Enhanced mechanical properties in ceramic multilayer composites through integrating crystallographic texture and second-phase toughening

Author(s):  
Yuan Sun ◽  
Hang Xie ◽  
Linjing Liu ◽  
Qiangwei Kou ◽  
Shantao Zhang ◽  
...  
Author(s):  
H.-J. Kleebe ◽  
J.S. Vetrano ◽  
J. Bruley ◽  
M. Rühle

It is expected that silicon nitride based ceramics will be used as high-temperature structural components. Though much progress has been made in both processing techniques and microstructural control, the mechanical properties required have not yet been achieved. It is thought that the high-temperature mechanical properties of Si3N4 are limited largely by the secondary glassy phases present at triple points. These are due to various oxide additives used to promote liquid-phase sintering. Therefore, many attempts have been performed to crystallize these second phase glassy pockets in order to improve high temperature properties. In addition to the glassy or crystallized second phases at triple points a thin amorphous film exists at two-grain junctions. This thin film is found even in silicon nitride formed by hot isostatic pressing (HIPing) without additives. It has been proposed by Clarke that an amorphous film can exist at two-grain junctions with an equilibrium thickness.


Author(s):  
E. Sukedai ◽  
H. Mabuchi ◽  
H. Hashimoto ◽  
Y. Nakayama

In order to improve the mechanical properties of an intermetal1ic compound TiAl, a composite material of TiAl involving a second phase Ti2AIN was prepared by a new combustion reaction method. It is found that Ti2AIN (hexagonal structure) is a rod shape as shown in Fig.1 and its side surface is almost parallel to the basal plane, and this composite material has distinguished strength at elevated temperature and considerable toughness at room temperature comparing with TiAl single phase material. Since the property of the interface of composite materials has strong influences to their mechanical properties, the structure of the interface of intermetallic compound and nitride on the areas corresponding to 2, 3 and 4 as shown in Fig.1 was investigated using high resolution electron microscopy and image processing.


Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 79
Author(s):  
Ruopeng Lu ◽  
Kai Jiao ◽  
Yuhong Zhao ◽  
Kun Li ◽  
Keyu Yao ◽  
...  

Mg alloys with fine mechanical properties and high damping capacities are essential in engineering applications. In this work, Mg–Zn–Y based alloys with lamellar long period stacking ordered (LPSO) phases were obtained by different processes. The results show that a more lamellar second phase can be obtained in the samples with more solid solution atoms. The density of the lamellar LPSO phase has an obvious effect on the damping of the magnesium alloy. The compact LPSO phase is not conducive to dislocation damping, but sparse lamellar phases can improve the damping capacity without significantly reducing the mechanical properties. The Mg95.3Zn2Y2.7 alloy with lamellar LPSO phases and ~100 μm grain size exhibited a fine damping property of 0.110 at ε = 10–3.


2014 ◽  
Vol 58 ◽  
pp. 535-542 ◽  
Author(s):  
P. Shaterani ◽  
A. Zarei-Hanzaki ◽  
S.M. Fatemi-Varzaneh ◽  
S.B. Hassas-Irani

2011 ◽  
Vol 291-294 ◽  
pp. 1082-1086
Author(s):  
Yao Jin Wu ◽  
Zhi Ming Zhang ◽  
Bao Cheng Li ◽  
Bao Hong Zhang ◽  
Jian Min Yu ◽  
...  

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75) and extrusion temperature (300°C, 330°C, 360°C, 390°C, 420°C) on the mechanical properties and microstructure changes of AZ80 magnesium alloy have been investigated through tensile test and via ZEISS digital metallographic microscope observation. Research indicates that the alloy’s plasticity gradually decreases as the temperature increases, and that the alloy’s tensile strength varies with the extrusion ratio. At 330°C, the alloy’s particle grain is small and a small amount of black hard and brittle second-phase β (Mg17Al12) are precipitated uniformly along the grain boundary causing the gradual increase of the alloy’s tensile strength. When the extrusion temperature is up to 390°C, the grain size increases significantly, but the second phase precipitation along grain boundaries transforms into continuous and uniform-distribution precipitation within the grain. In this case, when the extrusion ratio is 60, the alloy’s tensile strength reaches its peak 390 Mpa. As the extrusion temperature increases, inhomogeneous precipitation of the second-phase along grain boundaries increases, causing the decrease of the alloy’s strength. At the same temperature, both the tensile strength and plasticity increases firstly and then decreases as extrusion ratio increases. With the gradual increase of the refinement grain, the dispersed precipitates increase and the alloy’s tensile strength and plasticity reach their peaks when the extrusion temperature is 390°C. As the grain grows, the second phase becomes inhomogeneous distribution, and the alloy’s strength and plasticity gradually decrease.


2021 ◽  
Vol 118 (6) ◽  
pp. 601
Author(s):  
Chunhui Jin ◽  
Honglin Zhou ◽  
Yuan Lai ◽  
Bei Li ◽  
Kewei Zhang ◽  
...  

The influence of aging temperature on microstructure and mechanical properties of Cr15Ni5 precipitation hardening stainless steel (15-5 PH stainless steel) were investigated at aging temperature range of 440–610 °C. The tensile properties at ambient temperature of the 15-5 PH stainless steel processed by different aging temperatures were tested, and the microstructural features were further analyzed utilizing optical microscope (OM), transmission electron microscope (TEM), electron backscatter diffraction (EBSD) as well as X-ray diffraction (XRD), respectively. Results indicated the strength of the 15-5 PH stainless steel was firstly decreased with increment of aging temperature from 440 to 540 °C, and then increased with the increment of aging temperature from 540 to 610 °C. The strength and ductility were well matched at aging temperature 470 °C, and the yield strength, tensile strength as well as elongation were determined to be 1170 MPa, 1240 MPa and 24%, respectively. The microstructures concerning to different aging temperatures were overall confirmed to be lath martensite. The strengthening mechanisms induced by dislocation density and the second phase precipitation of Cu-enriched metallic compound under different aging temperatures were determined to be the predominant strengthening mechanisms controlling the variation trend of mechanical properties corresponding to different aging temperatures with respect to 15-5 PH stainless steel.


2010 ◽  
Vol 139-141 ◽  
pp. 180-184
Author(s):  
Yong Xue ◽  
Zhi Min Zhang ◽  
Li Hui Lang

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75) and extrusion temperatures (300°C, 330°C, 360°C, 390°C, 420°C) on the mechanical properties and microstructure of homogenized AZ80 alloy have been investigated through the tensile tests and via metallographic microscope observation. The results show that the alloy’s grain is small and small amounts of black hard and brittle second-phase β (Mg17Al12) are precipitated uniformly along the grain boundary causing the gradual increase of the alloy’s tensile strength at 330°C. When the extrusion temperature is up to 390°C, the grain size increases significantly, but the second phase precipitation along grain boundaries transforms into continuous and uniform-distribution precipitation within the grain. In this case, when the extrusion ratio is 60, the alloy’s tensile strength reaches its peak 390Mpa. As the extrusion temperature increases, inhomogeneous precipitation of the second-phase along grain boundaries increases, causing the decrease of the alloy’s strength. At the same temperature, the tensile strength increases firstly and then decreases as extrusion ratio increases. With the gradual increase of the refinement grain, the dispersed precipitates increase and the alloy’s tensile strength and plasticity reach their peaks when the extrusion temperature is 390°C. As the grain grows, the second phase becomes inhomogeneous distribution, and the alloy’s strength and plasticity gradually decrease.


Metals ◽  
2020 ◽  
Vol 10 (3) ◽  
pp. 385
Author(s):  
Yushi Qi ◽  
Heng Wang ◽  
Lili Chen ◽  
Hongming Zhang ◽  
Gang Chen ◽  
...  

A ZK61-Y magnesium (Mg) alloy wheel hub was prepared via liquid forging—isothermal forging process. The effects of Y-element contents on the microstructure and mechanical properties of liquid forging blanks were investigated. The formation order of the second phase was I-phase (Mg3Zn6Y) → W-phase (Mg3Zn3Y2) → Z-phase (Mg12ZnY) with the increase of the Y-element content. Meanwhile, the I-phase and Z-phase formed in the liquid forging process were beneficial to the grain refinement. The numerical simulation of the isothermal forging process was carried out to analyze the effects of forming temperature on the temperature and stress field in the forming parts using the software Deform-3D. Isothermal forging experiments and post heat treatments were conducted. The influence of isothermal forging temperature, heat treatment temperature and preservation time on the microstructure and mechanical properties of the forming parts were also studied. The dynamic recrystallization (DRX), second-phase hardening, and work hardening account for the improvement of properties after the isothermal forging process. The forming part forged at 380 °C displayed the outstanding properties. The elongation, yield strength, and ultimate tensile strength were 18.5%, 150 MPa and 315 MPa, respectively. The samples displayed an increased elongation and decreased strength after heat treatments. The 520 °C—1 h sample possessed the best mechanical properties, the elongation was 25.5%, the yield stress was 125 MPa and the ultimate tensile strength was 282 MPa. This can be ascribed to the recrystallization and the elimination of working hardening. Meanwhile, the second phase transformation (I-phase → W-phase → Mg2Y + MgZn2), dissolution, and decomposition can be observed, as well.


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