The morphology of polymer fracture surfaces

2007 ◽  
Vol 3 (1) ◽  
pp. 91-101 ◽  
Author(s):  
J. P. Berry
Keyword(s):  
Fracture Surfaces ◽  
Polymer Fracture

Scanning tunneling microscope observations of polymer fracture surfaces

1992 ◽  
Vol 7 (5) ◽  
pp. 1292-1302 ◽  
Author(s):  
D.M. Kulawansa ◽  
S.C. Langford ◽  
J.T. Dickinson
Keyword(s):  
Crack Growth ◽  
Scanning Tunneling Microscope ◽  
Room Temperature ◽  
Slow Crack Growth ◽  
Liquid Nitrogen Temperature ◽  
Scanning Tunneling ◽  
Tunneling Microscope ◽  
Fracture Surfaces ◽  
Polymer Fracture ◽  
Double Torsion

Scanning tunneling microscope observations of gold-coated polymer fracture surfaces are reported. We compare nm-scale surface features of poly(methyl methacrylate) (PMMA) fractured under three different loading conditions: in tension at room temperature, in tension at liquid nitrogen temperature, and in the double torsion geometry at room temperature (slow crack growth). Fracture surfaces of polystyrene and polycarbonate loaded in tension at room temperature are also described. Each of these surfaces shows distinctive nm-scale features which we interpret in terms of the interaction between craze growth (fibril formation) and crack growth along the craze boundary. The resolution of these images is sufficient to greatly complement other fractographic studies.

New Dimensions in Freeze-Etching

1969 ◽  
Vol 27 ◽  
pp. 202-203 ◽  
Author(s):  
Russell L. Steere ◽  
Michael Moseley
Keyword(s):  
Fracture Surfaces ◽  
Aluminum Specimen ◽  
Specimen Holder ◽  
Freeze Etching ◽  
The Right

A redesigned specimen holder and cap have made possible the freeze-etching of both fracture surfaces of a frozen fractured specimen. In principal, the procedure involves freezing a specimen between two specimen holders (as shown in A, Fig. 1, and the left side of Fig. 2). The aluminum specimen holders and brass cap are constructed so that the upper specimen holder can be forced loose, turned over, and pressed down firmly against the specimen stage to a position represented by B, Fig. 1, and the right side of Fig. 2.

Locating Al in the DABCO catalyst before and after Al extraction

1990 ◽  
Vol 48 (4) ◽  
pp. 265-267
Author(s):  
Kathleen B. Reuter
Keyword(s):  
Active Site ◽  
Inverse Relationship ◽  
Transverse Direction ◽  
Reaction Rate ◽  
Acid Phosphate ◽  
Fracture Surfaces ◽  
Al Content ◽  
Before And After ◽  
Relationship Of

The reaction rate and efficiency of piperazine to 1,4-diazabicyclo-octane (DABCO) depends on the Si/Al ratio of the MFI topology catalysts. The Al was shown to be the active site, however, in the Si/Al range of 30-200 the reaction rate increases as the Si/Al ratio increases. The objective of this work was to determine the location and concentration of Al to explain this inverse relationship of Al content with reaction rate.Two silicalite catalysts in the form of 1/16 inch SiO2/Al2O3 bonded extrudates were examined: catalyst A with a Si/Al of 83; and catalyst B, the acid/phosphate Al extracted form of catalyst A, with a Si/Al of 175. Five extrudates from each catalyst were fractured in the transverse direction and particles were obtained from the fracture surfaces near the center of the extrudate diameter. Particles were also obtained from the outside surfaces of five extrudates.

scholarly journals A Model for Triboluminescence from Fracture Surfaces of Silica Glass

2015 ◽  
Vol 13 (0) ◽  
pp. 159-163
Author(s):  
Hiroki Kanehira ◽  
Muhammad Zainurin ◽  
Shuji Shimamura
Keyword(s):  
Silica Glass ◽  
Fracture Surfaces

scholarly journals Low Cycle Fatigue Characteristics of Oxygen-Free Copper for Electric Power Equipment

Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4237
Author(s):  
Takuma Tanaka ◽  
Togo Sugioka ◽  
Tatsuya Kobayashi ◽  
Ikuo Shohji ◽  
Yuya Shimada ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Electric Power ◽  
Stress Amplitude ◽  
Low Cycle Fatigue ◽  
Ebsd Analysis ◽  
Fatigue Properties ◽  
Power Equipment ◽  
Cycle Fatigue ◽  
Fracture Surfaces ◽  
Heat Treated

The effect of heat treatment on tensile and low cycle fatigue properties of the oxygen-free copper for electric power equipment was investigated. The heat treatment at 850 °C for 20 min, which corresponds to the vacuum brazing process, caused the grain growth and relaxation of strain by recrystallization, and thus, the residual stress in the oxygen-free copper was reduced. The tensile strength and 0.2% proof stress were decreased, and elongation was increased by the heat treatment accompanying recrystallization. The plastic strain in the heat-treated specimen was increased compared with that in the untreated specimen under the same stress amplitude condition, and thus, the low cycle fatigue life of the oxygen-free copper was degraded by the heat treatment. Striation was observed in the crack initiation area of the fractured surface in the case of the stress amplitude less than 100 MPa regardless of the presence of the heat treatment. With an increase in the stress amplitude, the river pattern and the quasicleavage fracture were mainly observed in the fracture surfaces of the untreated specimens, and they were observed with striations in the fracture surfaces of the heat-treated ones. The result of the electron backscattered diffraction (EBSD) analysis showed that the grain reference orientation deviation (GROD) map was confirmed to be effective to investigate the fatigue damage degree in the grain by low cycle fatigue. In addition, the EBSD analysis revealed that the grains were deformed, and the GROD value reached approximately 28° in the fractured areas of heat-treated specimens after the low cycle fatigue test.

scholarly journals Boundary Morphology for Hierarchical Simplification of Archaeological Fragments

2020 ◽  
Vol 4 (1) ◽  
pp. 46-63
Author(s):  
Hanan ElNaghy ◽  
Leo Dorst
Keyword(s):  
Mathematical Morphology ◽  
Masking Effect ◽  
Morphological Operations ◽  
Fracture Surfaces ◽  
Morphological Approach ◽  
Archaeological Artifacts ◽  
Scale Spaces ◽  
Extrusion Method

AbstractWhen fitting archaeological artifacts, one would like to have a representation that simplifies fragments while preserving their complementarity. In this paper, we propose to employ the scale-spaces of mathematical morphology to hierarchically simplify potentially fitting fracture surfaces. We study the masking effect when morphological operations are applied to selected subsets of objects. Since fitting locally depends on the complementarity of fractures only, we introduce ‘Boundary Morphology’ on surfaces rather than volumes. Moreover, demonstrating the Lipschitz nature of the terracotta fractures informs our novel extrusion method to compute both closing and opening operations simultaneously. We also show that in this proposed representation the effects of abrasion and uncertainty are naturally bounded, justifying the morphological approach. This work is an extension of our contribution earlier published in the proceedings of ISMM2019 [10].

scholarly journals Investigation of Failure in Gas Turbines: Part 2 — Engineering and Metallographic Aspects of Failure Investigation

1993 ◽  
Author(s):  
Robert E. Dundas
Keyword(s):  
Gas Turbine ◽  
Gas Turbines ◽  
Heavy Duty ◽  
Metallographic Examination ◽  
Fracture Surfaces ◽  
Failure Investigation ◽  
Materials Used ◽  
Component Failures

This paper opens with a discussion of the various mechanisms of cracking and fracture encountered in gas turbine failures, and discusses the use of metallographic examination of crack and fracture surfaces. The various types of materials used in the major components of heavy-duty industrial and aeroderivative gas turbines are tabulated. A collection of macroscopic and microscopic fractographs of the various mechanisms of failure in gas turbine components is then presented for reference in failure investigation. A discussion of compressor damage due to surge, as well as some overall observations on component failures, follows. Finally, a listing of the most likely types of failure of the various major components is given.

scholarly journals Evolution of Friction and Permeability in a Propped Fracture under Shear

Geofluids ◽  
2017 ◽  
Vol 2017 ◽  
pp. 1-13 ◽  
Author(s):  
Fengshou Zhang ◽  
Yi Fang ◽  
Derek Elsworth ◽  
Chaoyi Wang ◽  
Xiaofeng Yang
Keyword(s):  
Normal Stress ◽  
Shear Loading ◽  
Particle Crushing ◽  
Normal Loading ◽  
Fracture Surfaces ◽  
Frictional Strength ◽  
Transport Response ◽  
Shear Slip ◽  
High Normal Stress ◽  
Proppant Embedment

We explore the evolution of friction and permeability of a propped fracture under shear. We examine the effects of normal stress, proppant thickness, proppant size, and fracture wall texture on the frictional and transport response of proppant packs confined between planar fracture surfaces. The proppant-absent and proppant-filled fractures show different frictional strength. For fractures with proppants, the frictional response is mainly controlled by the normal stress and proppant thickness. The depth of shearing-concurrent striations on fracture surfaces suggests that the magnitude of proppant embedment is controlled by the applied normal stress. Under high normal stress, the reduced friction implies that shear slip is more likely to occur on propped fractures in deeper reservoirs. The increase in the number of proppant layers, from monolayer to triple layers, significantly increases the friction of the propped fracture due to the interlocking of the particles and jamming. Permeability of the propped fracture is mainly controlled by the magnitude of the normal stress, the proppant thickness, and the proppant grain size. Permeability of the propped fracture decreases during shearing due to proppant particle crushing and related clogging. Proppants are prone to crushing if the shear loading evolves concurrently with the normal loading.

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