Inductively Coupled Plasma Process for Reconditioning Ti and Ni Alloy Powders for Additive Manufacturing

Author(s):  
E. J. Garboczi ◽  
Adam J. Brooks ◽  
Lee Kerwin ◽  
Rutuja Samant
Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4267
Author(s):  
Stefano Ponzoni ◽  
Sonia Freddi ◽  
Marta Agati ◽  
Vincent Le Borgne ◽  
Simona Boninelli ◽  
...  

To exploit the optoelectronic properties of silicon nanostructures (SiNS) in real devices, it is fundamental to study the ultrafast processes involving the photogenerated charges separation, migration and lifetime after the optical excitation. Ultrafast time-resolved optical measurements provide such information. In the present paper, we report on the relaxation dynamics of photogenerated charge-carriers in ultrafine SiNS synthesized by means of inductively-coupled-plasma process. The carriers’ transient regime was characterized in high fluence regime by using a tunable pump photon energy and a broadband probe pulse with a photon energy ranging from 1.2 eV to 2.8 eV while varying the energy of the pump photons and their polarization. The SiNS consist of Si nanospheres and nanowires (NW) with a crystalline core embedded in a SiOx outer-shell. The NW inner core presents different typologies: long silicon nanowires (SiNW) characterized by a continuous core (with diameters between 2 nm and 15 nm and up to a few microns long), NW with disconnected fragments of SiNW (each fragment with a length down to a few nanometers), NW with a “chaplet-like” core and NW with core consisting of disconnected spherical Si nanocrystals. Most of these SiNS are asymmetric in shape. Our results reveal a photoabsorption (PA) channel for pump and probe parallel polarizations with a maximum around 2.6 eV, which can be associated to non-isotropic ultra-small SiNS and ascribed either to (i) electron absorption driven by the probe from some intermediate mid-gap states toward some empty state above the bottom of the conduction band or (ii) the Drude-like free-carrier presence induced by the direct-gap transition in the their band structure. Moreover, we pointed up the existence of a broadband and long-living photobleaching (PB) in the 1.2–2.0 eV energy range with a maximum intensity around 1.35 eV which could be associated to some oxygen related defect states present at the Si/SiOx interface. On the other hand, this wide spectral energy PB can be also due to both silicon oxide band-tail recombination and small Si nanostructure excitonic transition.


2021 ◽  
Vol 60 (1) ◽  
pp. 936-945
Author(s):  
Nikolai Ozerskoi ◽  
Alexey Silin ◽  
Nikolay Razumov ◽  
Anatoly Popovich

Abstract For use in additive manufacturing (AM), powders that have a spherical shape, high fluidity, and packing density are required. One of the methods for producing spherical powders is spheroidization using inductively coupled plasma. In this work, the powder of steel grade EI961 was used. To obtain the powder for subsequent use in 3D printing, the selection of modes was carried out with the change in various parameters of the unit: different power, powder feed rate to the plasma as well as the height of feed rate. The optimal spheroidization mode is as follows: power of 15 kW, pressure of 1 atm, feed rate height of 0 mm, and powder feed rate of 28 g·min−1. The temperature distribution over the plasma torch cross section was calculated and the maximum plasma temperature was also determined. In addition, the effect of plasma treatment on the granulometric composition, phase composition, and chemical composition was studied.


2016 ◽  
Vol 704 ◽  
pp. 282-286 ◽  
Author(s):  
Romain Vert ◽  
Remy Pontone ◽  
Richard Dolbec ◽  
Luc Dionne ◽  
M.I. Boulos

Powder metallurgy technologies require specific powders to ensure a good quality to the manufactured parts. The critical properties are; the powder chemistry, flow ability, packing density, and the absence of porosity. This review highlights the capability of Tekna’s Inductively Coupled Plasma (ICP) technology for the production of high quality powders for the additive manufacturing industry.


Materials ◽  
2019 ◽  
Vol 12 (15) ◽  
pp. 2426 ◽  
Author(s):  
Mirko Riede ◽  
Matthias Knoll ◽  
Christoph Wilsnack ◽  
Samira Gruber ◽  
Alba Alegre Cubillo ◽  
...  

Recently, additive manufacturing (AM) by laser metal deposition (LMD) has become a key technology for fabricating highly complex parts without any support structures. Compared to the well-known powder bed fusion process, LMD enhances manufacturing possibilities to overcome AM-specific challenges such as process inherent porosity, minor build rates, and limited part size. Moreover, the advantages aforementioned combined with conventional machining enable novel manufacturing approaches in various fields of applications. Within this contribution, the additive manufacturing of filigree flexure pivots using 316L-Si by means of LMD with powder is presented. Frictionless flexure pivot bearings are used in space mechanisms that require high reliability, accuracy, and technical cleanliness. As a contribution to part qualification, the manufacturing process, powder material, and fabricated specimens were investigated in a comprehensive manner. Due to its major impact on the process, the chemical powder composition was characterized in detail by energy dispersive X-ray spectroscopy (EDX) and inductively coupled plasma optical emission spectrometry (ICP-OES). Moreover, a profound characterization of the powder morphology and flowability was carried out using scanning electron microscopy (SEM) and novel rheological investigation techniques. Furthermore, quantitative image analysis, mechanical testing, laser scanning microscopy, and 3D shape measurement of manufactured specimens were conducted. As a result, the gained knowledge was applied for the AM-specific redesign of the flexure pivot. Finally, a qualified flexure pivot has been manufactured in a hybrid manner to subsequently ensure its long-term durability in a lifetime test bench.


RSC Advances ◽  
2014 ◽  
Vol 4 (108) ◽  
pp. 63349-63353 ◽  
Author(s):  
Eunho Kim ◽  
Yong Seung Kim ◽  
Jaehyun Park ◽  
Sajjad Hussain ◽  
Seung-Hyun Chun ◽  
...  

Graphene film growth on a Cu–Ni alloy thin film with various alloy compositions is reported in this paper.


Author(s):  
Yu-Hsin Lin ◽  
Hung-Ling Yin ◽  
Yung-Yu Hsu ◽  
Yi-Chiuen Hu ◽  
Hsiao-Yu Chou ◽  
...  

A novel fabrication process to etch, to passivate, and to release single-crystal silicon structures totally in just only one process by inductively coupled plasma reactive ion etching (ICP-RIE) has been presented in this paper. Several kinds of movable actuators such as relay, comb-drive, and capacitance with thickness of 30 μm have been fabricated successfully to demonstrate this fabrication process. Here, experimental investigations about fabrication parameters to get well profile and suspension structures are performed in a STS ICP-RIE system.


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