, on liquid distribution under the packing. Experiments were carried out for liquid flow rates of 1-12 ml/s.

Flexible distillation test rig on a laboratory scale for characterization of additively manufactured packings

Additive manufacturing is increasingly being used to develop innovative packings for absorption and desorption columns. Since distillation has not been in focus so far, this paper aims to fill this gap. The objective is to obtain a miniaturized 3D printed packed column with optimized properties in terms of scalability and reproducibility, which increases process development efficiency. For this purpose, a flexible laboratory scale test rig is presented combining standard laboratory equipment with 3D printed components such as innovative multifunctional trays or the column wall with packing. The test rig offers a particularly wide operating range (F=0.15 Pa…1.0 Pa) for column diameters between 20 mm and 50 mm. First results regarding the time to reach steady-state, operational stability and separation efficiency measurements are presented using a 3D printable version of the Rombopak 9M. Currently, innovative packings are being characterized, which should exhibit a optimized bevavior regarding scalability, reproducibility and separation efficiency.

Analysis of the estimated remaining service life of gas rectification columns

Gas rectification columns are process apparatuses which are very important part of each onshore plant. Sudden failure of these types of columns causes huge daily losses, while fluid leakage can be very dangerous for the people and hazardous for the environment. For that reason, a regular and correct examination of the column is of great importance for the continual process of leading. Together with the detailed examination of the column, a risk-based inspection was applied to maximize savings, both material, time, and costs. The expected remaining service life of rectification columns was also analyzed, while the corrosion rates were calculated according to the various international standards. The minimum required column wall thickness was calculated according to the most commonly used international standard and the obtained difference was analyzed. Detailed analysis of the total risks of the column due to potential failure is presented.

A Comparison Study on the Effect of Various Layered Sandy Soil Deposited on Final Settlement under Dynamic Loading

The foundation is expansion in base of column, wall or other structure in order to transmit the loads from the structure to under footing with a suitable pressure with soil property. There are two conditions to design foundation: 1. The stress is applied by footing on soil is not exceeded allowable bearing capacity ( ). 2. The foundation settlement and differential settlement are due to applied loads are not exceeding the allowable settlement that based on the type and size of structure, the nature of soil. Rigid square machine footing with dimension 200*200 mm with two types of relative density (50 and 85)% medium and dense density respectively are using in this study in different 28 models to show the effect of layered sandy soil in two configuration, medium-dense MD and dense-medium DM on the final settlement in magnitudes and behaviors under dynamics loads applying with different amplitude of loads (0.25 and 2) tons at surface with amplitude-frequency 0.5 Hz with explain the effect of reinforcements material on reduction the magnitude of settlement. The final results appeared with respect to the specified continuous pressure and the number of loading cycles, the resulting settlement from the dynamic loading increases with the increase in the dynamic pressure magnitude, the variation on densities of layered soil effect on the amount of settlement due to different loads applied...

ANALYSIS OF A CANTILEVER COLUMN SUBJECTED TO CYCLIC LOADING

In a seismic incident, the structural steel columns are commonly damaged with local buckling formulation at either the top or bottom ends. This study analyzes and simulates the hysteretic behavior of a hollow square steel column under cyclic loading by adopting the fiber-element approach. This method discretizes the hinge zone into a series of fibers and considers buckling behavior of those fibers along the column wall. The analytical result was achieved in good agreement with the component test.

Absorber Sizing and Costing Required to Control SO2 Emission from A Combustion System

This work was predicated on the design and costing of a packed column absorber required to remove SO2 from an air/SO2 mixture. The absorber is intended to be developed into an already existing combustion system as a retrofit. The gas flow rate basis of the computation was 40,000Kg/h. The Onda Method was used to estimate the column height as 9m and the column diameter as 2.5m while the column wall thickness as well as the domed head thickness was found to be 9mm using the BS 5500 Standard Method. In order to limit expenses, H2O was utilized as the absorber solvent and a flow rate of 29.5Kg/s to limit solvent usage. A pressure drop of 20mmH2O/m was assumed in the design with metal pall rings of diameter 51mm and surface area of 102m2/m3 chosen as the packing material. The study estimated a profound $306,559.87 as the cost of the absorber required to remove 95% SO2 content from the combustion waste stream.

Theoretical Analysis of Forced Segmented Temperature Gradients in Liquid Chromatography

An equilibrium model is applied to study the effect of forced temperature gradients introduced through heat exchange via specific segments of the wall of a chromatographic column operating with a liquid mobile phase. For illustration of the principle, the column is divided into two segments in such a manner that the first segment is kept at a fixed reference temperature, while the temperature of the second segment can be changed stepwise through fixed heating or cooling over the column wall to modulate the migration speeds of the solute concentration profiles. The method of characteristics is used to obtain the solution trajectories analytically. It is demonstrated that appropriate heating or cooling in the second segment can accelerate or decelerate the specific concentration profiles in order to improve certain performance criteria. The results obtained verify that the proposed analysis is well suited to evaluate the application of forced segmented temperature gradients. The suggested gradient procedure provides the potential to reduce the cycle time and, thus, improving the production rate of the chromatographic separation process compared to conventional isothermal (isocratic) operation.