Supercritical CO2 extraction of linseed: Optimization by experimental design with regards to oil yield and composition

2017 ◽  
Vol 119 (9) ◽  
pp. 1600078 ◽  
Author(s):  
Natacha Rombaut ◽  
Raphaëlle Savoire ◽  
Elisabeth Van Hecke ◽  
Brigitte Thomasset
Keyword(s):  
Experimental Design ◽  
Supercritical Co2 ◽  
Oil Yield ◽  
Supercritical Co2 Extraction

scholarly journals Obtaining of β-Sitosterol from Cardamom by Supercritical CO2 Extraction

2017 ◽  
Author(s):  
Hacer İçen ◽  
Hatice Tuğba Çelik ◽  
Mustafa Serhat Ekinci ◽  
Metin Gürü
Keyword(s):  
Flow Rate ◽  
Supercritical Co2 ◽  
Oil Yield ◽  
Gas Chromatography Mass Spectrometry ◽  
Operating Parameters ◽  
Protective Effects ◽  
Supercritical Co2 Extraction ◽  
Cosmetic Industry ◽  
Co2 Flow ◽  
Optimized Conditions

Cardamom is plant of the Zingiberaceae family. It has been used for the treatment of many diseases such as migraine, bronchitis, stomach and intestinal disorders. Cardamom contains triterpenes, resins, starch and fatty compounds. Phytosterols (stigmasterol, campesterol and β-sitosterol) are a group steroid alcohol in plants. They are used food, medicine and cosmetic industry. They are protective effects against some types of cancer too. Phytosterols are found in the vegetable oil such as the spindle, corn and soybean oil. This paper deals with the maximum oil and β-sitosterol yield were investigated by means of the supercritical CO2 extraction of cardamom. The effect of operating parameters as temperature, pressure and CO2 flow rate were investigated on oil yield. The amount of β-sitosterol was analyzed by Gas Chromatography-Mass Spectrometry (GC-MS) at optimized conditions. The optimized conditions were recorded as temperature of 40oC, pressure of 200 bar and CO2 flow rate of 4 L/min. The maximum oil yield and amount of β-sitosterol were found as 74.83 mg oil/g seed and 4.73 mg β-sitosterol/g seed cardamom under these conditions.

Effects of supercritical CO2 extraction parameters on soybean oil yield

2012 ◽  
Vol 90 (4) ◽  
pp. 693-699 ◽  
Author(s):  
Stela Jokić ◽  
Bence Nagy ◽  
Zoran Zeković ◽  
Senka Vidović ◽  
Mate Bilić ◽  
...  
Keyword(s):  
Soybean Oil ◽  
Supercritical Co2 ◽  
Oil Yield ◽  
Supercritical Co2 Extraction ◽  
Extraction Parameters

scholarly journals Optimized Supercritical CO2 Extraction Enhances the Recovery of Valuable Lipophilic Antioxidants and Other Constituents from Dual-Purpose Hop (Humulus lupulus L.) Variety Ella

Antioxidants ◽  
2021 ◽  
Vol 10 (6) ◽  
pp. 918
Author(s):  
Nóra Emilia Nagybákay ◽  
Michail Syrpas ◽  
Vaiva Vilimaitė ◽  
Laura Tamkutė ◽  
Audrius Pukalskas ◽  
...  
Keyword(s):  
Supercritical Co2 ◽  
Antioxidant Properties ◽  
Extraction Yield ◽  
Biologically Active ◽  
High Yield ◽  
Acid Extraction ◽  
Supercritical Co2 Extraction ◽  
Bioactive Constituents ◽  
Total Extract

The article presents the optimization of supercritical CO2 extraction (SFE-CO2) parameters using response surface methodology (RSM) with central composite design (CCD) in order to produce single variety hop (cv. Ella) extracts with high yield and strong in vitro antioxidant properties. Optimized SFE-CO2 (37 MPa, 43 °C, 80 min) yielded 26.3 g/100 g pellets of lipophilic fraction. This extract was rich in biologically active α- and β-bitter acids (522.8 and 345.0 mg/g extract, respectively), and exerted 1481 mg TE/g extract in vitro oxygen radical absorbance capacity (ORAC). Up to ~3-fold higher extraction yield, antioxidant recovery (389.8 mg TE/g pellets) and exhaustive bitter acid extraction (228.4 mg/g pellets) were achieved under the significantly shorter time compared to the commercially used one-stage SFE-CO2 at 10–15 MPa and 40 °C. Total carotenoid and chlorophyll content was negligible, amounting to <0.04% of the total extract mass. Fruity, herbal, spicy and woody odor of extracts could be attributed to the major identified volatiles, namely β-pinene, β-myrcene, β-humulene, α-humulene, α-selinene and methyl-4-decenoate. Rich in valuable bioactive constituents and flavor compounds, cv. Ella hop SFE-CO2 extracts could find multipurpose applications in food, pharmaceutical, nutraceutical and cosmetics industries.

scholarly journals Supercritical CO2 extraction of Moroccan argan (Argania spinosa L.) oil: Extraction kinetics and solubility determination

2021 ◽  
Vol 46 ◽  
pp. 101458
Author(s):  
Adil Mouahid ◽  
Isabelle Bombarda ◽  
Magalie Claeys-Bruno ◽  
Sandrine Amat ◽  
Emmanuelle Myotte ◽  
...  
Keyword(s):  
Supercritical Co2 ◽  
Oil Extraction ◽  
Supercritical Co2 Extraction ◽  
Extraction Kinetics ◽  
Argania Spinosa ◽  
Solubility Determination

scholarly journals Supercritical CO2 Extraction of Palladium Oxide from an Aluminosilicate-Supported Catalyst Enhanced by a Combination of Complexing Polymers and Piperidine

Molecules ◽  
2021 ◽  
Vol 26 (3) ◽  
pp. 684
Author(s):  
Andrea Ruiu ◽  
Bernhard Bauer-Siebenlist ◽  
Marin Senila ◽  
W. S. Jennifer Li ◽  
Karine Seaudeau-Pirouley ◽  
...  
Keyword(s):  
Energy Saving ◽  
Supercritical Co2 ◽  
Supported Catalyst ◽  
Precious Metals ◽  
Palladium Oxide ◽  
Supercritical Co2 Extraction ◽  
Wide Range

Precious metals, in particular Pd, have a wide range of applications in industry. Due to their scarcity, precious metals have to be recycled, preferably with green and energy-saving recycling processes. In this article, palladium extraction from an aluminosilicate-supported catalyst, containing about 2 wt% (weight%) of Pd (100% PdO), with supercritical CO2 (scCO2) assisted by complexing polymers is described. Two polymers, p(FDA)SH homopolymer and p(FDA-co-DPPS) copolymer (FDA: 1,1,2,2-tetrahydroperfluorodecyl acrylate; DPPS: 4-(diphenylphosphino)styrene), were tested with regards to their ability to extract palladium. Both polymers showed relatively low extraction conversions of approximately 18% and 30%, respectively. However, the addition of piperidine as activator for p(FDA-co-DPPS) allowed for an increase in the extraction conversion of up to 60%.

Particle size distribution and stratification of pelletized oilseeds affects cumulative supercritical CO2 extraction plots

2019 ◽  
Vol 146 ◽  
pp. 189-198 ◽  
Author(s):  
José M. del Valle ◽  
Constanza V. Carrasco ◽  
Felipe R. Toledo ◽  
Gonzalo A. Núñez
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Supercritical Co2 ◽  
Supercritical Co2 Extraction

Effect of pelletization on supercritical CO2 extraction of rosemary antioxidants

2019 ◽  
Vol 147 ◽  
pp. 162-171 ◽  
Author(s):  
Caroline Sielfeld ◽  
José M. del Valle ◽  
Federico Sastre
Keyword(s):  
Supercritical Co2 ◽  
Supercritical Co2 Extraction
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