Room-temperature water adsorption on the Si(100) surface examined by UPS, XPS, and static SIMS

1994 ◽  
Vol 81 (4) ◽  
pp. 449-463 ◽  
Author(s):  
Roland K. Schulze ◽  
John F. Evans
1996 ◽  
Vol 32 (8) ◽  
pp. 761 ◽  
Author(s):  
C.R. Kurkjian ◽  
M.J. Matthewson

ChemInform ◽  
2009 ◽  
Vol 40 (2) ◽  
Author(s):  
Bruce H. Lipshutz ◽  
David W. Chung ◽  
Brian Rich

Synlett ◽  
2017 ◽  
Vol 28 (16) ◽  
pp. 2153-2156 ◽  
Author(s):  
Wen-Ting Wei ◽  
Hongze Liang ◽  
Wen-Ming Zhu ◽  
Weida Liang ◽  
Yi Wu ◽  
...  

A radical–radical cross-coupling reaction of phenols with tert-butyl nitrite has been developed with the use of water as an additive. This method allows the construction of C–N bonds under an air atmosphere at room temperature, providing the ortho-nitrated phenol derivative in moderate to good yields.


Author(s):  
M. F. M. Tajudin ◽  
A. H. Ahmad ◽  
M. M. Rashidi

This paper highlights the effects of pouring temperature and holding time on the mechanical properties of aluminium 6061 semisolid feedstock billets. The semisolid metal feedstock billets were prepared by a direct thermal method (DTM), in which the molten metal was poured into a cylindrical copper mould with a different combination of pouring temperature and holding time before it was solidified in room temperature water. The results show that the sample with pouring temperature slightly above aluminium 6061 liquidus temperature has the lowest porosity, thereby the highest mechanical properties value. The sample with a pouring temperature of 660 °C and holding time of 60 s has the density, tensile strength and hardness properties of 2.701 g/cm3, 146.797 MPa, and 86.5 HV, respectively. Meanwhile, the sample at a pouring temperature of 640 °C and holding time of 20 s has density, tensile strength and hardness properties of 2.527 g/cm3, 65.39 MPa, and 71.79 HV, respectively. The density and fractography tests were conducted to confirm the existence of porosity within the samples. The results from these experimental works suggested that the mechanical properties of DTM semisolid feedstock billet merely depended on processing parameters, which influenced the porosity level within the feedstock billet, thus directly affected their mechanical properties.


2015 ◽  
Vol 69 ◽  
pp. 564-569 ◽  
Author(s):  
Seiichi Takami ◽  
Ken-ichi Sugioka ◽  
Kyohei Ozawa ◽  
Takao Tsukada ◽  
Tadafumi Adschiri ◽  
...  

Author(s):  
Said Abdul Ghafour Saeedy ◽  
Ahmad Faisal Faiz ◽  
Marjan Nikbakhtzadeh ◽  
Bagher Minaei Zangi ◽  
Mansoor Keshavarz

Drinking ice-cold water is prohibited in Avicenna’s “The Canon of Medicine” book in which he emphasized that ice-cold water drinking was hazardous for the body organs such as the liver. Little information can be found regarding the effects of ice-cold fluid drinks on liver and its probable sequels on this vital organ. Accordingly, we investigated the effects of long-term ice-cold water drink on the rat liver function and histology. Eighteen male Wistar rats, weighing 180±20 g, were randomly divided into three groups of six as two months ice-cold water drink, CW2M; three months ice-cold water drink, CW3M; and three months room temperature water drink; control group. Upon completion of the care period, a blood sample has been taken for liver enzymes and lipid profile assessment. Liver tissue has also been used for histological studies of H&E staining and microscopic examination. Histological findings showed hepatocellular micro-vesicle formation, necrosis and derangement of the cellular cords and infiltration of Kupffer cells in ice-cold water taken animals. Serum TGs, VLDL-C and ALP significantly increased with sound decrease in FBS and LDL-C in ice-cold water taken animals. It seems that long-term ice-cold water has deleterious functional and structural effects on the liver.


2011 ◽  
Vol 194-196 ◽  
pp. 1326-1332
Author(s):  
Jun You Liu ◽  
Jie Liu ◽  
Qing he Zhao ◽  
Jin Xiu Song

In order to prolong the life of inner liner of coke can, the thermal fatigue property of Cr17Mn10Ni3 heat-resisting steel was analyzed and studied from cast metallurgical structure, the morphology of crack surface and cross-section, the injury factor by OM, SEM, photoshop and imagetool software. The results shows, Cr17Mn10Ni3 has a good thermal fatigue property because of the microstructure with good thermal conductivity, austenite matrix and break carbide lying in treelike crystals. It decreases the innerstress and postpones the time of crack formation and extension, during the process with 1100°C and room- temperature water cooling. The cracks mainly appear in the phase interfaces between carbides and matrix, ferrite and austenite, and grain boundaries. The thin and deep cracks with high concentration are beneficial to relax the elastic strain energy. But a single and thick crack easily widens and deepens to be detrimental to the thermal fatigue property.


1990 ◽  
Vol 33 (8) ◽  
pp. 847-848
Author(s):  
Yu. D. Gorchakov ◽  
�. T. Frantsuz ◽  
S. N. Gershkovich ◽  
V. M. Khavinson ◽  
T. N. Musta

2014 ◽  
Vol 92 (1) ◽  
pp. 26-32 ◽  
Author(s):  
Jillian N. Murakami ◽  
Kevin B. Thurbide

The properties of subcritical water extraction (SWE) in the sample preparation of pharmaceutical tablets were investigated. Tablets comprised of microcrystalline cellulose excipients broke apart up to 80 times faster in subcritical water than they did in room temperature water, while those containing starch readily broke apart in either. Tablets containing starch were also observed to gelatinize or “paste” over several SWE conditions, impeding subsequent filtration and analysis. This effect was avoidable, however, since it was demonstrated to disappear with increases in extraction time and temperature or decreases in sample size. Using SWE, two common over-the-counter pharmaceuticals were extracted under optimized conditions from tablets comprised of either microcrystalline cellulose or starch excipients. Analyte recoveries of 95% or more were obtained at 150 °C for vitamin C (ascorbic acid) tablets in as little as 8 min for the extraction of a whole intact tablet, 6 min for two half tablets, and 5 min for a ground tablet. By comparison, this occurred at 250 °C in just 2 min for an intact slice of an acetaminophen tablet. Reproducibility was generally quite good with these trials producing RSD values of less than 2%. The results indicate that SWE can be a potentially viable and efficient method for the sample preparation of whole, sliced, or ground pharmaceutical tablets, and further exploration of this approach is promising.


Sign in / Sign up

Export Citation Format

Share Document