Low-temperature, sol–gel-synthesized, silver-doped titanium oxide coatings to improve ultraviolet-blocking properties for cotton fabrics

2007 ◽  
Vol 106 (1) ◽  
pp. 514-525 ◽  
Author(s):  
Nurhan Onar ◽  
M. Faruk Ebeoglugil ◽  
Isıl Kayatekin ◽  
Erdal Celik
2011 ◽  
Vol 71-78 ◽  
pp. 972-975 ◽  
Author(s):  
Hui Dong Su ◽  
Hong Lei Du

Titanium oxide coatings(TiO2/Ti) were formed on the titanium surface by micro-arc oxidation(MAO) in Na3PO4solution.And using the TiO2/Ti as anod electrode, the titanium as counter electrode in the system of three-dimensional electrode.Coated γ- Al2O3(TiO2/γ-Al2O3) that prepared by sol-gel dipcoating method ,and scrap iron mixture as particle electrode, combining with the UV lamp and regulated power supply make up the three-dimensional electrode photoelectrocatalysis system. The photoelectrocatalysis system use 0.02M Na2SO4aqueous solution as supporting electrolyte.The photoelectrocatalytic ability of titanium oxide coatings were evaluated by photoelectrocatalytic degradation of methylene blue aqueous solution.The experiment demonstrate that compare to photoelectrocatalytic degradation of single TiO2/Ti film and only adsorbtion, the photoelectrocatalysis of three-dimensional electrode with coated particle electrode have the synergistic effect with them, which can improve the degradation of methylene blue aqueous solution. When the methylthionine chloride concentration of 5mg/L, cell voltage of 7V. The three-dimensional electrode photoelectrocatalysis degradation of methylene blue compare to traditional two-dimensional plate electrodes which without particle electrode increase 43.35% after 3 hours photoelectrocatalysis.


2012 ◽  
Vol 260-261 ◽  
pp. 1041-1046 ◽  
Author(s):  
Shi Ye Feng ◽  
Pan Gao ◽  
Chang Qing Dong ◽  
Qiang Lu

A series of manganese-cerium oxide support titanium oxide with different Fe/Ti, Ce/Ti ratio were investigated for selectivity catalytic reduction of NO low at temperature with NH3 as a reducing agent. The catalysts base Mn/TiO2were prepared by sol-gel. The effect of amount of Ce and Fe oxide on the NO conversion of Mn/TiO22was studied. X-ray diffraction (XRD), temperature program desorption (TPD) were carried out. It was known that cerium oxides and iron oxide promoted preformance of Mn/TiO2 for low temperature. because Lewis is mainly take important role in the reaction for low temperature.


2010 ◽  
Vol 156-157 ◽  
pp. 344-349 ◽  
Author(s):  
Hui Dong Su ◽  
Hong Lei Du

Titanium oxide coatings(TiO2/Ti) were formed on the titanium surface by micro-arc oxidation(MAO) in Na3PO4 solution.Using the TiO2/Ti as anod electrode, the titanium as counter electrode.Coated activated carbon(TiO2/AC) that prepared by sol-gel dipcoating method ,and activated carbon mixture as particle electrode,combining with the UV lamp and regulated power supply make up the three-dimensional electrode photoelectrocatalysis system. The photoelectrocatalysis system use Na2SO4 aqueous solution as supporting electrolyte.The photoelectrocatalytic ability of titanium oxide coatings were evaluated by photoelectrocatalytic degradation of methylthionine chloride aqueous solution.The experiment demonstrate that there was photoelectrocatalytic degradation of single TiO2/Ti film or only adsorbtion, the photoelectrocatalysis of three-dimensional electrode with particle electrode have the synergistic effect,which can improve the degradation of methylene blue aqueous solution.The influence of some factors was studied,including initial solution,cell voltage, electrolyte concentration and some other factors.When the methylthionine chloride concentration of 5mg/L, cell voltage of 8V, electrolyte concentration of 0.04M. The three-dimensional electrode photoelectrocatalysis degradation of methylene blue compare to traditional two-dimensional plate electrodes which without particle electrode increase 40.36% after 3 hours photoelectrocatalysis.


2003 ◽  
Vol 769 ◽  
Author(s):  
C. K. Liu ◽  
P. L. Cheng ◽  
S. Y. Y. Leung ◽  
T. W. Law ◽  
D. C. C. Lam

AbstractCapacitors, resistors and inductors are surface mounted components on circuit boards, which occupy up to 70% of the circuit board area. For selected applications, these passives are packaged inside green ceramic tape substrates and sintered at temperatures over 700°C in a co-fired process. These high temperature processes are incompatible with organic substrates, and low temperature processes are needed if passives are to be embedded into organic substrates. A new high permeability dual-phase Nickel Zinc Ferrite (DP NZF) core fabricated using a low temperature sol-gel route was developed for use in embedded inductors in organic substrates. Crystalline NZF powder was added to the sol-gel precursor of NZF. The solution was deposited onto the substrates as thin films and heat-treated at different temperatures. The changes in the microstructures were characterized using XRD and SEM. Results showed that addition of NZF powder induced low temperature transformation of the sol-gel NZF phase to high permeability phase at 250°C, which is approximately 350°C lower than transformation temperature for pure NZF sol gel films. Electrical measurements of DP NZF cored two-layered spiral inductors indicated that the inductance increased by three times compared to inductors without the DP NZF cores. From microstructural observations, the increase is correlated with the changes in microstructural connectivity of the powder phase.


Nanomaterials ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1738
Author(s):  
Saeid Vafaei ◽  
Alexander Wolosz ◽  
Catlin Ethridge ◽  
Udo Schnupf ◽  
Nagisa Hattori ◽  
...  

SnO2 nanoparticles are regarded as attractive, functional materials because of their versatile applications. SnO2 nanoaggregates with single-nanometer-scale lumpy surfaces provide opportunities to enhance hetero-material interfacial areas, leading to the performance improvement of materials and devices. For the first time, we demonstrate that SnO2 nanoaggregates with oxygen vacancies can be produced by a simple, low-temperature sol-gel approach combined with freeze-drying. We characterize the initiation of the low-temperature crystal growth of the obtained SnO2 nanoaggregates using high-resolution transmission electron microscopy (HRTEM). The results indicate that Sn (II) hydroxide precursors are converted into submicrometer-scale nanoaggregates consisting of uniform SnO2 spherical nanocrystals (2~5 nm in size). As the sol-gel reaction time increases, further crystallization is observed through the neighboring particles in a confined part of the aggregates, while the specific surface areas of the SnO2 samples increase concomitantly. In addition, X-ray photoelectron spectroscopy (XPS) measurements suggest that Sn (II) ions exist in the SnO2 samples when the reactions are stopped after a short time or when a relatively high concentration of Sn (II) is involved in the corresponding sol-gel reactions. Understanding this low-temperature growth of 3D SnO2 will provide new avenues for developing and producing high-performance, photofunctional nanomaterials via a cost-effective and scalable method.


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