Dyeing of cotton fabric by Caesalpinia sappan aqueous extract at different temperatures and mordants

The colour is one of the most important features in textile industry and customers requirements. Synthetic colours are available at affordable prices due to their bulk production. On the other hand, they pose undesirable taste (in case of foods) and harmful effects to ecosystem. The natural colours when used in textiles do not threat the environments and do not cause any skin allergy, toxicity and other hazards to living things as compared to the synthetic counterparts. In the present study, dyeing experiments were conducted with the aqueous extract of bark chips of Caesalpinia sappan at 60, 80 and100° C and using different mordant treatments. The fastness to washing for most of cotton fabrics showed fair grey scale rating. Among the mordants Alum, CuSo4 and Myrobalan used, the natural mordant myrobalan showed poor fastness properties compared to other two mordants. The staining tests showed that most of fabrics exhibited only slight/completely no pilling in majority of the treatments.

Green Miles in Dyeing Technology Metal-Rich Pumpkin Extracts in Aid of Natural Dyes

To reduce environmental pollution, it is essential to use green processes in dyeing and meet its requirements. One of the common methods to get better results in dyeing is to use mordant. To get a green dyeing, using natural mordant (bio-mordant) is very effective, but the search for an alternative having a higher stability and absorption interval, along with an absolute affinity towards natural fibers of various kinds was central to the focus of studies in the meanwhile. Pumpkin extract as a natural source metal-rich can be used as a bio-mordant in green dyeing of natural fibers such as wool fibers. Two natural dyes native to Iran; Reseda luteolaare and Madder were employed in this study. The effectiveness of bio-mordant presence on fibers was evaluated by FTIR-ATR test from mordanted and mordanted-dyed wool samples. Fastness performance of wool dyes with pumpkin alternated from good to excellent depending on natural dye type and concentration, due to the formation of complex structures that compensated for the lack of affinity-characteristic of tannin-based first-generation biomordants, at best with good fastness.

Green Extraction, Characterization, Applications and Antimicrobial Analysis of Natural Dye from Phyllanthus emblica

Global consciousness towards the organic value of eco-friendly products has attracted the interest of people towards the use of naturally dyed textiles and organic mordants. The present study has been focused not only on exploring the bio-colourant activity of Phyllanthus emblica (Amala) but also on the application of natural mordant for textile dyeing and analysis of its medicinal properties. It has been discovered from the investigation that biomordants like extract of Aloe vera’s as well as extract of mango’s bark extract were able to evince their characteristic colour ameliorate behaviour close to synthetic ones. Besides, the disparity in absorbance band in ultraviolet spectroscopy, distinction in functional groups and differences in surface morphology of two extracted dyes were observed that provided information on colour variation in the cotton fabrics. An eagle gray shade and brown-hued on the cotton fabric were noticed from water and ethanol extracted dyes, respectively. Further, it is confirmed that the natural dyes contain bioactive phytochemicals like tannins, phenols and flavonoids that provide a significant antibacterial activity which will help it to be beneficially utilized in protective medical clothing.

Aplikasi Mordan Tanin pada Pewarnaan Kain Batik Katun Menggunakan Warna Alam Tingi (Ceriops tagal)

The aim of the study was to evaluate the performance of tannin mordant from Psidium guajava leaves, Peltophorum pterocarpum bark, and Coffea arabica leaves in cotton batik dyeing using tingi bark (Ceriops tagal). This research was conducted by initial quantitative analysis of each extract to measure the quantity of tannin using UV-Vis spectrophotometry with tannic acid as a standard solution. The next process was a fabric pre-mordanting using each mordant extract, batik process, coloring with tingi bark extract, and post-mordanting using each alum solution and guava leaves extract. The dyed batik fabric was tested toward its color intensity and durability/fastness properties. From the quantitative analysis, guava leaves extract contains the biggest tannin content compared with jambal bark and coffee leaves extract, which is 1151.5 μg/mL. The dyed sample from combination of Guava leaves extract pre-mordanting with alum post-mordanting provided the best color intensity of 15.52. While all variables had an equal good value for washing fastness. It can be concluded that all material had potential as natural mordant for cotton batik dyeing with natural dye, but with consideration of using metal mordant for combination to get better results in terms of both color intensity and fastness properties.Keywords: batik; biomordant; natural dye; tannin mordant A B S T R A KTujuan dari penelitian ini adalah untuk mengetahui kinerja mordan tanin dari daun jambu biji (Psidium guajava), kulit kayu jambal (Peltophorum pterocarpum) dan daun kopi (Coffea arabica) dalam pewarnaan kain batik katun dengan pewarna alami tingi (Ceriops tagal). Penelitian dilakukan dengan terlebih dahulu mengukur kadar tanin total dari masing-masing ekstrak secara kuantitatif menggunakan spektrofotometri UV-Vis dengan larutan standar asam tanat. Proses selanjutnya adalah mordan awal kain menggunakan masing-masing ekstrak mordan, pembatikan, pewarnaan menggunakan ekstrak kulit kayu tingi, dan mordan akhir menggunakan masing-masing larutan tawas dan ekstrak daun jambu biji. Kain batik berwarna diuji ketuaan warna dan ketahanan luntur warnanya. Dari hasil analisis kuantitatif, didapatkan kandungan tanin terbesar dari ekstrak daun jambu biji yaitu 1.151,5 μg/mL. Hasil uji ketuaan warna paling besar didapatkan dari perlakuan mordan awal daun jambu biji dan mordan akhir tawas dengan nilai 15,52, sedangkan ketahanan luntur warna terhadap pencucian secara rata-rata memberikan nilai 4 (baik) untuk semua variabel. Kesimpulan yang dapat diambil yaitu ekstrak daun jambu biji, kulit kayu jambal, dan daun kopi memiliki potensi untuk digunakan sebagai bahan mordan pada pewarnaan batik. Penggunaan ketiga bahan mordan alami memerlukan kehadiran mordan logam untuk memperkuat intensitas warna dan ketahanan luntur warna kain.Kata kunci: batik; biomordan; mordan tannin; pewarna alam

Eco-friendly Methods of Natural Dye Extraction from Bark of Ficus religiosa and Their Impacts on Dyeing Technology in Nepal

Plant-based natural dyes are eco-friendly and less allergic to the human body. Different reports on toxicity and allergic reactions that appeared in synthetic dyes cause interest in natural dyes in recent years. The present study focused on the feasibility of aqueous extraction of plant dyes from the bark of Ficus religiosa (Peepal), a historical tree of Hindu culture. Extracted dyes were characterized by ultra-violet visible (UV-Vis) spectroscopy and Fourier transform infrared (FTIR) spectroscopy to reveal the structural and functional confirmation of extracted dye. Dye was used for dyeing fabric using both natural and commercial mordant. Mordants such as lemon juice and metallic salts such as potassium dichromate (K2Cr2O7), copper sulphate (CuSO4.5H2O), and iron sulphate (FeSO4) are used to set extracted dye on cotton fabrics and other fibers. This research aims to find the effectiveness and feasibility study of the use of natural mordant instead of metallic mordant. The use of natural dyeing with natural mordant is very effective for health purpose but found to be expensive.

Colorimetric Analysis and Fastness Properties of Jute Fabric Dyed with Eucalyptus Leaves

Natural dyestuff has reverted its position in the colouration of textile substrates due to rising concerns of consumers and buyers, particularly about environmental impacts and health issues. Eucalyptus leaves were selected in this study as a source of natural dye along with some of the most generally used mordants to observe the impact of dyeing on jute fabric while trying to keep the dyeing parameters at a minimum level. Dyes were extracted from eucalyptus leaves by boiling in water. Then, the fabric was pre-mordanted using different synthetic mordanting agents, such as alum, potassium dichromate, copper sulphate and ferrous sulphate, which are generally used to substantively enhance the dyestuff on textile fabrics and to improve the fastness properties. Synthetic mordant was used here instead of natural mordant due to the better dyeing compatibility of jute fabric with eucalyptus leaves, since natural mordant has little effect on jute fabric during the process of dyeing. Another aim of this research is to curb the time and energy consumption of the jute dyeing process and so the dyeing is carried out at 75 °C for about 30 minutes. Various types of evaluations were conducted through visual assessment, checking the colour-coordinate values and colour strength values. While colour fastness properties were evaluated by different fastness testing, such as colour fastness to water, washing, rubbing and perspiration. This dyeing process yields a colour range from yellowish to brown with the variation of mordants applied on the fabric. In addition to that, colour co-ordinate and colour strength values ensure better results of dyed fabrics pretreated with ferrous sulphate. Jute fabric dyed with only extracted eucalyptus solution provided satisfactory results in all colour fastness tests, while fabric treated with different mordants showed variations in fastness ratings, and fabric treated with ferrous sulphate and copper sulphate had slightly better fastness ratings.